BS EN 16158:2012
Current
The latest, up-to-date edition.
Animal feeding stuffs. Determination of semduramicin content. Liquid chromatographic method using a \'tree\' analytical approach
Hardcopy , PDF
English
31-03-2012
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Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Sampling
7 Preparation of test sample
8 Procedure
9 Calculation
10 Precision
11 Test report
Annex A (informative) - Results of collaborative study
Bibliography
Describes a high-performance liquid chromatographic (HPLC) method for the determination of the semduramicin content at authorized level in animal feeding stuffs, using mass spectrometry detection or post-column derivatization and (UV)-VIS detection (hereinafter UV detection).
| Committee |
AW/10
|
| DevelopmentNote |
Supersedes 10/30199743 DC. (04/2012)
|
| DocumentType |
Standard
|
| Pages |
29
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
| Supersedes |
This European standard specifies a high-performance liquid chromatographic (HPLC) method for the determination of the semduramicin content at authorized level in animal feeding stuffs [2], using mass spectrometry detection or post-column derivatization and (UV)-VIS detection (hereinafter UV detection). This method is applicable to poultry feed. The limit of quantitation is 1,0 mg/kg when mass spectrometry is used for detection and 3,0 mg/kg when the detection is performed by UV with post-column derivatization. Lower limits of quantitation are achievable but this is to be validated by the user.
The method allows the discrimination of semduramicin from monensin, salinomycin, narasin, maduramicin and lasalocid.
| Standards | Relationship |
| EN 16158:2012 | Identical |
| ISO 6497:2002 | Animal feeding stuffs Sampling |
| PREN ISO 6498 : DRAFT 2009 | ANIMAL FEEDING STUFFS - GUIDELINES FOR SAMPLE PREPARATION |
| EN ISO 6497:2005 | Animal feeding stuffs - Sampling (ISO 6497:2002) |
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