• DIN EN 13925-3:2005-07

    Current The latest, up-to-date edition.

    NON-DESTRUCTIVE TESTING - X RAY DIFFRACTION FROM POLYCRYSTALLINE AND AMORPHOUS MATERIALS - PART 3: INSTRUMENTS

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  01-01-2005

    Publisher:  German Institute for Standardisation (Deutsches Institut für Normung)

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Description of equipment
       4.1 General
       4.2 X-ray sources
            4.2.1 General
            4.2.2 Conventional X-ray sources (sealed tubes
                   and rotating anode sources)
            4.2.3 Synchrotron radiation sources
       4.3 Incident and diffracted X-ray beam optics
            4.3.1 General
            4.3.2 Monochromators
            4.3.3 Beam dimensions and geometry
       4.4 Detectors
            4.4.1 Types of detector
            4.4.2 Spatial resolution of detectors
            4.4.3 Energy resolution of detectors
       4.5 Goniometers
            4.5.1 General
            4.5.2 Specimen positioning
       4.6 Specimen stage
       4.7 Data collection system
    5 Characterisation of equipment components
    6 Equipment alignment and calibration
       6.1 General
       6.2 Alignment
       6.3 Calibration
    7 Performance testing and monitoring
    Annex A (informative) Relationship between the XRPD
            standards
    Annex B (informative) Alignment of Bragg-Brentano
            diffractometers
    Annex C (informative) Procedures for instrument performance
            characterisation
     C.1 General
     C.2 Position, intensity and breadth of a limited number
          of diffraction lines
     C.3 Angular Deviation Curve
     C.4 Line breadth
     C.5 Intensity diagrams
     C.6 Shape Analysis Curve
     C.7 Lattice parameters
     C.8 The use of the Fundamental Parameter Approach
     C.9 Whole pattern fitting
    Annex D (informative) Sample report forms for characterisation
            of instruments
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines the characteristics of instruments used for X-ray powder diffraction as a basis for their control and hence quality assurance of the measurements made by this technique.

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    Document Type Standard
    Publisher German Institute for Standardisation (Deutsches Institut für Normung)
    Status Current

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
    EN 13925-1:2003 Non-destructive testing - X-ray diffraction from polycrystalline and amorphous material - Part 1: General principles
    EN 13925-2:2003 Non-destructive testing - X-ray diffraction from polycrystalline and amorphous materials - Part 2: Procedures
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