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ASTM E 2994 : 2021

Current

Current

The latest, up-to-date edition.

Standard Test Method for Analysis of Titanium and Titanium Alloys by Spark Atomic Emission Spectrometry and Glow Discharge Atomic Emission Spectrometry (Performance-Based Method)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

06-01-2022

€61.92
Excluding VAT

Committee
E 01
DocumentType
Test Method
Pages
15
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1This test method describes the analysis of titanium and its alloys by spark atomic emission spectrometry (Spark-AES) and glow discharge atomic emission spectrometry (GD-AES). The titanium specimen to be analyzed may be in the form of a disk, casting, foil, sheet, plate, extrusion, or some other wrought form or shape. The elements and ranges covered in the scope by spark-AES of this test method are listed below.

Element

Tested Mass Fraction Range (%)

Aluminum

0.008 to 7.0

Chromium

0.006 to 0.1

Copper

0.014 to 0.1

Iron

0.043 to 0.3

Manganese

0.005 to 0.1

Molybdenum

0.014 to 0.1

Nickel

0.006 to 0.1

Silicon

0.018 to 0.1

Tin

0.02 to 0.1

Vanadium

0.015 to 5.0

Zirconium

0.013 to 0.1

1.1.1The elements oxygen, nitrogen, carbon, niobium, boron, yttrium, palladium, and ruthenium, were included in the ILS but the data did not contain the required six laboratories. Precision tables were provided for informational use only.

1.2The elements and ranges covered in the scope by GD-AES of this test method are listed below.

Element

Tested Mass Fraction Range (%)

Aluminum

0.02 to 7.0

Carbon

0.02 to 0.1

Chromium

0.006 to 0.1

Copper

0.028 to 0.1

Iron

0.09 to 0.3

Molybdenum

0.016 to 0.1

Nickel

0.006 to 0.1

Silicon

0.018 to 0.1

Tin

0.022 to 0.1

Vanadium

0.054 to 5.0

Zirconium

0.026 to 0.1

1.2.1The elements boron, manganese, oxygen, nitrogen, niobium, yttrium, palladium, and ruthenium were included in the ILS, but the data did not contain the required six laboratories. Precision tables were provided for informational use only.

1.3The elements and mass fractions given in the above scope tables are the ranges validated through the interlaboratory study. However, it is known that the techniques used in this standard allow the useable range, for the elements listed, to be extended higher or lower based on individual instrument capability, available reference materials, laboratory capabilities, and the spectral characteristics of the specific element wavelength being used. It is also acceptable to analyze elements not listed in 1.1 or 1.2 and still meet compliance to this standard test method. Laboratories must provide sufficient evidence of method validation when extending the analytical range or when analyzing elements not reported in Section 18 (Precision and Bias), as described in Guide E2857.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM F 1108 : 2021 Standard Specification for Titanium-6Aluminum-4Vanadium Alloy Castings for Surgical Implants (UNS R56406)
ASTM F 1472 : 2020 : REV A Standard Specification for Wrought Titanium-6Aluminum-4Vanadium Alloy for Surgical Implant Applications (UNS R56400)
ASTM F 2989 : 2021 Standard Specification for Metal Injection Molded Unalloyed Titanium Components for Surgical Implant Applications
ASTM B 861 : 2019 Standard Specification for Titanium and Titanium Alloy Seamless Pipe
ASTM B 862 : 2019 Standard Specification for Titanium and Titanium Alloy Welded Pipe
ASTM F 620 : 2020 Standard Specification for Titanium Alloy Forgings for Surgical Implants in the Alpha Plus Beta Condition
ASTM B 381 : 2021 Standard Specification for Titanium and Titanium Alloy Forgings
ASTM B 348/B348M : 2021 Standard Specification for Titanium and Titanium Alloy Bars and Billets
ASTM F 3046 : 2021 Standard Specification for Wrought Titanium-3Aluminum-2.5Vanadium Alloy for Surgical Implant Applications (UNS R56320)
ASTM B 1009 : 2020 Standard Specification for Titanium Alloy Bars for Near Surface Mounts in Civil Structures
ASTM B 863 : 2019 Standard Specification for Titanium and Titanium Alloy Wire
SAE AMS6901D Titanium Alloy Bars, Forgings, and Forging Stock, 5Al - 2.5Sn, Extra Low Interstitial, Annealed
SAE AMS4934J Titanium Alloy, Extrusions and Flash Welded Rings, 6Al - 4V, Solution Heat Treated and Aged
SAE AMS6952A Titanium Alloy, Forgings 5.8Al - 4.0Sn - 3.5Zr - 2.8Mo - 0.7Nb - 0.35Si - 0.06C Solution and Precipitation Heat Treated
SAE AMS4895 Titanium Alloy, Round Bars 5Al - 1Fe Annealed

ASTM E 29 : 2013 : R2019 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 2857 : 2021 Standard Guide for Validating Analytical Methods
ASTM E 135 : 2023 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2024 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2021 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 135 : 2023 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 2857 : 2022 Standard Guide for Validating Analytical Methods
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 135 : 2022 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 2857 : 2011 : R2021 : EDT 1 Standard Guide for Validating Analytical Methods
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 135 : 2022 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2022 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

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