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BS ISO 18363-1:2015

Current

Current

The latest, up-to-date edition.

Animal and vegetable fats and oils. Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS Method using fast alkaline transesterification and measurement for 3-MCPD and differential measurement for glycidol

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

28-09-2018

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Sample
8 Procedure
9 Expression of results
10 Precision
11 Test report
Annex A (informative) - Results of an collaborative trial
Bibliography

Explains a procedure for the indirect determination of 3-MCPD esters (bound 3-MCPD) and possible free 3-MCPD after alkaline catalysed ester cleavage and derivatization with phenylboronic acid (PBA).

This part of ISO18363 describes a procedure for the indirect determination of 3-MCPD esters (bound 3-MCPD) and possible free 3-MCPD after alkaline catalysed ester cleavage and derivatization with phenylboronic acid(PBA). Furthermore, this part of ISO18363 enables the indirect determination of glycidyl esters (bound glycidol) under the assumption that no other substances are present that react at room temperature with inorganic chloride to generate 3-MCPD.

This part of ISO18363 is applicable to solid and liquid fats and oils. Milk and milk products (or fat coming from milk and milk products) are excluded from the scope of this part of ISO18363.

Committee
AW/307
DevelopmentNote
Supersedes 14/30278508 DC. (09/2015)
DocumentType
Standard
ISBN
9780539025279
Pages
22
PublisherName
British Standards Institution
Status
Current
Supersedes

Standards Relationship
ISO 18363-1:2015 Identical

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