EN 12457-3:2002

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Characterisation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 3: Two stage batch test at a liquid to solid ratio of 2 l/kg and 8 l/kg for materials with high solid content and with particle size below 4 mm (without or with size reduction)

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Published date: 18-09-2002

Publisher: Comite Europeen de Normalisation

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Table of Contents - (Show below) - (Hide below)

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
  3.1 Leaching test
  3.2 Leachant
  3.3 Eluate
  3.4 Single batch leaching test
  3.5 Serial batch leaching test
  3.6 Liquid to solid ratio L/S (abbreviation: L/S)
  3.7 Liquid waste
  3.8 Sludge
  3.9 Monolithic waste
  3.10 Granular waste
  3.11 Dry matter content ratio (abbreviation: DR)
  3.12 Moisture content ratio (abbreviation MC)
  3.13 Laboratory sample
  3.14 Test sample
  3.15 Test portion
4 Compliance test
  4.1 Principle
  4.2 Equipment and reagents
  4.3 Sampling strategy and sample preparation
5 Procedure
  5.1 Testing conditions
  5.2 Description of the procedure
  5.3 Further preparation of the eluate for analysis
  5.4 Blank test for the verification of the leaching
       procedure
6 Calculation
  6.1 Expression of the results
  6.2 First step batch at L/S = 2
  6.3 Second step batch at L/S = 8
7 Documentation and test report
  7.1 Sample preparation
  7.2 Production of eluate
  7.3 Analytical determination
  7.4 Calculations and blank test information
8 Performance characteristics
  8.1 Objective of the validation
  8.2 Validation study
  8.3 Validation results
  8.4 Summary of the performance characteristics evaluation
Annex A (informative) Information on the influence on the
         test results of the parameters that effect leaching
Annex B (informative) Test for determining whether waste is
         in the liquid state
Annex C (informative) Example of datasheet for EN 12457-3
Annex D (informative) Process map for EN 12457-3
Annex E (informative) Example of a specific liquid-solid
         separation procedure for soil sample
Annex ZA (informative) National deviation A from France
Bibliography

Abstract - (Show below) - (Hide below)

This part of the European Standard specifies a compliance test providing information on leaching of granular wastes and sludges under the experimental conditions specified hereafter, and particularly a liquid to solid ratio of 2 l/kg dry matter and subsequently of 8 l/kg dry matter. It applies to waste which has a particle size below 4 mm without or with size reduction. The test procedure specified in this Standard produces an eluate which shall subsequently be characterised physically and chemically according to appropriate standard methods.

General Product Information - (Show below) - (Hide below)

Committee	CEN/TC 444
Document Type	Standard
ISBN
Pages
Published
Publisher	Comite Europeen de Normalisation
Status	Current

National Adoptions - (Show below) - (Hide below)

Equivalent Standard(s)	Relationship
NF EN 12457-3 : 2002	Identical
UNE-EN 12457-3:2003	Identical
ONORM EN 12457-3 : 2003	Identical
ÖNORM EN 12457-3:2021 11 15	Identical
NS EN 12457-3 : 1ED 2003	Identical
SN EN 12457-3 : 2002	Identical
I.S. EN 12457-3:2002	Identical
NBN EN 12457-3 : 2002	Identical
UNI EN 12457-3 : 2004	Identical
BS EN 12457-3:2002	Identical
PN EN 12457-3 : 2006	Identical
NEN EN 12457-3 : 2002	Identical
DIN EN 12457-3:2003-01	Identical

Standards Referenced By This Book - (Show below) - (Hide below)

DIN EN 14405:2017-05	CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
I.S. EN 12506:2003	CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, BA, CD, CL[-], CO, CR, CR (6), CU, MO, NI, NO[2-], PB, TOTAL S, SO[4][2-], V AND ZN
BS EN 14405:2017	Characterization of waste - Leaching behaviour test - Up-flow percolation test (under specified conditions)
14/30304804 DC : 0	BS EN 14405 - CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
I.S. EN 14405:2017	CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
PD CEN/TR 16376:2012	Characterization of waste. Overall guidance document for characterization of waste from the extractive industries
DIN EN 15863:2015-06	CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
DIN EN 12506:2003-09	CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, BA, CD, CI[-], CO, CR, CR(VI), CU, MO, NI, NO[2-], PB, TOTAL S, SO[4][2-], V AND ZN
EN 12506:2003	Characterization of waste - Analysis of eluates - Determination of pH, As, Ba, Cd, Cl-, Co, Cr, Cr Vl, Cu, Mo, Ni, NO2-, Pb, total S, SO42-, V and Zn
CEN/TR 16376:2012	Characterization of waste - Overall guidance document for characterization of waste from the extractive industries
EN 14405:2017	Characterization of waste - Leaching behaviour test - Up-flow percolation test (under specified conditions)
EN 15863:2015	Characterization of waste - Leaching behaviour test for basic characterization - Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions
UNI EN 16457 : 2014	CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
10/30233988 DC : 0	BS EN 16192 - CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
DIN EN 14405 E : 2017	CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
I.S. EN 16457:2014	CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
CEN/TS 16637-1:2014	Construction products - Assessment of release of dangerous substances - Part 1: Guidance for the determination of leaching tests and additional testing steps
PREN 14405 : DRAFT 2014	CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
UNI CEN/TS 16637-1 : 2014	CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 1: GUIDANCE FOR THE DETERMINATION OF LEACHING TESTS AND ADDITIONAL TESTING STEPS
UNE-EN 14405:2017	Characterization of waste - Leaching behaviour test - Up-flow percolation test (under specified conditions)
DIN EN 15863 E : 2015	CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
17/30348303 DC : 0	BS EN 17087 - CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE FOR TESTING OF RELEASE AND ANALYSIS OF CONTENT
UNE-EN 15863:2015	Characterization of waste - Leaching behaviour test for basic characterization - Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions
UNE-EN 15002:2015	Characterization of waste - Preparation of test portions from the laboratory sample
DIN EN 13370:2003-09	CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF AMMONIUM, AOX, CONDUCTIVITY, HG, PHENOL INDEX, TOC, CN[-] EASILY LIBERATABLE, F[-]
I.S. EN 15002:2015	CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
PD CEN/TS 16660:2015	Characterization of waste. Leaching behaviour test. Determination of the reducing character and the reducing capacity
BS EN 16192:2011	Characterization of waste. Analysis of eluates
DIN EN 16192:2012-02	Characterization of waste - Analysis of eluates
UNE-EN 16457:2014	Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
S.R. CEN/TR 16110:2010	CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
I.S. EN 16192:2011	CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
PD CEN/TS 16637-1:2014	Construction products. Assessment of release of dangerous substances Guidance for the determination of leaching tests and additional testing steps
S.R. CEN/TR 16376:2012	CHARACTERIZATION OF WASTE - OVERALL GUIDANCE DOCUMENT FOR CHARACTERIZATION OF WASTE FROM THE EXTRACTIVE INDUSTRIES
S.R. CEN/TS 16637-1:2014	CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 1: GUIDANCE FOR THE DETERMINATION OF LEACHING TESTS AND ADDITIONAL TESTING STEPS
BS EN 12506:2003	Characterization of waste. Analysis of eluates. Determination of pH, As, Ba, Cd, Cl$u-, Co, Cr, Cr VI, Cu, Mo, Ni, NO₂$u-, Pb, total S, SO₄²$u-, V and Zn
I.S. EN 13370:2003	CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF AMMONIUM, AOX, CONDUCTIVITY, HG, PHENOL INDEX, TOC, EASILY LIBERATABLE CN[-], F[-]
I.S. EN 15863:2015	CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
12/30263896 DC : 0	BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
DIN EN 16457:2014-07	CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
13/30291099 DC : 0	BS EN 15002 - CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
BS EN 15863:2015	Characterization of waste. Leaching behaviour test for basic characterization. Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions
BS EN 13370:2003	Characterization of waste. Analysis of eluates. Determination of Ammonium, AOX, conductivity, Hg, phenol index, TOC, easily liberatable CN$u-, F$u-
DIN EN 15002:2015-07	CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
EN 15002:2015	Characterization of waste - Preparation of test portions from the laboratory sample
EN 16457:2014	Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
13/30286658 DC : 0	BS EN 16660 - CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
DIN EN 16457 E : 2014	CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
BS EN 16457:2014	Characterization of waste. Framework for the preparation and application of a testing programme. Objectives, planning and report
04/30116791 DC : DRAFT JUL 2004	BS EN 15002 - CHARACTERISATION OF WASTE - PREPARATION OF TEST PORTIONS FROM LABORATORY SAMPLE
UNE-EN 16192:2012	Characterization of waste - Analysis of eluates
S.R. CEN/TS 16660:2015	CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
UNE-CEN/TR 16110:2011 IN	Characterization of waste - Guidance on the use of ecotoxicity tests applied to waste
UNI EN 16192 : 2012	CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
DIN EN 15002 E : 2015	CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
13/30286655 DC : 0	BS EN 15863 - CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED TEST CONDITIONS
BS EN 15002:2015	Characterization of waste. Preparation of test portions from the laboratory sample
EN 13370:2003	Characterization of waste - Analysis of eluates - Determination of Ammonium, AOX, conductivity, Hg, phenol index, TOC, easily liberatable CN-, F-
CEN/TR 16110:2010	Characterization of waste - Guidance on the use of ecotoxicity tests applied to waste
CEN/TS 16660:2015	Characterization of waste - Leaching behaviour test - Determination of the reducing character and the reducing capacity
EN 16192:2011	Characterization of waste - Analysis of eluates

Standards Referencing This Book - (Show below) - (Hide below)

ENV 12920 : 1997	CHARACTERIZATION OF WASTE - METHODOLOGY FOR THE DETERMINATION OF THE LEACHING BEHAVIOUR OF WASTE UNDER SPECIFIED CONDITIONS
EN 12880:2000	Characterization of sludges - Determination of dry residue and water content
ENV 12506 : DRAFT 2000	CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, CD, CR (6), CU, NI, PB, ZN, CL[-], NO[2][-], SO[4][2-]
ISO 5667-3:2012	Water quality Sampling Part 3: Preservation and handling of water samples
DIN 38414 : LATEST
ENV 13370 : DRAFT 2001	CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF AMMONIUM - N, AOX, CONDUCTIVITY, HG, PHENOL INDEX, TOC, CN - EASILY LIBERATABLE, F
EN ISO 5667-3:2012	Water quality - Sampling - Part 3: Preservation and handling of water samples (ISO 5667-3:2012)
ISO 3696:1987	Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995	Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
NFX 31 210 : 1998
NEN 7343 : 1995	LEACHING CHARACTERISTICS OF SOLID EARTHY AND STONY BUILDING AND WASTE MATERIALS - LEACHING TESTS - DETERMINATION OF THE LEACHING OF INORGANIC COMPONENTS FROM GRANULAR MATERIALS WITH THE COLUMN TEST
ISO 5725-5:1998	Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method

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