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EN 12393-1:2013

Current

Current

The latest, up-to-date edition.

Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 1: General considerations

Published date

13-11-2013

Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Procedure
7 Determination
8 Confirmatory tests
9 Evaluation of results
10 Test report
Annex A (informative) - Purification of solvents and
        reagents
Bibliography

This European Standard gives general considerations for the determination of pesticide residues in foods of plant origin.Each method specified in this European Standard is suitable for identifying and quantifying a definite range of those organohalogen, and/or organophosphorus and/or organonitrogen pesticides which occur as residues in foodstuffs of plant origin.This European Standard contains the following methods that have been subjected to interlaboratory studies and/or are adopted throughout Europe:-method M: Extraction with acetone and liquid liquid partition with dichloromethane/light petroleum, if necessary clean-up on Florisil® 1) [1], [2], [3];-method N: Extraction with acetone, liquid liquid partition with dichloromethane or cyclohexane/ethyl acetate and clean-up with gel permeation and silica gel chromatography [4], [5];-method P: Extraction with ethyl acetate and, if necessary, clean-up with gel permeation chromatography [6].The applicability of the three methods M, N and P for residue analysis of organohalogen, organophosphorus and organonitrogen pesticides, respectively, is given for each method.

Committee
CEN/TC 275
DevelopmentNote
Supersedes PREN 12393-1. (11/2013)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current
Supersedes

DIN EN 12393-2:2014-03 FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 2: METHODS FOR EXTRACTION AND CLEANUP
UNE-EN 12393-2:2014 Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 2: Methods for extraction and clean-up
EN 12393-3:2013 Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 3: Determination and confirmatory tests
EN 12396-3 : 2000 NON-FATTY FOODS - DETERMINATION OF DITHIOCARBAMATE AND THIURAM DISULFIDE RESIDUES - PART 3: UV SPECTROMETRIC XANTHOGENATE METHOD
EN 12396-1 : 1998 NON-FATTY FOODS - DETERMINATION OF DITHIOCARBAMATE AND THIURAM DISULFIDE RESIDUES - PART 1: SPECTROMETRIC METHOD
EN 12393-2:2013 Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 2: Methods for extraction and clean-up
EN 12396-2 : 1998 NON-FATTY FOODS - DETERMINATION OF DITHIOCARBAMATE AND THIURAM DISULFIDE RESIDUES - PART 2: GAS CHROMATOGRAPHIC METHOD
I.S. EN 12393-3:2013 FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 3: DETERMINATION AND CONFIRMATORY TESTS
I.S. EN 12393-2:2013 FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 2: METHODS FOR EXTRACTION AND CLEAN-UP
BS EN 12393-2:2013 Foods of plant origin. Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS Methods for extraction and clean-up
UNE-EN 12393-3:2014 Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 3: Determination and confirmatory tests
UNI EN 12393-2 : 2014 FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 2: METHODS FOR EXTRACTION AND CLEAN-UP
UNI EN 12393-3 : 2014 FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 3: DETERMINATION AND CONFIRMATORY TESTS
BS EN 12396-2:1999 Non-fatty foods. Determination of dithiocarbamate and thiuram disulfide residues Gas chromatographic method
BS EN 12396-3:2000 Non-fatty foods. Determination of dithiocarbamate and thiuram disulfide residues UV spectrometric xanthogenate method
BS EN 12393-3:2013 Foods of plant origin. Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS Determination and confirmatory tests
07/30160744 DC : 0 BS EN 12393-2 - FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE GAS CHROMATOGRAPHIC DETERMINATION OF PESTICIDE RESIDUES - PART 2: METHODS FOR EXTRACTION AND CLEAN-UP
DIN EN 12393-3:2014-01 FOODS OF PLANT ORIGIN - MULTIRESIDUE METHODS FOR THE DETERMINATION OF PESTICIDE RESIDUES BY GC OR LC-MS/MS - PART 3: DETERMINATION AND CONFIRMATORY TESTS
BS EN 12396-1:1999 Non-fatty foods. Determination of dithiocarbamate and thiuram disulfide residues Spectrometric method

EN 12393-3:2013 Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 3: Determination and confirmatory tests
EN 12393-2:2013 Foods of plant origin - Multiresidue methods for the determination of pesticide residues by GC or LC-MS/MS - Part 2: Methods for extraction and clean-up

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