• BS ISO 18917:1999

    Current The latest, up-to-date edition.

    Photography. Determination of residual thiosulfate and other related chemicals in processed photographic materials. Methods using iodine-amylose, methylene blue and silver sulfide

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  15-04-2000

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    1 Scope
    2 Normative references
    3 General requirements
    4 Iodine-amylose method
    5 Methylene blue method
    6 Silver densitometric method
    Annex A (informative) Appraisal of keeping characteristics
    Annex B (informative) Guidance in the selection of test method
    Annex C (informative) Preparation for 0,2 mol/l sodium
                          hydroxide solution
    Annex D (informative) Preparation of 1,000 mol/l sodium
                          thiosulfate solution
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines test procedures for determining residual thiosulfate and other related chemicals in processed photographic materials.

    Scope - (Show below) - (Hide below)

    1.1 This International Standard specifies test methods for the determination of residual thiosulfate and other related chemicals in processed photographic materials.

    1.2 This International Standard applies to silver halide/gelatin products that have been processed with a final thiosulfate fixing bath and a water wash. This International Standard does not apply to stabilised black-and-white products, thermally processed films, or instant-type products. The procedures given in this International Standard measure residual thiosulfate, and the silver densitometric method measures residual related polythionate materials as well. Measurements carried out by the procedures in this International Standard may, within the limitations stated in annexes A and B, correlate with the image stabilities of processed photographs.

    1.3 Film or plates with photographic-sensitive layers on both sides, or with a photographic sensitive layer on one side and a gelatin backing layer on the reverse side, may contain approximately twice as much thiosulfate after processing as samples having a coating on one side only. This situation will be true for materials for which residual thiosulfate is determined by the iodine-amylose or methylene blue procedures.

    NOTE For the method of reporting such results, see figure 1, example 2.

    1.4 The iodine-amylose can be used with fibre-based paper, resin-coated paper, films and plates. It is the method to be used with films and papers containing incorporated developing agents.

    1.5 The methylene blue method can be used with fibre-based paper, resin-coated paper, films and plates but not with films and paper containing incorporated developing agents.

    1.6 The silver sulfide densitometric method measures thiosulfates, polythionates and all other residual chemicals in a processed product that react with silver ion to form a silver \'stain\' under the conditions of the test.

    1.7 A tabulated summary of methods, scope, etc. is given in annex B.

    General Product Information - (Show below) - (Hide below)

    Committee CPW/42
    Development Note Supersedes BS ISO 417. (03/2000) Supersedes 97/712494 DC. (07/2005) Reviewed and confirmed by BSI, August 2016. (07/2016)
    Document Type Standard
    Publisher British Standards Institution
    Status Current
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    BS 6313:2003 Micrographics. 35 mm microfilming of serials. Specification
    BS 0-3:1997 A standard for standards Specification for structure, drafting and presentation

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 835-4:1981 Laboratory glassware Graduated pipettes Part 4: Blow-out pipettes
    ISO 6051:1997 Photography Processed reflection prints Storage practices
    ISO 3897:1997 Photography Processed photographic plates Storage practices
    ISO 6353-1:1982 Reagents for chemical analysis — Part 1: General test methods
    ISO 5466:1996 Photography — Processed safety photographic films — Storage practices
    ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
    ISO 10602:1995 Photography — Processed silver-gelatin type black-and-white film — Specifications for stability
    ISO 648:2008 Laboratory glassware — Single-volume pipettes
    ISO 4788:2005 Laboratory glassware Graduated measuring cylinders
    ISO 835-2:1981 Laboratory glassware Graduated pipettes Part 2: Pipettes for which no waiting time is specified
    ISO 10349-1:2002 Photography Photographic-grade chemicals Test methods Part 1: General
    ISO 385-1:1984 Laboratory glassware — Burettes — Part 1: General requirements
    ISO 835-3:1981 Laboratory glassware Graduated pipettes Part 3: Pipettes for which a waiting time of 15 s is specified
    ISO 6353-3:1987 Reagents for chemical analysis — Part 3: Specifications — Second series
    ISO 5-3:2009 Photography and graphic technology Density measurements Part 3: Spectral conditions
    ISO 835-1:1981 Laboratory glassware Graduated pipettes Part 1: General requirements
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