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BS EN 13585:2002

Current

Current

The latest, up-to-date edition.

Foodstuffs. Determination of fumonisins B1 and B2 in maize. HPLC method with solid phase extraction clean-up

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

04-03-2002

Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Apparatus
6 Sampling
7 Preparation of the test sample
8 Procedure
9 Calculation
10 Precision
11 Test report
Annex A (informative) Typical chromatogram
Annex B (informative) Recovery and relative standard
        deviation
Annex C (informative) Precision data
Bibliography

Defines a method for the determination of fumonisin B1 (FB1) and fumonisin B2 (FB2) in maize using high performance liquid chromatography (HPLC).

Committee
AW/275
DevelopmentNote
Supersedes 99/703223 DC (03/2002)
DocumentType
Standard
Pages
18
PublisherName
British Standards Institution
Status
Current
Supersedes

This European Standard specifies a method for the determination of fumonisin B1 (FB1) and fumonisin B2 (FB2) in maize using high performance liquid chromatography (HPLC). The method has been successfully validated in an interlaboratory study according to AOAC Guidelines for Collaborative Studies [1] on maize containing 405 µg/kg to 6732 mg/kg fumonisin B1 and 152 mg/kg to 2619 mg/kg fumonisin B2. The method works well with maize or minimally processed maize (e.g. fresh, dried and milled maize), but does not provide reliable results with most maize-based processed products.

Standards Relationship
SN EN 13585 : 2001 Identical
NF EN 13585 : 2002 Identical
NEN EN 13585 : 2002 Identical
EN 13585:2001 Identical
I.S. EN 13585:2002 Identical
UNE-EN 13585:2002 Identical
NBN EN 13585 : 2002 Identical
NS EN 13585 : 1ED 2002 Identical
UNI EN 13585 : 2002 Identical
DIN EN 13585:2002-03 Identical

ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)

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