• BS EN 12916:2016

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

    Petroleum products. Determination of aromatic hydrocarbon types in middle distillates. High performance liquid chromatography method with refractive index detection

    Available format(s):  Hardcopy, PDF

    Superseded date:  21-05-2019

    Language(s):  English

    Published date:  29-02-2016

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    European foreword
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Reagents and materials
    6 Apparatus
    7 Sampling
    8 Apparatus preparation
    9 Calibration
    10 Procedure
    11 Calculation
    12 Expression of results
    13 Precision
    14 Test report
    Annex A (informative) - Column selection and use
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines a test method for the determination of the content of mono-aromatic, di-aromatic and tri+-aromatic hydrocarbons in diesel fuels that may contain fatty acid methyl esters (FAME) up to 30 % (V/V) and petroleum distillates in the boiling range from 150 degrees C to 400 degrees C.

    Scope - (Show below) - (Hide below)

    This European Standard specifies a test method for the determination of the content of mono-aromatic, di-aromatic and tri+-aromatic hydrocarbons in diesel fuels that may contain fatty acid methyl esters (FAME) up to 30% (V/V) and petroleum distillates in the boiling range from 150°C to 400°C. The polycyclic aromatic hydrocarbons content is calculated from the sum of di-aromatic and tri+-aromatic hydrocarbons and the total content of aromatic compounds is calculated from the sum of the individual aromatic hydrocarbon types. Compounds containing sulfur, nitrogen and oxygen can interfere in the determination; mono-alkenes do not interfere, but conjugated di-alkenes and poly-alkenes, if present, may do so. The precision statement of the test method has been established for diesel fuels with and without FAME blending components, with a mono-aromatic content in the range from 6% ( m/m) to 30% ( m/m), a di-aromatic content from 1% ( m/m) to 10% ( m/m), a tri+-aromatic content from 0% ( m/m) to 2% ( m/m), a polycyclic aromatic content from 1% ( m/m) to 12% ( m/m), and a total aromatic content from 7% ( m/m) to 42% ( m/m). NOTE1 For the purpose of this European Standard, the terms “% (m/m)?? and “% ( V/V)?? are used to represent the mass fraction and the volume fraction of a material respectively. NOTE2 By convention, the aromatic hydrocarbon types are defined on the basis of their elution characteristics from the specified liquid chromatography column relative to model aromatic compounds. Their quantification is performed using an external calibration with a single aromatic compound for each of them, which may or may not be representative of the aromatics present in the sample. Alternative techniques and test methods may classify and quantify individual aromatic hydrocarbon types differently. WARNING— The use of this Standard can involve hazardous materials, operations and equipment. This Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this standard to take appropriate measures to ensure the safety and health of personnel prior to application of the standard, and fulfil statutory and regulatory requirements for this purpose.

    General Product Information - (Show below) - (Hide below)

    Committee PTI/15
    Development Note Supersedes 97/122560 DC. (03/2004) Supersedes 04/30113923 DC. (12/2006) Supersedes BS 2000-391(2006). (02/2016) Supersedes 14/30304453 DC. (03/2016)
    Document Type Standard
    Publisher British Standards Institution
    Status Superseded
    Superseded By
    Supersedes

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
    ISO 3170:2004 Petroleum liquids — Manual sampling
    ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
    EN ISO 1042 : 1999 LABORATORY GLASSWARE - ONE-MARK VOLUMETRIC FLASKS
    ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
    EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
    EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)
    EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)
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