BS EN 13585:2002
Current
The latest, up-to-date edition.
Foodstuffs. Determination of fumonisins B1 and B2 in maize. HPLC method with solid phase extraction clean-up
Hardcopy , PDF
English
04-03-2002
Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Apparatus
6 Sampling
7 Preparation of the test sample
8 Procedure
9 Calculation
10 Precision
11 Test report
Annex A (informative) Typical chromatogram
Annex B (informative) Recovery and relative standard
deviation
Annex C (informative) Precision data
Bibliography
Defines a method for the determination of fumonisin B1 (FB1) and fumonisin B2 (FB2) in maize using high performance liquid chromatography (HPLC).
| Committee |
AW/275
|
| DevelopmentNote |
Supersedes 99/703223 DC (03/2002)
|
| DocumentType |
Standard
|
| Pages |
18
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
| Supersedes |
This European Standard specifies a method for the determination of fumonisin B1 (FB1) and fumonisin B2 (FB2) in maize using high performance liquid chromatography (HPLC). The method has been successfully validated in an interlaboratory study according to AOAC Guidelines for Collaborative Studies [1] on maize containing 405 µg/kg to 6732 mg/kg fumonisin B1 and 152 mg/kg to 2619 mg/kg fumonisin B2. The method works well with maize or minimally processed maize (e.g. fresh, dried and milled maize), but does not provide reliable results with most maize-based processed products.
| Standards | Relationship |
| SN EN 13585 : 2001 | Identical |
| NF EN 13585 : 2002 | Identical |
| NEN EN 13585 : 2002 | Identical |
| EN 13585:2001 | Identical |
| I.S. EN 13585:2002 | Identical |
| UNE-EN 13585:2002 | Identical |
| NBN EN 13585 : 2002 | Identical |
| NS EN 13585 : 1ED 2002 | Identical |
| UNI EN 13585 : 2002 | Identical |
| DIN EN 13585:2002-03 | Identical |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
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