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ASTM E 381 : 2017 : REDLINE

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Method of Macroetch Testing Steel Bars, Billets, Blooms, and Forgings

Available format(s)

PDF

Superseded date

30-07-2020

Language(s)

English

Published date

01-06-2017

€67.30
Excluding VAT

CONTAINED IN VOL. 03.01, 2017 Defines the etching of specimens for macrostructural examination at low magnifications, is a frequently used technique for evaluating steel products such as bars, billets, blooms, and forgings.

Committee
E 04
DevelopmentNote
Supersedes ASTM A 317. (03/2002) Supersedes MIL STD 430. (07/2004)
DocumentType
Redline
Pages
6
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1Macroetching, which is the etching of specimens for macrostructural examination at low magnifications, is a frequently used technique for evaluating steel products such as bars, billets, blooms, and forgings.

1.2Included in this method is a procedure for rating steel specimens by a graded series of photographs showing the incidence of certain conditions. The method is limited in application to bars, billets, blooms, and forgings of carbon and low alloy steels.

1.3A number of different etching reagents may be used depending upon the type of examination to be made. Steels react differently to etching reagents because of variations in chemical composition, method of manufacture, heat treatment and many other variables. Establishment of general standards for acceptance or rejection for all conditions is impractical as some conditions must be considered relative to the part in which it occurs.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See the specific precautionary statement in 5.3.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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SAE AMS6280M Steel Bars, Forgings, and Rings 0.50Cr - 0.55Ni - 0.20Mo (0.28 – 0.33C) (SAE 8630)
MIL-S-6758 Revision B:1993 STEEL, CHROME-MOLYBDENUM (4130) BARS AND REFORGING STOCK (AIRCRAFT QUALITY)
ASTM E 340 : 2015 : REDLINE Standard Practice for Macroetching Metals and Alloys
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ASTM A 943/A943M : 2001 Standard Specification for Spray-Formed Seamless Austenitic Stainless Steel Pipes
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SAE AMS6427M Steel Bars, Forgings, and Tubing 0.88Cr - 1.8Ni - 0.42Mo - 0.08V (0.28 - 0.33C) (4330 Mod)
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ASTM A 1021/A1021M : 2005 : R2010 Standard Specification for Martensitic Stainless Steel Forgings and Forging Stock for High-Temperature Service
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SAE AMS6300G Steel Bars and Forgings 0.25Mo (0.35 - 0.40C) (SAE 4037)
SAE AMS6349E Steel Bars 0.95Cr - 0.20Mo (0.38 to 0.43C) (SAE 4140) Normalized
ASTM A 604 : 1993 : R2003 Standard Test Method for Macroetch Testing of Consumable Electrode Remelted Steel Bars and Billets
ASTM A 21 : 1994 : R1999 Standard Specification for Carbon Steel Axles, Non-Heat-Treated and Heat-Treated, for Railway Use (Withdrawn 2003)
SAE AMS6432C Steel Bars, Forgings, and Tubing, 1.05Cr - 0.55Ni - 1.0Mo - 0.12V (0.43 - 0.49C)
ASTM F 2511 : 2005 Standard Specification for Rollers, Bearing, Needle, Ferrous, Solid
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ASTM A 949/A949M : 2001 Standard Specification for Spray-Formed Seamless Ferritic/Austenitic Stainless Steel Pipe
SAE AMS6348D Steel, Bars 0.95Cr - 0.20Mo (0.28 to 0.33C) (SAE 4130) Normalized
ASTM A 1021 : 2002 Standard Specification for Martensitic Stainless Steel Forgings and Forging Stock for High-Temperature Service
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DEFSTAN 13-47/5(2007) : 2007 STEEL FOR SHELL BODIES AND PROOF SHOT
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ASTM A 949/A949M : 2001 : R2005 Standard Specification for Spray-Formed Seamless Ferritic/Austenitic Stainless Steel Pipe
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MIL-S-46119 Revision C:1988 Steel Forgings, Tubular Parts for Cannon
ASTM E 1180 : 2008 : R2014 Standard Practice for Preparing Sulfur Prints for Macrostructural Evaluation
ASTM A 982 : 2002 Standard Specification for Steel Forgings, Stainless, for Compressor and Turbine Airfoils
ASTM A 660 : 1996 : R2005 Standard Specification for Centrifugally Cast Carbon Steel Pipe for High-Temperature Service
16/30321447 DC : DRAFT SEP 2016 BS ISO 20438 - SHIPS AND MARINE TECHNOLOGY - OFFSHORE MOORING CHAINS
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ASTM A 521/A521M : 2006 Standard Specification for Steel, Closed-Impression Die Forgings for General Industrial Use
ASTM A 943/A943M : 2001 : R2009 Standard Specification for Spray-Formed Seamless Austenitic Stainless Steel Pipes
MIL-P-70997 Base Document:1991 PROJECTILE, 81MM, HE, M821E1/M889E1 BODY ASSEMBLY
MIL-B-12504 Revision E:1987 BAR, METAL AND WIRE (NONELECTRICAL), CARBON AND ALLOY STEEL, COLD DRAWN FOR AP BULLET CORES AND SHOT
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MIL-S-81054 Revision A:1976 STEEL, BARS AND FORGINGS, CHROMIUM NICKEL MOLYBDENUM VANADIUM (FOR TORPEDO MK 46 MOD O)
MIL-DTL-12235 Revision A:2009 PROJECTILE, PLATE-PROOFING (FOR IMPACT OR SHOCK TESTING) 37 MM M1000, 57 MM M1001, 75 MM M1002, 90 MM M1003, 105 MM M1004, 20 MM M1005, 57 MM M1001A, AND 75 MM M1002A
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API 20B : 2013 OPEN DIE SHAPED FORGINGS FOR USE IN THE PETROLEUM AND NATURAL GAS INDUSTRY
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UNI EN ISO 13680 : 2010 PETROLEUM AND NATURAL GAS INDUSTRIES - CORROSION-RESISTANT ALLOY SEAMLESS TUBES FOR USE AS CASING, TUBING AND COUPLING STOCK - TECHNICAL DELIVERY CONDITIONS
EN ISO 13680:2010 Petroleum and natural gas industries - Corrosion-resistant alloy seamless tubes for use as casing, tubing and coupling stock - Technical delivery conditions (ISO 13680:2010)
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MIL-S-70703 Base Document:1987 Strand Cast Steel, Carbon and Alloy, for Projectile Applications
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MIL-R-10185 Revision E:1992 RING, BREECH, STEEL FORGINGS FOR
ASTM A 1028 : 2003 : R2015 Standard Specification for Stainless Steel Bars for Compressor and Turbine Airfoils (Withdrawn 2021)
MIL-S-46047 Revision E:1988 STEEL, BARS AND BLANKS (1-3/4 INCHES AND OVER IN DIAMETER) FOR BARRELS OF SMALL ARMS WEAPONS
ASTM E 1180 : 2008 Standard Practice for Preparing Sulfur Prints for Macrostructural Evaluation
MIL-C-24633 Revision A:1990 Chain, Stud Link, Anchor, Low Alloy Steel, Flash Butt Welded
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MIL S 13823 : C STEEL, SHAPES, ROLLED OR FORGED, BARS, FLATS AND SPECIAL SECTIONS (FOR ARMOR)
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ASTM A 452 : 1988 Specification for Centrifugally Cast Austenitic Steel Cold-Wrought Pipe for High-Temperature Service (Withdrawn 1995)
SAE AMS6325K Steel, Bars, and Forgings 0.50Cr - 0.55Ni - 0.25Mo (0.38 - 0.43C) (SAE 8740) Heat Treated, 105 ksi (724 MPa) Tensile Strength
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ASTM A 295/A295M : 2014 : REDLINE Standard Specification for High-Carbon Anti-Friction Bearing Steel
ASTM A 521/A521M : 2006 : R2016 Standard Specification for Steel, Closed-Impression Die Forgings for General Industrial Use (Withdrawn 2018)
BS EN ISO 13680:2010 Petroleum and natural gas industries. Corrosion-resistant alloy seamless tubes for use as casing, tubing and coupling stock Technical delivery conditions
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SAE AMS6430J Steel, Bars, Forgings, Tubing, and Rings 0.75Mn - 0.78Cr - 1.8Ni - 0.35Mo - 0.20V (0.32 – 0.38C) (4335 Modified)
SAE AMS6475K Steel, Nitriding, Bars, Forgings, and Tubing 1.1Cr – 3.5Ni – 0.25Mo – 1.2Al (0.21 – 0.26C)
SAE AMS6484E Steel, Bars, Forgings, and Tubing 0.80Cr - 1.8Ni - 0.25Mo (0.38 - 0.43C) (SAE 4340) Normalized and Tempered
MIL-S-8690 Revision B:1978 STEEL, CHROME NICKEL MOLYBDENUM 8620, BARS AIRCRAFT QUALITY
ASTM A 604/A604M : 2007 : R2012 Standard Practice for Macroetch Testing of Consumable Electrode Remelted Steel Bars and Billets
SAE AMS6422K Steel, Bars, Forgings, and Tubing 0.80Cr - 0.85Ni - 0.20Mo - 0.003B - 0.04V (0.38 - 0.43C) (Modified 98BV40)
ASTM A 943/A943M : 2001 : R2019 Standard Specification for Spray-Formed Seamless Austenitic Stainless Steel Pipes (Withdrawn 2024)
MIL-S-46172 Revision A:1984 STEEL FORGINGS
MIL-T-13915 Revision E:1987 TUBE, STEEL , SEAMLESS, FOR CANNONS AND RECOILLESS RIFLES
SAE AMS5620G Steel, Corrosion and Heat-Resistant, Bars, Wire, and Forgings 13Cr (0.30 - 0.40C) (SAE 51420F, 51420FSe) Free-Machining Grade
MIL-DTL-13823 Revision D:1998 STEEL; SHAPES, ROLLED OR FORGED; BARS, FLATS AND SPECIAL SECTIONS (FOR ARMOR)
ASTM A 943/A943M : 2001 : R2005 Standard Specification for Spray-Formed Seamless Austenitic Stainless Steel Pipes
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SAE AMS5899B Steel, Corrosion-Resistant, Bars, Wire, and Forgings 17Cr - 0.52Mo (0.95 - 1.20C) Powder Metallurgy Product, Hot Isostatically Pressed
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ISO 4969:2015 Steel Etching method for macroscopic examination
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CSA N285.6 SERIES : 2005 MATERIAL STANDARDS FOR REACTOR COMPONENTS FOR CANDU NUCLEAR POWER PLANTS
API TR 17TR8 : 2018 HIGH-PRESSURE HIGH-TEMPERATURE DESIGN GUIDELINES
ASTM A 521/A521M : 2006 : R2011 Standard Specification for Steel, Closed-Impression Die Forgings for General Industrial Use
ASTM A 604 : 1993 : R1998 Standard Test Method for Macroetch Testing of Consumable Electrode Remelted Steel Bars and Billets
ASTM F 2511 : 2005 : R2013 Standard Specification for Rollers, Bearing, Needle, Ferrous, Solid

ASTM E 7 : 2017 : REDLINE Standard Terminology Relating to Metallography
ASTM E 340 : 2015 : REDLINE Standard Practice for Macroetching Metals and Alloys

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