![header thumbnail](/images/publishers\bsi_cover.gif)
BS EN ISO 22959:2009
Current
The latest, up-to-date edition.
![header thumbnail](/images/publishers\bsi_cover.gif)
Animal and vegetable fats and oils. Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection
Hardcopy , PDF
English
30-06-2009
Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents, materials and standards
6 Apparatus
7 Sampling and preparation of the test sample
8 Sample preparation
9 Procedure
9.1 HPLC analysis
9.2 Identification of PAHs
10 Calculation of individual PAHs
11 Method validation data
11.1 Accuracy
11.2 Within-laboratory precision
11.3 Recovery
11.4 Dynamic range
11.5 Limit of quantification
12 Precision
12.1 International collaborative trial
12.2 Repeatability
12.3 Reproducibility
13 Test report
Annex A (informative) - Example of the individual parts
of an HPLC system
Annex B (informative) - Example of the operating conditions
of the pumps of the HPLC system
Annex C (informative) - Example of the operating conditions
of the column thermostat and the detector of the
HPLC system
Annex D (informative) - Example of the autosampler programme
of the HPLC system
Annex E (informative) - Tubing connections of the HPLC system
Annex F (informative) - Chromatogram of a standard calibration
sample
Annex G (informative) - Determination precision for a sunflower
oil, range 0,1 [mu]g/kg to 3,5 [mu]g/kg
Annex H (informative) - Determination precision for an olive
oil, range 0,1 [mu]g/kg to 3,5 [mu]g/kg
Annex I (informative) - Determination precision for a soybean
oil, range 0,1 [mu]g/kg to 3,5 [mu]g/kg
Annex J (informative) - Determination precision for a coconut
oil, range 0,1 [mu]g/kg to 3,5 [mu]g/kg
Annex K (informative) - Interlaboratory test
Bibliography
Access your standards online with a subscription
Features
-
Simple online access to standards, technical information and regulations.
-
Critical updates of standards and customisable alerts and notifications.
-
Multi-user online standards collection: secure, flexible and cost effective.