DD ENV 13999-4:2002
Superseded
A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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Adhesives. Short term method for measuring the emission properties of low-solvent or solvent-free adhesives after application Determination of volatile diisocyanates
Hardcopy , PDF
31-05-2007
English
12-12-2002
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Foreword
1 Scope
2 Normative references
3 Principle
4 Safety
5 Reagents and materials
6 Apparatus
6.1 Sampler
6.1.1 Filter holder
6.1.2 Filter
6.2 Filtration equipment
6.3 Sampling pump
6.4 Tubing
6.5 Flow meter calibrator
6.6 High performance liquid chromatograph (HPLC)
7 Procedure
7.1 Preparation of sampling devices
7.2 Test chamber air sampling
7.3 Storage of loaded sampling filters
7.4 Blanks
7.5 Analysis
7.5.1 Cleaning of glassware
7.5.2 Sample desorption and pre-reaction before HPLC
analysis
7.5.3 Preparation of calibration standards
7.5.4 Calibration of liquid chromatograph
7.5.5 Analysis of pre-reacted sample solutions
8 Identification and calculation
8.1 Identification and isocyanates
8.2 Concentration of analytes in the sampled air
9 Interferences
10 Precision and bias
11 Test report
12 Quality control
Bibliography
Gives a procedure for the determination of volatile organic isocyanates in the exhaust air of an emission test chamber after application of an adhesive.
| Committee |
PRI/52
|
| DevelopmentNote |
Reviewed and confirmed by BSI, October 2005. (10/2005)
|
| DocumentType |
Standard
|
| Pages |
14
|
| PublisherName |
British Standards Institution
|
| RevisionOf | |
| Status |
Superseded
|
| SupersededBy |
| Standards | Relationship |
| ENV 13999-4 : DRAFT 2002 | Identical |
| EN ISO 16017-1:2000 | Indoor, ambient and workplace air - Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography - Part 1: Pumped sampling (ISO 16017-1:2000) |
| ISO 16017-1:2000 | Indoor, ambient and workplace air — Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography — Part 1: Pumped sampling |
| ISO 16702:2007 | Workplace air quality — Determination of total organic isocyanate groups in air using 1-(2-methoxyphenyl)piperazine and liquid chromatography |
| ENV 13999-1 : DRAFT 2001 | ADHESIVES - SHORT TERM METHOD FOR MEASURING THE EMISSION PROPERTIES OF LOW-SOLVENT OR SOLVENT-FREE ADHESIVES AFTER APPLICATION - PART 1: GENERAL PROCEDURE |
| EN 1232:1997 | Workplace atmospheres - Pumps for personal sampling of chemical agents - Requirements and test methods |
| ENV 13419-1 : DRAFT 99 | BUILDING PRODUCTS - DETERMINATION OF THE EMISSION OF VOLATILE ORGANIC COMPOUNDS - PART 1: EMISSION TEST CHAMBER METHOD |
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