EN 12393-1:2013
Current
The latest, up-to-date edition.
Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 1: General considerations
13-11-2013
Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Procedure
7 Determination
8 Confirmatory tests
9 Evaluation of results
10 Test report
Annex A (informative) - Purification of solvents and
reagents
Bibliography
This European Standard gives general considerations for the determination of pesticide residues in foods of plant origin.Each method specified in this European Standard is suitable for identifying and quantifying a definite range of those organohalogen, and/or organophosphorus and/or organonitrogen pesticides which occur as residues in foodstuffs of plant origin.This European Standard contains the following methods that have been subjected to interlaboratory studies and/or are adopted throughout Europe:-method M: Extraction with acetone and liquid liquid partition with dichloromethane/light petroleum, if necessary clean-up on Florisil® 1) [1], [2], [3];-method N: Extraction with acetone, liquid liquid partition with dichloromethane or cyclohexane/ethyl acetate and clean-up with gel permeation and silica gel chromatography [4], [5];-method P: Extraction with ethyl acetate and, if necessary, clean-up with gel permeation chromatography [6].The applicability of the three methods M, N and P for residue analysis of organohalogen, organophosphorus and organonitrogen pesticides, respectively, is given for each method.
Committee |
CEN/TC 275
|
DevelopmentNote |
Supersedes PREN 12393-1. (11/2013)
|
DocumentType |
Standard
|
PublisherName |
Comite Europeen de Normalisation
|
Status |
Current
|
Supersedes |
Standards | Relationship |
UNE-EN 12393-1:2014 | Identical |
NBN EN 12393-1 : 2014 | Identical |
UNI EN 12393-1 : 2014 | Identical |
I.S. EN 12393-1:2013 | Identical |
BS EN 12393-1:2013 | Identical |
NF EN 12393-1 : 2013 | Identical |
NEN EN 12393-1 : 2013 | Identical |
DIN EN 12393-1:2014-01 | Identical |
PN EN 12393-1 : 2014 | Identical |
NS EN 12393-1 : 2013 | Identical |
SN EN 12393-1 : 2014 | Identical |
DIN EN 12393-2:2014-03 | FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 2: METHODS FOR EXTRACTION AND CLEANUP |
UNE-EN 12393-2:2014 | Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 2: Methods for extraction and clean-up |
EN 12393-3:2013 | Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 3: Determination and confirmatory tests |
EN 12396-3:2000 | Non-fatty foods - Determination of dithiocarbamate and thiuram disulfide residues - Part 3: UV spectrometric xanthogenate method |
EN 12396-1:1998 | Non-fatty foods - Determination of dithiocarbamate and thiuram disulfide residues - Part 1: Spectrometric method |
EN 12393-2:2013 | Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 2: Methods for extraction and clean-up |
EN 12396-2:1998 | Non-fatty foods - Determination of dithiocarbamate and thiuram disulfide residues - Part 2: Gas chromatographic method |
I.S. EN 12393-3:2013 | FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 3: DETERMINATION AND CONFIRMATORY TESTS |
I.S. EN 12393-2:2013 | FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 2: METHODS FOR EXTRACTION AND CLEAN-UP |
BS EN 12393-2:2013 | Foods of plant origin. Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS Methods for extraction and clean-up |
UNE-EN 12393-3:2014 | Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 3: Determination and confirmatory tests |
UNI EN 12393-2 : 2014 | FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 2: METHODS FOR EXTRACTION AND CLEAN-UP |
UNI EN 12393-3 : 2014 | FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 3: DETERMINATION AND CONFIRMATORY TESTS |
BS EN 12396-2:1999 | Non-fatty foods. Determination of dithiocarbamate and thiuram disulfide residues Gas chromatographic method |
BS EN 12396-3:2000 | Non-fatty foods. Determination of dithiocarbamate and thiuram disulfide residues UV spectrometric xanthogenate method |
BS EN 12393-3:2013 | Foods of plant origin. Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS Determination and confirmatory tests |
07/30160744 DC : 0 | BS EN 12393-2 - FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE GAS CHROMATOGRAPHIC DETERMINATION OF PESTICIDE RESIDUES - PART 2: METHODS FOR EXTRACTION AND CLEAN-UP |
DIN EN 12393-3:2014-01 | FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 3: DETERMINATION AND CONFIRMATORY TESTS |
BS EN 12396-1:1999 | Non-fatty foods. Determination of dithiocarbamate and thiuram disulfide residues Spectrometric method |
EN 12393-3:2013 | Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 3: Determination and confirmatory tests |
EN 12393-2:2013 | Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 2: Methods for extraction and clean-up |
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