BS ISO 13913:2014
Current
The latest, up-to-date edition.
Soil quality. Determination of selected phthalates using capillary gas chromatography with mass spectrometric detection (GC/MS)
Hardcopy , PDF
English
30-09-2014
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Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling and sample storage
8 Procedure
9 Calibration
10 Calculation
11 Expression of results
12 Precision
13 Test report
Annex A (informative) - Repeatability and reproducibility
data
Annex B (informative) - Example of a reference solution
for multipoint calibration
Annex C (informative) - Examples for gas chromatographic
conditions
Annex D (informative) - Flow scheme of the determination
of phthalates
Bibliography
Defines a method for the determination of selected phthalates in sludge, treated biowaste, and soil, after extraction and gas chromatographic analysis with mass spectrometric detection.
| Committee |
EH/4
|
| DevelopmentNote |
Supersedes 12/30231394 DC. (09/2014)
|
| DocumentType |
Standard
|
| Pages |
32
|
| PublisherName |
British Standards Institution
|
| Status |
Current
|
| Supersedes |
This International Standard specifies a method for the determination of selected phthalates in sludge, treated biowaste, and soil, after extraction and gas chromatographic analysis with mass spectrometric detection. The method is applicable for the determination of phthalates (see Table2) at the lowest mass content of 0,1mg/kg to 0,5mg/kg (expressed as dry matter), depending on the individual substance. The applicability of the method to other phthalates not specified in Table2 is not excluded except the isomeric mixtures, e.g. DiNP (Di-isononylphthalate), but shall be verified in each case. Table2 Phthalates that can be determined according to this International Standard No Name Formula Abbreviation Molar massg/mol CAS-RNa 1 Dimethylphthalate C10H10O4 DMP 194,2 00131-11-3 2 Diethylphthalate C12H14O4 DEP 222,2 00084-66-2 3 Dipropylphthalate C14H18O4 DPP 250,3 00131-16-8 4 Di-(2-methyl-propyl)phthalate C16H22O4 DiBP 278,4 00084-69-5 5 Dibutylphthalate C16H22O4 DBP 278,4 00084-74-2 6 Butylbenzylphthalate C19H20O4 BBzP 312,4 00085-68-7 7 Dicyclohexylphthalate C20H26O4 DCHP 330,4 00084-61-7 8 Di-(2-ethylhexyl)phthalate C24H38O4 DEHP 390,6 00117-81-7 9 Dioctylphthalate C24H38O4 DOP 390,6 00117-84-0 10 Didecylphthalate C28H46O4 DDcP 446,7 00084-77-5 11 Diundecylphthalate C30H50O4 DUP 474,4 03648-20-2 a Chemical Abstracts Service Registry Number.
| Standards | Relationship |
| ISO 13913:2014 | Identical |
| ISO 5667-13:2011 | Water quality Sampling Part 13: Guidance on sampling of sludges |
| ISO 22892:2006 | Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| ISO 383:1976 | Laboratory glassware — Interchangeable conical ground joints |
| ISO 10381-2:2002 | Soil quality Sampling Part 2: Guidance on sampling techniques |
| ISO 5667-15:2009 | Water quality — Sampling — Part 15: Guidance on the preservation and handling of sludge and sediment samples |
| ISO 14507:2003 | Soil quality Pretreatment of samples for determination of organic contaminants |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 8466-1:1990 | Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function |
| EN 15934:2012 | Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content |
| EN 16179:2012 | Sludge, treated biowaste and soil - Guidance for sample pretreatment |
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