• ASTM E 691 : 2008

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

    Available format(s):  Hardcopy, PDF

    Superseded date:  11-11-2014

    Language(s):  English

    Published date:  01-10-2008

    Publisher:  American Society for Testing and Materials

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    1.1 This practice describes the techniques for planning, conducting, analyzing, and treating the results of an interlaboratory study (ILS) of a test method. The statistical techniques described in this practice provide adequate information for formulating the precision statement of a test method.

    1.2 This practice does not concern itself with the development of test methods but rather with gathering the information needed for a test method precision statement after the development stage has been successfully completed. The data obtained in the interlaboratory study may indicate, however, that further effort is needed to improve the test method.

    1.3 Since the primary purpose of this practice is the development of the information needed for a precision statement, the experimental design in this practice may not be optimum for evaluating materials, apparatus, or individual laboratories.

    1.4 Field of ApplicationThis practice is concerned exclusively with test methods which yield a single numerical figure as the test result, although the single figure may be the outcome of a calculation from a set of measurements.

    1.4.1 This practice does not cover methods in which the measurement is a categorization, such as a go-no-go allocation (two categories) or a sorting scheme into two or more categories. For practical purposes, the discontinuous nature of measurements of these types may be ignored when a test result is defined as an average of several individual measurements. Then, this practice may be applicable, but caution is required and a statistician should be consulted.

    1.5 The information in this practice is arranged as follows:

    Section
    Scope1
    Referenced Documents2
    Terminology3
    Summary of Practice4
    Significance and Use5
    Planning the Interlaboratory Study (ILS)
    ILS Membership6
    Basic Design7
    Test Method8
    Laboratories9
    Section
    Materials10
    Number of Test Results per Material11
    Protocol12
    Conducting the Testing Phase of the ILS
    Pilot Run13
    Full Scale Run14
    Section
    Calculation and Display of Statistics
    Calculation of the Statistics15
    Tabular and Graphical Display of Statistics16
    Data Consistency
    Flagging Inconsistent Results17
    Investigation18
    Task Group Actions19
    Examples of Interlaboratory Studies20
    Precision Statement Information
    Repeatability and Reproducibility21
    Appendixes
    Theoretical ConsiderationsA1
    Index to Selected TermsA2
    References
    Tables and Figures
    TablesTable
    Glucose in Serum Example14 & 67
    Pentosans in Pulp Example811
    Critical Values of Consistency Statistics, h and k5
    FiguresFig.
    Glucose in Serum Example15
    Pentosans in Pulp Example610

    1.6 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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    Committee E 11
    Document Type Standard Practice
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes
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