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ASTM E 840 : 1995 : R2021 : EDT 1

Current

Current

The latest, up-to-date edition.

Standard Practice for Using Flame Photometric Detectors in Gas Chromatography

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

05-05-2021

€61.92
Excluding VAT

Committee
E 13
DocumentType
Standard Practice
Pages
12
ProductNote
ε1NOTE—Section references in8.7.2and10.2.1.1were corrected and editorial changes made throughout in May 2021.
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

1.1This practice is intended as a guide for the use of a flame photometric detector (FPD) as the detection component of a gas chromatographic system.

1.2This practice is directly applicable to an FPD that employs a hydrogen-air flame burner, an optical filter for selective spectral viewing of light emitted by the flame, and a photomultiplier tube for measuring the intensity of light emitted.

1.3This practice describes the most frequent use of the FPD which is as an element-specific detector for compounds containing sulfur (S) or phosphorus (P) atoms. However, nomenclature described in this practice are also applicable to uses of the FPD other than sulfur or phosphorus specific detection.

1.4This practice is intended to describe the operation and performance of the FPD itself independently of the chromatographic column. However, the performance of the detector is described in terms which the analyst can use to predict overall system performance when the detector is coupled to the column and other chromatographic system components.

1.5For general gas chromatographic procedures, Practice E260 should be followed except where specific changes are recommended herein for use of an FPD.

1.6The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.7This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific safety information, see Section 4, Hazards.

1.8This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ASTM D 6968 : 2003 : R2015 Standard Test Method for Simultaneous Measurement of Sulfur Compounds and Minor Hydrocarbons in Natural Gas and Gaseous Fuels by Gas Chromatography and Atomic Emission Detection (Withdrawn 2024)
ASTM D 6228 : 2019 Standard Test Method for Determination of Sulfur Compounds in Natural Gas and Gaseous Fuels by Gas Chromatography and Flame Photometric Detection
ASTM D 4735 : 2019 Standard Test Method for Determination of Trace Thiophene in Refined Benzene by Gas Chromatography
ASTM D 7041 : 2016 Standard Test Method for Determination of Total Sulfur in Liquid Hydrocarbons and Hydrocarbon-Oxygenate Blends by Gas Chromatography with Flame Photometric Detection
ASTM D 7800/D7800M : 2014 Standard Test Method for Determination of Elemental Sulfur in Natural Gas (Withdrawn 2023)
ASTM D 5303 : 2020 Standard Test Method for Trace Carbonyl Sulfide in Propylene by Gas Chromatography
ASTM E 260 : 1996 : R2019 Standard Practice for Packed Column Gas Chromatography

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