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ASTM E 399 : 2023

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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Standard Test Method for Linear-Elastic Plane-Strain Fracture Toughness of Metallic Materials

Available format(s)

Hardcopy , PDF

Superseded date

23-10-2024

Superseded by

ASTM E 399 : 2024

Language(s)

English

Published date

01-06-2023

€96.91
Excluding VAT

Committee
E 08
DocumentType
Test Method
Pages
40
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

1.1This test method covers the determination of fracture toughness (KIc and optionally KIsi) of metallic materials under predominantly linear-elastic, plane-strain conditions using fatigue precracked specimens having a thickness of 1.6 mm (0.063 in.) or greater2 subjected to slowly, or in special (elective) cases rapidly, increasing crack-displacement force. Details of test apparatus, specimen configuration, and experimental procedure are given in the annexes. Two procedures are outlined for using the experimental data to calculate fracture toughness values:

1.1.1The KIc test procedure is described in the main body of this test standard and is a mandatory part of the testing and results reporting procedure for this test method. The KIc test procedure is based on crack growth of up to 2 % percent of the specimen width. This can lead to a specimen size dependent rising fracture toughness resistance curve, with larger specimens producing higher fracture toughness results.

1.1.2The KIsi test procedure is described in Appendix X1 and is an optional part of this test method. The KIsi test procedure is based on a fixed amount of crack extension of 0.5 mm, and as a result, KIsi is less sensitive to specimen size than KIc. This less size-sensitive fracture toughness, KIsi, is called size-insensitive throughout this test method. Appendix X1 contains an optional procedure for reinterpreting the force-displacement test record recorded as part of this test method to calculate the additional fracture toughness value, KIsi.

Note 1:Plane-strain fracture toughness tests of materials thinner than 1.6 mm (0.063 in.) that are sufficiently brittle (see 7.1) can be made using other types of specimens (1).3 There is no standard test method for such thin materials.

1.2This test method is divided into two parts. The first part gives general recommendations and requirements for testing and includes specific requirements for the KIc test procedure. The second part consists of Annexes that give specific information on displacement gage and loading fixture design, special requirements for individual specimen configurations, and detailed procedures for fatigue precracking. Additional annexes are provided that give specific procedures for beryllium and rapid-force testing, and the KIsi test procedure, which provides an optional additional analysis procedure for the test data collected as part of the KIc test procedure.

1.3General information and requirements common to all specimen configurations:

Section

Referenced Documents

2

Terminology

3

 Stress-Intensity Factor

3.1.1

 Plane-Strain Fracture Toughness

3.1.2

 Crack Plane Orientation

3.1.4

Summary of Test Method

4

Significance and Use

5

 Significance

5.1

 Precautions

5.1.1 – 5.1.5

 Practical Applications

5.2

Apparatus (see also 1.4)

6

 Tension Machine

6.1

 Fatigue Machine

6.2

 Loading Fixtures

6.3

 Displacement Gage, Measurement

6.4

Specimen Size, Configurations, and Preparation (see also 1.5)

7

 Specimen Size Estimates

7.1

 Standard and Alternative Specimen Configurations

7.2

 Fatigue Crack Starter Notches

7.3.1

 Fatigue Precracking (see also 1.6)

7.3.2

 Crack Extension Beyond Starter Notch

7.3.2.2

General Procedure

8

 Specimen Measurements

  Thickness

8.2.1

  Width

8.2.2

  Crack Size

8.2.3

  Crack Plane Angle

8.2.4

 Specimen Testing

  Loading Methods

8.3

  Loading Rate

8.4

  Test Record

8.5

Calculation and Interpretation of Results

9

 Test Record Analysis

9.1

Pmax/PQ Validity Requirement

9.1.3

 Specimen Size Validity Requirements

9.1.4

Reporting

10

Precision and Bias

11

1.4Specific requirements related to test apparatus:

Double-Cantilever Displacement Gage

Annex A1

Testing Fixtures

Annex A2

Bend Specimen Loading Fixture

Annex A2.1

Compact Specimen Loading Clevis

Annex A2.2

1.5Specific requirements related to individual specimen configurations:

Bend Specimen SE(B)

Annex A3

Compact Specimen C(T)

Annex A4

Disk-Shaped Compact Specimen DC(T)

Annex A5

Arc-Shaped Tension Specimen A(T)

Annex A6

Arc-Shaped Bend Specimen A(B)

Annex A7

1.6Specific requirements related to special test procedures:

Fatigue Precracking KIc and KIsi Specimens

Annex A8

Hot-Pressed Beryllium Testing

Annex A9

Rapid-Force Testing

Annex A10

Determination of KIsi

Appendix X1

1.7The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.8This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.9This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM E 1221 : 2012 : REV A : R2018 : EDT 1 Standard Test Method for Determining Plane-Strain Crack-Arrest Fracture Toughness, <emph type="bdit">K<inf>Ia</inf></emph>, of Ferritic Steels
ASTM E 647 : 2023 : REV A Standard Test Method for Measurement of Fatigue Crack Growth Rates
ASTM F 1940 : 2007 : REV A : R2019 Standard Test Method for Process Control Verification to Prevent Hydrogen Embrittlement in Plated or Coated Fasteners
ASTM E 1304 : 1997 : R2020 Standard Test Method for Plane-Strain (Chevron-Notch) Fracture Toughness of Metallic Materials
ASTM F 3056 : 2014 : R2021 Standard Specification for Additive Manufacturing Nickel Alloy (UNS N06625) with Powder Bed Fusion
ASTM E 604 : 2018 Standard Test Method for Dynamic Tear Testing of Metallic Materials
ASTM B 646 : 2019 Standard Practice for Fracture Toughness Testing of Aluminum Alloys
ASTM D 7779 : 2020 Standard Test Method for Determination of Fracture Toughness of Graphite at Ambient Temperature
ASTM G 168 : 2017 Standard Practice for Making and Using Precracked Double Beam Stress Corrosion Specimens
ASTM E 1681 : 2023 Standard Test Method for Determining Threshold Stress Intensity Factor for Environment-Assisted Cracking of Metallic Materials
ASTM G 107 : 1995 : R2020 : EDT 1 Standard Guide for Formats for Collection and Compilation of Corrosion Data for Metals for Computerized Database Input
ASTM D 5045 : 2014 : R2022 Standard Test Methods for Plane-Strain Fracture Toughness and Strain Energy Release Rate of Plastic Materials
ASTM F 3213 : 2017 Standard for Additive Manufacturing – Finished Part Properties – Standard Specification for Cobalt-28 Chromium-6 Molybdenum via Powder Bed Fusion
ASTM E 606/E606M : 2021 Standard Test Method for Strain-Controlled Fatigue Testing
ASTM A 788/A788M : 2022 : REV A Standard Specification for Steel Forgings, General Requirements
ASTM D 8044 : 2023 Standard Test Method for Evaluation of Asphalt Mixture Cracking Resistance Using the Semi-Circular Bend Test (SCB) at Intermediate Temperatures
ASTM F 3318 : 2018 Standard for Additive Manufacturing – Finished Part Properties – Specification for AlSi10Mg with Powder Bed Fusion – Laser Beam
ASTM E 2760 : 2019 : EDT 1 Standard Test Method for Creep-Fatigue Crack Growth Testing
ASTM A 504/A504M : 2018 : R2023 Standard Specification for Wrought Carbon Steel Wheels
ASTM E 2208 : 2002 : R2018 : EDT 1 Standard Guide for Evaluating Non-Contacting Optical Strain Measurement Systems
ASTM C 1576 : 2005 : R2017 Standard Test Method for Determination of Slow Crack Growth Parameters of Advanced Ceramics by Constant Stress Flexural Testing (Stress Rupture) at Ambient Temperature
ASTM D 6068 : 2010 : R2018 Standard Test Method for Determining <emph type="bdit">J-R </emph>Curves of Plastic Materials
ASTM E 1820 : 2023 : REV A Standard Test Method for Measurement of Fracture Toughness
ASTM C 1834 : 2016 Standard Test Method for Determination of Slow Crack Growth Parameters of Advanced Ceramics by Constant Stress Flexural Testing (Stress Rupture) at Elevated Temperatures
ASTM E 561 : 2023 Standard Test Method for <emph type="bdit">K<inf>R</inf></emph> Curve Determination
ASTM E 1922/E1922M : 2022 Standard Test Method for Translaminar Fracture Toughness of Laminated and Pultruded Polymer Matrix Composite Materials
ASTM G 58 : 1985 : R2015 Standard Practice for Preparation of Stress-Corrosion Test Specimens for Weldments
ASTM E 636 : 2020 Standard Guide for Conducting Supplemental Surveillance Tests for Nuclear Power Reactor Vessels
ASTM B 771 : 2011 : R2021 Standard Test Method for Short Rod Fracture Toughness of Cemented Carbides
ASTM E 2899 : 2019 : EDT 1 Standard Test Method for Measurement of Initiation Toughness in Surface Cracks Under Tension and Bending
ASTM F 3055 : 2014 : REV A : R2021 Standard Specification for Additive Manufacturing Nickel Alloy (UNS N07718) with Powder Bed Fusion
ASTM F 2924 : 2014 : R2021 Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium with Powder Bed Fusion
ASTM E 1823 : 2023 Standard Terminology Relating to Fatigue and Fracture Testing
ASTM F 3184 : 2016 Standard Specification for Additive Manufacturing Stainless Steel Alloy (UNS S31603) with Powder Bed Fusion
ASTM D 8255 : 2019 Standard Guide for Work of Fracture Measurements on Small Nuclear Graphite Specimens
ASTM G 129 : 2021 Standard Practice for Slow Strain Rate Testing to Evaluate the Susceptibility of Metallic Materials to Environmentally Assisted Cracking
ASTM B 645 : 2021 Standard Practice for Linear-Elastic Plane-Strain Fracture Toughness Testing of Aluminum Alloys
ASTM F 3122 : 2014 : R2022 Standard Guide for Evaluating Mechanical Properties of Metal Materials Made via Additive Manufacturing Processes
ASTM D 3433 : 1999 : R2020 Standard Test Method for Fracture Strength in Cleavage of Adhesives in Bonded Metal Joints
ASTM D 7313 : 2020 Standard Test Method for Determining Fracture Energy of Asphalt Mixtures Using the Disk-Shaped Compact Tension Geometry
ASTM F 3439 : 2022 Additive manufacturing of metals — Finished part properties — Orientation and location dependence of mechanical properties for metal powder bed fusion
ASTM E 740/E740M : 2003 : R2016 Standard Practice for Fracture Testing with Surface-Crack Tension Specimens
ASTM F 3302 : 2018 Standard for Additive Manufacturing – Finished Part Properties – Standard Specification for Titanium Alloys via Powder Bed Fusion
ASTM B 909 : 2021 : REV A Standard Guide for Plane Strain Fracture Toughness Testing of Non-Stress Relieved Aluminum Products
ASTM E 2472 : 2012 : R2018 : EDT 2 Standard Test Method for Determination of Resistance to Stable Crack Extension under Low-Constraint Conditions
ASTM E 1457 : 2019 : EDT 1 Standard Test Method for Measurement of Creep Crack Growth Times in Metals
ASTM F 1624 : 2012 : R2018 Standard Test Method for Measurement of Hydrogen Embrittlement Threshold in Steel by the Incremental Step Loading Technique
ASTM G 58 : 1985 : R2023 Standard Practice for Preparation of Stress-Corrosion Test Specimens for Weldments
ASTM E 740/E740M : 2023 Standard Practice for Fracture Testing with Surface-Crack Tension Specimens
ASTM C 1834 : 2016 : R2024 Standard Test Method for Determination of Slow Crack Growth Parameters of Advanced Ceramics by Constant Stress Flexural Testing (Stress Rupture) at Elevated Temperatures
ASTM F 3184 : 2016 : R2023 Standard Specification for Additive Manufacturing Stainless Steel Alloy (UNS S31603) with Powder Bed Fusion
ASTM E 2760 : 2019 : EDT 3 Standard Test Method for Creep-Fatigue Crack Growth Testing
ASTM F 1940 : 2007 : REV A : R2024 Standard Test Method for Process Control Verification to Prevent Hydrogen Embrittlement in Plated or Coated Fasteners
ASTM F 3607 : 2022 Standard Specification for Additive Manufacturing – Finished Part Properties – Maraging Steel via Powder Bed Fusion
ASTM E 1221 : 2023 Standard Test Method for Determining Plane-Strain Crack-Arrest Fracture Toughness, <emph type="bdit">K<inf>Ia</inf></emph>, of Ferritic Steels
ASTM E 2472 : 2012 : R2018 : EDT 4 Standard Test Method for Determination of Resistance to Stable Crack Extension under Low-Constraint Conditions
ASTM E 1457 : 2023 : EDT 1 Standard Test Method for Measurement of Creep Crack Growth Times in Metals
ASTM E 2899 : 2024 : EDT 1 Standard Test Method for Measurement of Initiation Toughness in Surface Cracks Under Tension and Bending
ASTM E 1681 : 2023 : EDT 1 Standard Test Method for Determining Threshold Stress Intensity Factor for Environment-Assisted Cracking of Metallic Materials
ASD-STAN prEN 4500-001 P3:2023 Aerospace series Metallic materials — Rules for drafting and presentation of material standards — Part 001: General rules
SAE AMS6532K Steel, Bars and Forgings, and Forging Stock 3.1Cr - 11.5Ni - 13.5Co - 1.2Mo (0.23 - 0.25C) Vacuum Melted, Normalized and Overaged Precipitation Hardenable
NASA-HDBK-5026:2024 GUIDANCE ON STRENGTH, FATIGUE, AND FRACTURE CONTROL REQUIREMENTS FOR ADDITIVELY MANUFACTURED SPACEFLIGHT HARDWARE

ASTM E 1820 : 2023 : REV B Standard Test Method for Measurement of Fracture Toughness
ASTM E 1823 : 2024 Standard Terminology Relating to Fatigue and Fracture Testing
ASTM E 8/E8M : 2024 Standard Test Methods for Tension Testing of Metallic Materials
ASTM E 1823 : 2024 : REV A Standard Terminology Relating to Fatigue and Fracture Testing
ASTM E 647 : 2024 Standard Test Method for Measurement of Fatigue Crack Growth Rates
ASTM E 456 : 2013 : REV A : R2022 Standard Terminology Relating to Quality and Statistics
ASTM E 456 : 2013 : REV A : R2022 : EDT 1 Standard Terminology Relating to Quality and Statistics
ASTM E 1823 : 2024 : REV B Standard Terminology Relating to Fatigue and Fracture Testing
ASTM E 1921 : 2023 : REV B Standard Test Method for Determination of Reference Temperature, <emph type="bdit">T<inf >0</inf></emph>, for Ferritic Steels in the Transition Range
ASTM E 647 : 2023 : REV B Standard Test Method for Measurement of Fatigue Crack Growth Rates
ASTM E 8/E8M : 2022 Standard Test Methods for Tension Testing of Metallic Materials
ASTM E 1820 : 2024 Standard Test Method for Measurement of Fracture Toughness
ASTM E 4 : 2021 Standard Practices for Force Calibration and Verification of Testing Machines
ASTM E 1921 : 2023 : REV A Standard Test Method for Determination of Reference Temperature, <emph type="bdit">T<inf >0</inf></emph>, for Ferritic Steels in the Transition Range
ASTM E 1921 : 2023 Standard Test Method for Determination of Reference Temperature, <emph type="bdit">T<inf >0</inf></emph>, for Ferritic Steels in the Transition Range
ASTM E 1921 : 2022 : REV A Standard Test Method for Determination of Reference Temperature, <emph type="bdit">T<inf >0</inf></emph>, for Ferritic Steels in the Transition Range
ASTM E 1823 : 2024 : REV C Standard Terminology Relating to Fatigue and Fracture Testing
ASTM E 1921 : 2024 Standard Test Method for Determination of Reference Temperature, <emph type="bdit">T<inf >0</inf></emph>, for Ferritic Steels in the Transition Range
ASTM E 4 : 2024 Standard Practices for Force Calibration and Verification of Testing Machines
ASTM E 1820 : 2023 : REV A Standard Test Method for Measurement of Fracture Toughness

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