• EN 10351:2011

    Current The latest, up-to-date edition.

    Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Mn, P, Cu, Ni, Cr, Mo, V, Co, Al (total) and Sn [Routine method]

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    Published date:  02-03-2011

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Principle
    4 Reagents
    5 Apparatus
    6 Sampling
    7 Sample solution preparation
    8 Calibration process
    9 Determination
    10 Expression of results
    11 Precision
    12 Test report
    Annex A (informative) - Plasma optical emission
            spectrometer - Suggested performance criteria
            to be checked
    Annex B (normative) - Synoptic of the operations
            related to Clause 9
    Annex C (informative) - Test samples used for the
            validation precision test
    Annex D (informative) - Detailed results obtained
            from the validation precision test
    Annex E (informative) - Graphical representation
            of the precision data
    Bibliography

    Abstract - (Show below) - (Hide below)

    This European Standard specifies an inductively coupled plasma optical emission spectrometry routine method for the analysis of unalloyed and low alloyed steels, whose iron content shall be at least 95 %.This method is applicable to the elements listed in Table 1 within the ranges shown.Table 1 - Application ranges(...)In all cases, the ranges specified can be extended or adapted (after validation) for the determination of other mass fractions, provided that the iron content in the samples under concern is above 95 %.Other elements may be included. However such elements and their mass fractions should be carefully checked, taking into account the possible interferences, the sensitivity, the resolution and the linearity criteria of each instrument and each wavelength.Depending also on the sensitivity of each instrument, suitable dilutions of the calibration and the test sample solutions may be necessary.Moreover, even if the method described is "multi elemental", it is not absolutely necessary to carry out the determination of all the elements of its scope simultaneously: the measurement conditions have to be optimised by each laboratory, depending on the performances of each apparatus available.NOTE 1The accuracy of the method is unsatisfactory for phosphorus contents from 0,05 to 0,1 %.NOTE 2The trueness of the method couldn't be checked for vanadium contents below 0,05 %.NOTE 3The precision of the method is unsatisfactory for aluminium (total) contents below 0,02 %.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 459/SC 2
    Development Note Supersedes PREN 10351. (08/2011)
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    EN 10355:2013 Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Si, Mn, P, Cu, Ni, Cr, Mo and Sn, following dissolution with nitric and sulphuric acids [Routine method]
    VDI 3405 Blatt 2:2013-08 Additive manufacturing processes, rapid manufacturing - Beam melting of metallic parts - Qualification, quality assurance and post processing
    11/30252539 DC : 0 BS EN 10355 - CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF SI, MN, P, CU, NI, CR, MO, SN [ROUTINE METHOD]
    DIN EN 10355:2013-11 Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Si, Mn, P, Cu, Ni, Cr, Mo and Sn, following dissolution with nitric and sulphuric acids [Routine method]
    DIN EN 10355 E : 2013 CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF SI, MN, P, CU, NI, CR, MO AND SN, FOLLOWING DISSOLUTION WITH NITRIC AND SULPHURIC ACIDS [ROUTINE METHOD]
    UNE-EN 10355:2014 Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Si, Mn, P, Cu, Ni, Cr, Mo and Sn, following dissolution with nitric and sulphuric acids [Routine method]
    BS EN 10355:2013 Chemical analysis of ferrous materials. Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels. Determination of Si, Mn, P, Cu, Ni, Cr, Mo and Sn, following dissolution with nitric and sulphuric acids [Routine method]
    UNI EN 10355 : 2013 CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF SI, MN, P, CU, NI, CR, MO AND SN, FOLLOWING DISSOLUTION WITH NITRIC AND SULPHURIC ACIDS [ROUTINE METHOD]
    PD CEN/TR 10261:2013 Iron and steel. European standards for the determination of chemical composition
    I.S. EN 10355:2013 CHEMICAL ANALYSIS OF FERROUS MATERIALS - INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRIC ANALYSIS OF UNALLOYED AND LOW ALLOYED STEELS - DETERMINATION OF SI, MN, P, CU, NI, CR, MO AND SN, FOLLOWING DISSOLUTION WITH NITRIC AND SULPHURIC ACIDS [ROUTINE METHOD]
    CEN/TR 10261:2013 Iron and steel - European standards for the determination of chemical composition

    Standards Referencing This Book - (Show below) - (Hide below)

    EN ISO 14284:2002 Steel and iron - Sampling and preparation of samples for the determination of chemical composition (ISO 14284:1996)
    ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
    ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
    ISO 648:2008 Laboratory glassware — Single-volume pipettes
    ISO 5725-3:1994 Accuracy (trueness and precision) of measurement methods and results — Part 3: Intermediate measures of the precision of a standard measurement method
    EN 29658:1991 Steel - Determination of aluminium content - Flame atomic absorption spectrometric method (ISO 9658:1990)
    EN 15605:2010 Copper and copper alloys - Inductively coupled plasma optical emission spectrometry
    CEN/TR 10345:2013 Guideline for statistical data treatment of inter laboratory tests for validation of analytical methods
    ISO 9658:1990 Steel — Determination of aluminium content — Flame atomic absorption spectrometric method
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
    EN 15079:2015 Copper and copper alloys - Analysis by spark optical emission spectrometry (S-OES)
    EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
    ISO 10138:1991 Steel and iron — Determination of chromium content — Flame atomic absorption spectrometric method
    ISO 14284:1996 Steel and iron — Sampling and preparation of samples for the determination of chemical composition
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