DD ENV 13999-2:2002
Withdrawn
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Adhesives. Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application Determination of volatile organic compounds
Hardcopy , PDF
31-05-2007
English
12-12-2002
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Foreword
1 Scope
2 Normative references
3 Principle
4 Safety
5 Reagents and materials
5.1 Volatile organic compounds for calibration, of gas
chromatographic grade
5.2 Methanol, of gas chromatographic grade
5.3 Sorbent material
5.4 Carrier gas
6 Apparatus
6.1 Sorbent tubes
6.2 Sorbent tube unions
6.3 Syringes
6.4 Sampling pump
6.5 Tubing
6.6 Flow meter calibrator
6.7 Gas chromatograph
6.8 Thermal desorption apparatus
6.9 Injection facility for preparing standards by liquid
spiking
7 Procedure
7.1 Preparation of sampling tubes
7.1.1 Preconditioning
7.1.2 Conditioning
7.1.3 Storage of conditioned sorbent tubes before
sampling
7.2 Test chamber air sampling
7.3 Storage of loaded sampling tubes
7.4 Blank tubes
7.5 Preparation of calibration blend solutions for liquid
spiking
7.5.1 Solution containing approximately 10 mg/ml of
each liquid component
7.5.2 Solution containing approximately 1000 micromg/ml
of each liquid comp
7.5.3 Solution containing approximately 100 micromg/ml of
each liquid component
7.5.4 Solution containing approximately 10 micromg/ml of
each liquid component
7.5.5 Stability of calibration blend solutions
7.6 Preparation of calibration sorbent tubes spiked with
standards
7.7 Analysis
7.7.1 Desorption
7.7.2 Gas chromatographic analysis
7.7.3 Calibration
8 Identification and calculation
8.1 Identification of single VOC's
8.1.1 Identification Classes
8.2 Concentration of single VOC's in the sampled air
8.3 Calculation of TVOC[eng 13999]
9 Precision and Bias
10 Test report
11 Quality control
Bibliography
Gives a method for the determination of single volatile organic compounds (VOC's) and of the total amount of volatile organic compounds in the exhaust air of an emission test chamber after application of an adhesive (TVOC[ENV 13999]).
| Committee |
PRI/52
|
| DevelopmentNote |
Reviewed and confirmed by BSI, October 2005. (10/2005)
|
| DocumentType |
Standard
|
| Pages |
16
|
| PublisherName |
British Standards Institution
|
| Status |
Withdrawn
|
| SupersededBy |
| Standards | Relationship |
| ENV 13999-2 : DRAFT 2002 | Identical |
| EN ISO 16017-1:2000 | Indoor, ambient and workplace air - Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography - Part 1: Pumped sampling (ISO 16017-1:2000) |
| ISO 16017-1:2000 | Indoor, ambient and workplace air — Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography — Part 1: Pumped sampling |
| ENV 13999-1 : DRAFT 2001 | ADHESIVES - SHORT TERM METHOD FOR MEASURING THE EMISSION PROPERTIES OF LOW-SOLVENT OR SOLVENT-FREE ADHESIVES AFTER APPLICATION - PART 1: GENERAL PROCEDURE |
| EN 1232:1997 | Workplace atmospheres - Pumps for personal sampling of chemical agents - Requirements and test methods |
| ENV 13419-1 : DRAFT 99 | BUILDING PRODUCTS - DETERMINATION OF THE EMISSION OF VOLATILE ORGANIC COMPOUNDS - PART 1: EMISSION TEST CHAMBER METHOD |
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