• BS EN 62021-2:2007

    Current The latest, up-to-date edition.

    Insulating liquids. Determination of acidity Colourimetric titration

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  31-08-2007

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    INTRODUCTION
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Reagents
       5.1 Titration reagent
       5.2 Titration solvent
       5.3 Potassium hydrogen phthalate, primary standard
       5.4 Standard hydrochloric acid solution
       5.5 Alkali Blue 6B indicator solution
       5.6 Cobalt nitrate solution
    6 Apparatus
       6.1 Titration vessel
       6.2 Stirrer
       6.3 Burette
    7 Sampling
    8 Procedure
       8.1 Standardization of alcoholic potassium hydroxide
            solution
       8.2 Blank titration
       8.3 Sample titration
    9 Calculation of results
    10 Precision
       10.1 Repeatability
       10.2 Reproducibility
    11 Report
    Annex A (informative) Determination of acidity in electrical
            insulating oils by photometric titration
    Annex ZA (normative) Normative references to international
             publications with their corresponding European
             publications

    Abstract - (Show below) - (Hide below)

    Describes a procedure for determination of the acidity of unused and used electrical mineral insulating oils.

    Scope - (Show below) - (Hide below)

    Describes a procedure for determination of the acidity of unused and used electrical mineral insulating oils. The method may be used to indicate relative changes that occur in a mineral insulating oil during use under oxidizing conditions that may or may not be shown by other properties of the resulting mineral oil. The acidity can be used in the quality control of unused mineral oil. As a variety of oxidation products present in used mineral oil contribute to acidity and these products vary widely in their corrosion properties, the test cannot be used to predict corrosiveness of a mineral oil under service conditions.

    General Product Information - (Show below) - (Hide below)

    Committee GEL/10
    Document Type Standard
    Publisher British Standards Institution
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    08/30167496 DC : DRAFT FEB 2008 BS 148 - RECLAIMED MINERAL INSULATING OIL FOR TRANSFORMERS AND SWITCHGEAR - SPECIFICATION
    BS 148:2009 Reclaimed mineral insulating oil for transformers and switchgear. Specification

    Standards Referencing This Book - (Show below) - (Hide below)

    IEC 60475:2011 Method of sampling insulating liquids
    IEC 60567:2011 Oil-filled electrical equipment - Sampling of gases and analysis of free and dissolved gases - Guidance
    ISO 6619:1988 Petroleum products and lubricants — Neutralization number — Potentiometric titration method
    EN 60567:2011 OIL-FILLED ELECTRICAL EQUIPMENT - SAMPLING OF GASES AND ANALYSIS OF FREE AND DISSOLVED GASES - GUIDANCE (IEC 60567:2011)
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