• Shopping Cart
    There are no items in your cart

ASTM E 3 : 2011 : R2017

Current

Current

The latest, up-to-date edition.

Standard Guide for Preparation of Metallographic Specimens

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

12-06-2017

€61.92
Excluding VAT

CONTAINED IN VOL. 03.01, 2017 Provides metallographic examinations to reveal the constituents and structure of metals and their alloys by means of a light optical or scanning electron microscope.

Committee
E 04
DevelopmentNote
Supersedes ASTM E 5 (12/2001)
DocumentType
Guide
Pages
12
ProductNote
Reconfirmed 2017
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1The primary objective of metallographic examinations is to reveal the constituents and structure of metals and their alloys by means of a light optical or scanning electron microscope. In special cases, the objective of the examination may require the development of less detail than in other cases but, under nearly all conditions, the proper selection and preparation of the specimen is of major importance. Because of the diversity in available equipment and the wide variety of problems encountered, the following text presents for the guidance of the metallographer only those practices which experience has shown are generally satisfactory; it cannot and does not describe the variations in technique required to solve individual specimen preparation problems.

Note 1:For a more extensive description of various metallographic techniques, refer to Samuels, L. E., Metallographic Polishing by Mechanical Methods, American Society for Metals (ASM) Metals Park, OH, 3rd Ed., 1982; Petzow, G., Metallographic Etching, ASM, 1978; and VanderVoort, G., Metallography: Principles and Practice, McGraw Hill, NY, 2nd Ed., 1999.

1.2This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

1.3This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM B 552 : 2019 Standard Specification for Seamless and Welded Copper–Nickel Tubes for Water Desalting Plants
ASTM G 46 : 2021 Standard Guide for Examination and Evaluation of Pitting Corrosion
ASTM E 2014 : 2017 Standard Guide on Metallographic Laboratory Safety
ASTM B 961 : 2013 : R2019 Standard Specification for Silver Coated Copper and Copper Alloy Stranded Conductors for Electronic Space Application
ASTM E 1181 : 2002 : R2023 Standard Test Methods for Characterizing Duplex Grain Sizes
ASTM F 1466 : 2020 Standard Specification for Iron-Nickel-Cobalt Alloys for Metal-to-Ceramic Sealing Applications (Withdrawn 2024)
ASTM B 395/B395M : 2018 Standard Specification for U-Bend Seamless Copper and Copper Alloy Heat Exchanger and Condenser Tubes
ASTM E 768 : 1999 : R2018 Standard Guide for Preparing and Evaluating Specimens for Automatic Inclusion Assessment of Steel
ASTM A 962/A962M : 2022 Standard Specification for Common Requirements for Bolting Intended for Use at Any Temperature from Cryogenic to the Creep Range
ASTM B 640 : 2012 : REV A : R2021 Standard Specification for Welded Copper Tube for Air Conditioning and Refrigeration Service
ASTM E 2015 : 2004 : R2021 Standard Guide for Preparation of Plastics and Polymeric Specimens for Microstructural Examination
ASTM E 2789 : 2010 : R2021 Standard Guide for Fretting Fatigue Testing
ASTM B 748 : 1990 : R2021 Standard Test Method for Measurement of Thickness of Metallic Coatings by Measurement of Cross Section with a Scanning Electron Microscope
ASTM E 606/E606M : 2021 Standard Test Method for Strain-Controlled Fatigue Testing
ASTM E 2283 : 2008 : R2019 Standard Practice for Extreme Value Analysis of Nonmetallic Inclusions in Steel and Other Microstructural Features
ASTM E 930 : 2018 Standard Test Methods for Estimating the Largest Grain Observed in a Metallographic Section (ALA Grain Size)
ASTM B 834 : 2022 Standard Specification for Pressure Consolidated Powder Nickel Alloy Pipe Flanges, Fittings, Valves, and Parts
ASTM A 681 : 2008 : R2022 Standard Specification for Tool Steels Alloy
ASTM F 1854 : 2015 Standard Test Method for Stereological Evaluation of Porous Coatings on Medical Implants (Withdrawn 2024)
ASTM B 1005 : 2017 Standard Specification for Copper-Clad Aluminum Bar for Electrical Purposes (Bus Bar)
ASTM B 379 : 2020 Standard Specification for Phosphorized Coppers—Refinery Shapes
ASTM A 579/A579M : 2020 Standard Specification for Superstrength Alloy Steel Forgings (Withdrawn 2024)
ASTM B 1014 : 2020 Standard Specification for Welded Copper and Copper Alloy Condenser and Heat Exchanger Tubes with a Textured Surface(s)
ASTM B 280 : 2020 Standard Specification for Seamless Copper Tube for Air Conditioning and Refrigeration Field Service
ASTM G 161 : 2000 : R2018 Standard Guide for Corrosion-Related Failure Analysis
ASTM B 68/B68M : 2019 Standard Specification for Seamless Copper Tube, Bright Annealed
ASTM B 129 : 2022 Standard Specification for Cartridge Brass Cartridge Case Cups
ASTM B 837 : 2019 Standard Specification for Seamless Copper Tube for Natural Gas and Liquified Petroleum (LP) Gas Fuel Distribution Systems
ASTM B 131 : 2022 Standard Specification for Copper Alloy Bullet Jacket Cups
ASTM E 2368 : 2010 : R2017 Standard Practice for Strain Controlled Thermomechanical Fatigue Testing
ASTM E 2567 : 2016 : REV A : R2023 Standard Test Method for Determining Nodularity And Nodule Count In Ductile Iron Using Image Analysis
ASTM F 29 : 1997 : R2022 Standard Specification for Dumet Wire for Glass-to-Metal Seal Applications (Withdrawn 2024)
ASTM F 3554 : 2022 Standard Specification for Additive Manufacturing – Finished Part Properties – Grade 4340 (UNS G43400) via Laser Beam Powder Bed Fusion for Transportation Applications
ASTM F 44 : 2021 Standard Specification for Metallized Surfaces on Ceramic (Withdrawn 2023)
ASTM F 15 : 2004 : R2022 Standard Specification for Iron-Nickel-Cobalt Sealing Alloy (Withdrawn 2024)
ASTM E 2142 : 2008 : R2015 Standard Test Methods for Rating and Classifying Inclusions in Steel Using the Scanning Electron Microscope
ASTM F 561 : 2019 Standard Practice for Retrieval and Analysis of Medical Devices, and Associated Tissues and Fluids
ASTM F 880M : 2016 Standard Specification for Stainless Steel Socket Set Screws (Metric) (Withdrawn 2023)
ASTM F 2328M : 2017 : R2022 Standard Test Method for Determining Decarburization and Carburization in Hardened and Tempered Threaded Steel Bolts, Screws, Studs, and Nuts (Metric)
ASTM E 1382 : 1997 : R2023 Standard Test Methods for Determining Average Grain Size Using Semiautomatic and Automatic Image Analysis
ASTM B 359/B359M : 2018 Standard Specification for Copper and Copper-Alloy Seamless Condenser and Heat Exchanger Tubes With Integral Fins
ASTM F 2885 : 2017 : R2023 Standard Specification for Metal Injection Molded Titanium-6Aluminum-4Vanadium Components for Surgical Implant Applications
ASTM E 45 : 2018 : REV A Standard Test Methods for Determining the Inclusion Content of Steel
ASTM G 209 : 2014 : R2022 Standard Practice for Detecting mu-phase in Wrought Nickel-Rich, Chromium, Molybdenum-Bearing Alloys
ASTM F 3213 : 2017 Standard for Additive Manufacturing – Finished Part Properties – Standard Specification for Cobalt-28 Chromium-6 Molybdenum via Powder Bed Fusion
ASTM F 3318 : 2018 Standard for Additive Manufacturing – Finished Part Properties – Specification for AlSi10Mg with Powder Bed Fusion – Laser Beam
ASTM G 30 : 2022 Standard Practice for Making and Using U-Bend Stress-Corrosion Test Specimens
ASTM B 743 : 2023 Standard Specification for Seamless Copper Tube in Coils
ASTM E 340 : 2015 Standard Practice for Macroetching Metals and Alloys
ASTM E 92 : 2017 Standard Test Methods for Vickers Hardness and Knoop Hardness of Metallic Materials
ASTM B 795 : 2020 Standard Test Method for Determining the Percentage of Alloyed or Unalloyed Iron Contamination Present in Powder Forged (PF) Steel Materials
ASTM E 466 : 2021 Standard Practice for Conducting Force Controlled Constant Amplitude Axial Fatigue Tests of Metallic Materials
ASTM B 919 : 2019 Standard Specification for Welded Copper Heat Exchanger Tubes With Internal Enhancement
ASTM B 643 : 2018 Standard Specification for Copper-Beryllium Alloy Seamless Tube
ASTM F 3184 : 2016 Standard Specification for Additive Manufacturing Stainless Steel Alloy (UNS S31603) with Powder Bed Fusion
ASTM F 3001 : 2014 : R2021 Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed Fusion
ASTM B 506 : 2022 Standard Specification for Copper-Clad Stainless Steel Sheet and Strip for Building Construction
ASTM E 1351 : 2001 : R2020 Standard Practice for Production and Evaluation of Field Metallographic Replicas
ASTM E 1405 : 1998 : R2022 Standard Specification for Laboratory Glass Distillation Flasks
ASTM F 3302 : 2018 Standard for Additive Manufacturing – Finished Part Properties – Standard Specification for Titanium Alloys via Powder Bed Fusion
ASTM B 577 : 2019 Standard Test Methods for Detection of Cuprous Oxide (Hydrogen Embrittlement Susceptibility) in Copper
ASTM E 235/E235M : 2019 Standard Specification for Type K and Type N Mineral-Insulated, Metal-Sheathed Thermocouples for Nuclear or for Other High-Reliability Applications
ASTM G 108 : 1994 : R2015 Standard Test Method for Electrochemical Reactivation (EPR) for Detecting Sensitization of AISI Type 304 and 304L Stainless Steels
ASTM F 75 : 2023 Standard Specification for Cobalt-28 Chromium-6 Molybdenum Alloy Castings and Casting Alloy for Surgical Implants (UNS R30075)
ASTM G 146 : 2001 : R2018 Standard Practice for Evaluation of Disbonding of Bimetallic Stainless Alloy/Steel Plate for Use in High-Pressure, High-Temperature Refinery Hydrogen Service
ASTM B 848/B848M : 2021 Standard Specification for Powder Forged (PF) Ferrous Materials
ASTM B 130 : 2019 Standard Specification for Commercial Bronze Strip for Bullet Jackets
ASTM F 3056 : 2014 : R2021 Standard Specification for Additive Manufacturing Nickel Alloy (UNS N06625) with Powder Bed Fusion
ASTM E 112 : 2013 : R2021 Standard Test Methods for Determining Average Grain Size
ASTM A 600 : 1992 : REV A : R2016 Standard Specification for Tool Steel High Speed
ASTM E 1245 : 2003 : R2023 Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis
ASTM E 384 : 2022 Standard Test Method for Microindentation Hardness of Materials
ASTM A 684/A684M : 2017 Standard Specification for Steel, Strip, High-Carbon, Cold-Rolled
ASTM B 19 : 2020 Standard Specification for Cartridge Brass Sheet, Strip, Plate, Bar, and Disks
ASTM B 476 : 2021 Standard Specification for General Requirements for Wrought Precious Metal Electrical Contact Materials
ASTM E 2546 : 2015 Standard Practice for Instrumented Indentation Testing
ASTM B 249/B249M : 2022 Standard Specification for General Requirements for Wrought Copper and Copper-Alloy Rod, Bar, Shapes and Forgings
ASTM G 4 : 2001 : R2014 Standard Guide for Conducting Corrosion Tests in Field Applications (Withdrawn 2023)
ASTM B 777 : 2015 : R2020 Standard Specification for Tungsten Base, High-Density Metal
ASTM B 1003 : 2016 Standard Specification for Seamless Copper Tube for Linesets
ASTM A 247 : 2019 Standard Test Method for Evaluating the Microstructure of Graphite in Iron Castings
ASTM F 912 : 2011 : R2017 Standard Specification for Alloy Steel Socket Set Screws
ASTM F 256 : 2005 : R2020 Standard Specification for Chromium-Iron Sealing Alloys with 18 or 28 Percent Chromium (Withdrawn 2023)
ASTM A 892 : 2009 : R2020 Standard Guide for Defining and Rating the Microstructure of High Carbon Bearing Steels
ASTM C 1220 : 2021 Standard Test Method for Static Leaching of Monolithic Waste Forms for Disposal of Radioactive Waste
ASTM F 2989 : 2021 Standard Specification for Metal Injection Molded Unalloyed Titanium Components for Surgical Implant Applications
ASTM G 110 : 1992 : R2022 : EDT 2 Standard Practice for Evaluating Intergranular Corrosion Resistance of Heat Treatable Aluminum Alloys by Immersion in Sodium Chloride + Hydrogen Peroxide Solution
ASTM E 1508 : 2012 : REV A : R2019 Standard Guide for Quantitative Analysis by Energy-Dispersive Spectroscopy
ASTM D 1654 : 2008 : R2016 : EDT 1 Standard Test Method for Evaluation of Painted or Coated Specimens Subjected to Corrosive Environments
ASTM B 797 : 2020 Standard Test Method for Surface Finger-Oxide Penetration Depth and Presence of Interparticle Oxide Networks in Powder Forged (PF) Steel Parts
ASTM F 1108 : 2021 Standard Specification for Titanium-6Aluminum-4Vanadium Alloy Castings for Surgical Implants (UNS R56406)
ASTM F 2111 : 2022 Standard Practice for Measuring Intergranular Attack or End Grain Pitting on Metals Caused by Aircraft Chemical Processes
ASTM E 839 : 2011 : R2016 : EDT 1 Standard Test Methods for Sheathed Thermocouples and Sheathed Thermocouple Cable
ASTM B 587 : 2019 Standard Specification for Welded Brass Tube
ASTM A 686 : 1992 : R2016 Standard Specification for Tool Steel, Carbon
ASTM E 562 : 2019 : EDT 1 Standard Test Method for Determining Volume Fraction by Systematic Manual Point Count
ASTM B 152/B152M : 2019 Standard Specification for Copper Sheet, Strip, Plate, and Rolled Bar
ASTM B 487 : 2020 Standard Test Method for Measurement of Metal and Oxide Coating Thickness by Microscopical Examination of Cross Section
ASTM G 34 : 2001 : R2018 : EDT 1 Standard Test Method for Exfoliation Corrosion Susceptibility in 2XXX and 7XXX Series Aluminum Alloys (EXCO Test)
ASTM B 251/B251M : 2017 Standard Specification for General Requirements for Wrought Seamless Copper and Copper-Alloy Tube
ASTM F 2886 : 2017 Standard Specification for Metal Injection Molded Cobalt-28Chromium-6Molybdenum Components for Surgical Implant Applications
ASTM B 747 : 2020 Standard Specification for Copper-Zirconium Alloy Sheet and Strip
ASTM B 694 : 2019 Standard Specification for Copper, Copper-Alloy, Copper-Clad Bronze (CCB), Copper-Clad Stainless Steel (CCS), and Copper-Clad Alloy Steel (CAS) Sheet and Strip for Electrical Cable Shielding
ASTM A 262 : 2015 : R2021 Standard Practices for Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels
ASTM B 796 : 2020 Standard Test Method for Nonmetallic Inclusion Content of Ferrous Powders Intended for Powder Forging (PF) Applications
ASTM B 447 : 2012 : REV A : R2021 Standard Specification for Welded Copper Tube
ASTM B 740 : 2021 Standard Specification for Copper-Nickel-Tin Spinodal Alloy Strip
ASTM F 3055 : 2014 : REV A : R2021 Standard Specification for Additive Manufacturing Nickel Alloy (UNS N07718) with Powder Bed Fusion
ASTM F 2924 : 2014 : R2021 Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium with Powder Bed Fusion
ASTM F 2328 : 2017 : R2022 Standard Test Method for Determining Decarburization and Carburization in Hardened and Tempered Threaded Steel Bolts, Screws, Studs, and Nuts
ASTM E 2109 : 2001 : R2021 Standard Test Methods for Determining Area Percentage Porosity in Thermal Sprayed Coatings
ASTM B 543/B543M : 2018 Standard Specification for Welded Copper and Copper-Alloy Heat Exchanger Tube
ASTM B 569 : 2019 Standard Specification for Brass Strip in Narrow Widths and Light Gage for Heat-Exchanger Tubing
ASTM E 2207 : 2015 : R2021 Standard Practice for Strain-Controlled Axial-Torsional Fatigue Testing with Thin-Walled Tubular Specimens
ASTM E 82/E82M : 2014 : R2019 Standard Test Method for Determining the Orientation of a Metal Crystal
ASTM B 250/B250M : 2019 Standard Specification for General Requirements for Wrought Copper Alloy Wire
ASTM F 3122 : 2014 : R2022 Standard Guide for Evaluating Mechanical Properties of Metal Materials Made via Additive Manufacturing Processes
ASTM B 903 : 2015 : R2022 Standard Specification for Seamless Copper Heat Exchanger Tubes With Internal Enhancement
ASTM E 1268 : 2019 Standard Practice for Assessing the Degree of Banding or Orientation of Microstructures
ASTM C 664 : 2010 : R2020 Standard Test Methods for Thickness of Diffusion Coating
ASTM E 1180 : 2008 : R2021 Standard Practice for Preparing Sulfur Prints for Macrostructural Evaluation

ASTM E 1245 : 2003 Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis
ASTM E 1268 : 1999 Standard Practice for Assessing the Degree of Banding or Orientation of Microstructures
ASTM E 1077 : 2014 Standard Test Methods for Estimating the Depth of Decarburization of Steel Specimens
ASTM E 1077 : 2014 : R2021 Standard Test Methods for Estimating the Depth of Decarburization of Steel Specimens
ASTM E 7 : 2017 : REDLINE Standard Terminology Relating to Metallography
ASTM A 90/A90M : 2021 Standard Test Method for Weight [Mass] of Coating on Iron and Steel Articles with Zinc or Zinc-Alloy Coatings
ASTM E 1920 : 2003 Standard Guide for Metallographic Preparation of Thermal Sprayed Coatings
ASTM E 1245 : 1995 Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis
ASTM E 1558 : 2009 : R2014 Standard Guide for Electrolytic Polishing of Metallographic Specimens
ASTM A 90/A90M : 2013 : R2018 Standard Test Method for Weight [Mass] of Coating on Iron and Steel Articles with Zinc or Zinc-Alloy Coatings
ASTM E 7 : 2017 Standard Terminology Relating to Metallography
ASTM E 1122 : 1996 : R2002 Standard Practice for Obtaining JK Inclusion Ratings Using Automatic Image Analysis (Withdrawn 2006)
ASTM E 1245 : 2003 : R2008 Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis
ASTM E 1920 : 2003 : R2021 Standard Guide for Metallographic Preparation of Thermal Sprayed Coatings
ASTM E 45 : 1997 : EDT 2 Standard Test Methods for Determining the Inclusion Content of Steel
ASTM E 45 : 2018 : REV A Standard Test Methods for Determining the Inclusion Content of Steel
ASTM E 7 : 2022 Standard Terminology Relating to Metallography
ASTM E 1268 : 2001 Standard Practice for Assessing the Degree of Banding or Orientation of Microstructures
ASTM E 1077 : 1991 : R1997 Standard Test Methods for Estimating the Depth of Decarburization of Steel Specimens
ASTM E 1268 : 2001 : R2016 Standard Practice for Assessing the Degree of Banding or Orientation of Microstructures
ASTM E 768 : 1999 : R2018 Standard Guide for Preparing and Evaluating Specimens for Automatic Inclusion Assessment of Steel
ASTM E 1558 : 1999 Standard Guide for Electrolytic Polishing of Metallographic Specimens
ASTM E 1077 : 2014 : REDLINE Standard Test Methods for Estimating the Depth of Decarburization of Steel Specimens
ASTM E 1920 : 2003 : R2014 Standard Guide for Metallographic Preparation of Thermal Sprayed Coatings
ASTM E 45 : 2018 : REV A : R2023 Standard Test Methods for Determining the Inclusion Content of Steel
ASTM E 1558 : 2009 Standard Guide for Electrolytic Polishing of Metallographic Specimens
ASTM E 1245 : 2000 Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis
ASTM E 1077 : 2001 : EDT 1 Standard Test Methods for Estimating the Depth of Decarburization of Steel Specimens
ASTM E 1077 : 2001 : R2005 Standard Test Methods for Estimating the Depth of Decarburization of Steel Specimens
ASTM E 1077 : 2001 Standard Test Methods for Estimating the Depth of Decarburization of Steel Specimens
ASTM E 1122 : 1996 Standard Practice for Obtaining JK Inclusion Ratings Using Automatic Image Analysis
ASTM E 1245 : 2003 : R2016 Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis
ASTM E 1558 : 2009 : R2021 Standard Guide for Electrolytic Polishing of Metallographic Specimens
ASTM E 1920 : 2003 : R2008 Standard Guide for Metallographic Preparation of Thermal Sprayed Coatings
ASTM E 1268 : 2018 Standard Practice for Assessing the Degree of Banding or Orientation of Microstructures
ASTM E 1268 : 2001 : R2007 Standard Practice for Assessing the Degree of Banding or Orientation of Microstructures
ASTM E 1920 : 1997 Standard Guide for Metallographic Preparation of Thermal Sprayed Coatings
ASTM E 1245 : 2003 : R2023 Standard Practice for Determining the Inclusion or Second-Phase Constituent Content of Metals by Automatic Image Analysis

Access your standards online with a subscription

Features

  • Simple online access to standards, technical information and regulations.

  • Critical updates of standards and customisable alerts and notifications.

  • Multi-user online standards collection: secure, flexible and cost effective.