BS EN 13130-6:2004
Current
The latest, up-to-date edition.
Materials and articles in contact with foodstuffs. Plastics substances subject to limitation Determination of vinylidene chloride in plastics
Hardcopy , PDF
English
21-06-2004
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Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Samples
6.1 Sample storage
6.2 Test sample preparation
6.2.1 General
6.2.2 Preparation of dissolved test sample solutions and
standard addition solutions
6.2.3 Preparation of blank samples
6.2.4 Preparation of 'hot jar' test samples
7 Procedure
7.1 GC preparation
7.1.1 GC parameters
7.1.2 Electron capture detector optimization
7.1.3 Performance of GC measurements
7.2 Calibration
8 Expression of results
8.1 Method of calculation
8.1.1 GC interferences
8.1.2 Graphical determination using internal standard
8.1.3 Graphical determination via external standardization
8.1.4 Calculation of the concentration using a response
factor
8.2 Precision
8.2.1 Validation
8.2.2 Repeatability and reproducibility
8.2.3 Detection limit
9 Confirmation
9.1 Requirement for confirmation
9.2 Confirmation by combined gas chromatography-mass
spectrometry
9.3 Confirmation by analysis on a GC column of different
polarity
10 Test report
Annex A (normative) Manual sample injection
Bibliography
Specifies a method for the determination of vinylidene chloride (VdC) in plastics materials and articles.
| Committee |
CW/29
|
| DevelopmentNote |
Supersedes DD ENV 13130-6 & 03/312203 DC To be read in conjunction with BS EN 13130-1 (06/2004)
|
| DocumentType |
Standard
|
| Pages |
20
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
| Supersedes |
This part of this European Standard specifies a method for the determination of vinylidene chloride (VdC) in plastics materials and articles. The method is applicable to poly(vinylidene chloride) (PVdC) films, PVdC coated films, and laminates and coextruded materials containing PVdC. The level of vinylidene chloride determined is expressed as milligrams of vinylidene chloride per kilogram of polymer. The method is appropriate for the quantitative determination of vinylidene chloride at a level of 5 mg/kg in plastics materials and articles.
| Standards | Relationship |
| EN 13130-6:2004 | Identical |
| SN EN 13130-6 : 2004 | Identical |
| UNI EN 13130-6 : 2005 | Identical |
| DIN EN 13130-6:2004-08 | Identical |
| NF EN 13130-6 : 2004 | Identical |
| NEN EN 13130-6 : 2004 | Identical |
| I.S. EN 13130-6:2004 | Identical |
| NBN EN 13130-6 : 2004 | Identical |
| NS EN 13130-6 : 1ED 2004 | Identical |
| UNE-EN 13130-6:2005 | Identical |
| ISO 5725-1:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| EN 13130-1:2004 | Materials and articles in contact with foodstuffs - Plastics substances subject to limitation - Part 1: Guide to test methods for the specific migration of substances from plastics to foods and food simulants and the determination of substances in plastics and the selection of conditions of exposure to food simulants |
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