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ASTM E 352 : 2018 : EDT 1

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Methods for Chemical Analysis of Tool Steels and Other Similar Medium- and High-Alloy Steels

Available format(s)

Hardcopy , PDF

Superseded date

23-12-2023

Superseded by

ASTM E 352 : 2023

Language(s)

English

Published date

23-02-2022

€96.91
Excluding VAT

Committee
E 01
DocumentType
Test Method
Pages
38
ProductNote
ε1NOTE—An editorial correction was made in Table 5 in February 2022.
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1These test methods cover the chemical analysis of tool steels and other similar medium- and high-alloy steels having chemical compositions within the following limits:

Element

Composition Range, %

Aluminum

  0.005 to 1.5

Boron

  0.001 to 0.10

Carbon

  0.03  to 2.50

Chromium

  0.10  to 14.0

Cobalt

  0.10  to 14.0

Copper

  0.01  to 2.0

Lead

  0.001 to 0.01

Manganese

  0.10  to 15.00

Molybdenum

  0.01  to 10.00

Nickel

  0.02  to 4.00

Nitrogen

  0.001 to 0.20

Phosphorus

  0.002 to 0.05

Silicon

  0.10  to 2.50

Sulfur

  0.002 to 0.40

Tungsten

  0.01  to 21.00

Vanadium

  0.02  to 5.50

1.2The test methods in this standard are contained in the sections indicated below:

Sections

Carbon, Total, by the Combustion—
 Thermal Conductivity Method—
Discontinued 1986

125–135

Carbon, Total, by the Combustion Gravimetric
 Method—Discontinued 2012

78–88

Chromium by the Atomic Absorption
 Spectrometry Method

(0.006 % to 1.00 %)

174–183

Chromium by the Peroxydisulfate
 Oxidation—Titration Method

  (0.10 % to 14.00 %)

184–192

Chromium by the Peroxydisulfate-Oxidation
 Titrimetric Method—Discontinued 1980

117–124

Cobalt by the Ion-Exchange—
 Potentiometric Titration Method

    (2 % to 14 %) 

52–59

Cobalt by the Nitroso-R-Salt
  Spectrophotometric Method

 (0.10 % to 5.0 %) 

60–69

Copper by the Neocuproine
  Spectrophotometric Method

 (0.01 % to 2.00 %)

89–98

Copper by the Sulfide Precipitation-
 Electrodeposition Gravimetric Method

  (0.01 % to 2.0 %) 

70–77

Lead by the Ion-Exchange—Atomic
  Absorption Spectrometry Method

(0.001 % to 0.01 %)

99–108

Manganese by the Periodate
  Spectrophotometric Method

 (0.10 % to 5.00 %)

9–18

Molybdenum by the Ion Exchange–
 8-Hydroxyquinoline Gravimetric Method 

203–210

Molybdenum by the Thiocyanate Spectrophotometric Method

 (0.01 % to 1.50 %)

162–173

Nickel by the Dimethylglyoxime
 Gravimetric Method

(0.1 % to 4.0 %)

144–151

Phosphorus by the Alkalimetric Method

 (0.01 % to 0.05 %)

136–143

Phosphorus by the Molybdenum Blue
  Spectrophotometric Method

(0.002 % to 0.05 %)

19–29

Silicon by the Gravimetric Method

 (0.10 % to 2.50 %)

45–51

Sulfur by the Gravimetric
 Method—Discontinued 1988

29–35

Sulfur by the Combustion-Iodate
  Titration Method—Discontinued 2012

36–44

Sulfur by the Chromatographic
 Gravimetric Method—Discontinued 1980

109–116

Tin by the Solvent Extraction—
 Atomic Absorption Spectrometry Method

(0.002 % to 0.10 %)

152–161

Vanadium by the Atomic
 Absorption Spectrometry Method

(0.006 % to 0.15 %)

193–202

1.3Test methods for the determination of carbon and sulfur not included in this standard can be found in Test Methods E1019.

1.4Some of the composition ranges given in 1.1 are too broad to be covered by a single test method and therefore this standard contains multiple test methods for some elements. The user must select the proper test method by matching the information given in the Scope and Interference sections of each test method with the composition of the alloy to be analyzed.

1.5The values stated in SI units are to be regarded as standard.

1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 6 and in special “Warning” paragraphs throughout these test methods.

1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM E 350 : 2018 Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron
ASTM E 351 : 2018 Standard Test Methods for Chemical Analysis of Cast Iron—All Types
ASTM E 1473 : 2016 Standard Test Methods for Chemical Analysis of Nickel, Cobalt and High-Temperature Alloys
ASTM B 733 : 2021 Standard Specification for Autocatalytic (Electroless) Nickel-Phosphorus Coatings on Metal
ASTM A 751 : 2021 Standard Test Methods and Practices for Chemical Analysis of Steel Products
ASTM B 733 : 2022 Standard Specification for Autocatalytic (Electroless) Nickel-Phosphorus Coatings on Metal
ASTM E 1473 : 2022 Standard Test Methods for Chemical Analysis of Nickel, Cobalt, and High-Temperature Alloys

ASTM E 29 : 2013 : R2019 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
ASTM E 135 : 2023 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2021 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 353 : 2019 : EDT 1 Standard Test Methods for Chemical Analysis of Stainless, Heat-Resisting, Maraging, and Other Similar Chromium-Nickel-Iron Alloys
ASTM E 60 : 2011 : R2016 Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry
ASTM E 135 : 2023 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 135 : 2022 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 354 : 2021 : EDT 1 Standard Test Methods for Chemical Analysis of High-Temperature, Electrical, Magnetic, and Other Similar Iron, Nickel, and Cobalt Alloys
ASTM E 135 : 2022 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1806 : 2018 Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
ASTM E 60 : 2011 : R2022 : EDT 1 Standard Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry
ASTM E 135 : 2022 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
ASTM E 1806 : 2023 Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

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