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ASTM E 291 : 1996

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Methods for Chemical Analysis of Caustic Soda and Caustic Potash (Sodium Hydroxide and Potassium Hydroxide)

Superseded date

11-11-2014

Superseded by

ASTM E 291 : 2001

Published date

10-10-2001

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Committee
E 15
DocumentType
Test Method
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy

1.1 These test methods cover only the analyses usually required on the following commercial products:

1.1.1 Caustic soda (sodium hydroxide), 50 and 73 % liquors; anhydrous (solid, flake, ground, or powdered), and

1.1.2 Caustic potash (potassium hydroxide), 45 % liquor; anhydrous (solid, flake, ground, or powdered).

1.2 The analytical procedures appear in the following order:

Alkalinity (Total), Titrimetric (for 50 to 100 %NaOH and 45 to 100 % KOH)8 to 14
Carbonate, Gas-Volumetric (0.001 g CO 2, min)15 to 24
Carbonate, Gravimetric (0.001 g CO 2, min)25 to 33
Chloride, Titrimetric, (0.001 g Cl , min)34 to 40
Chloride, Potentiometric Titration (0.3 to 1.2 %)41 to 47
Chloride, Ion Selective Electrode (0.6 to 120 ppm)48 to 55
Iron, Photometric (0.005 mg Fe, min)56 to 64
Sulfate, Gravimetric, (0.002 g SO 3, min)65 to 71
Keywords72

1.3 The values stated in inch-pound units are to be regarded as the standard. The values in parentheses are provided for information only.

1.4 Review the current Material Safety Data Sheet (MSDS) for detailed information concerning toxicity, first-aid procedures, handling, and safety precautions.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 6.

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