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EN 14078:2014

Current

Current

The latest, up-to-date edition.

Liquid petroleum products - Determination of fatty acid methyl ester (FAME) content in middle distillates - Infrared spectrometry method

Published date

07-05-2014

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Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Apparatus
6 Sampling and sample handling
7 Procedure
8 Calculation
9 Expression of results
10 Precision
11 Test report
Annex A (informative) - Specific adjustments for calibration
        and dilution
Bibliography

This European Standard specifies a test method for the determination of Fatty Acid Methyl Ester (FAME) content in diesel fuel or domestic heating fuel by mid infrared spectrometry, which applies to FAME contents of the two measurement ranges as follows:- range A: for FAME contents ranging from approx. 0,05 % (V/V) to approx. 3 % (V/V);- range B: for FAME contents ranging from approx. 3 % (V/V) to approx. 20 % (V/V);- range C: for FAME contents ranging from approx. 20 % (V/V) to approx. 50 % (V/V).Principally, higher FAME contents can also be analyzed if diluted; however, no precision data for results outside the specified range is available at present.This test method was verified to be applicable to samples which contain FAME conforming to EN 14214 or EN 14213. Reliable quantitative results are obtained only if the samples do not contain any significant amounts of other interfering components, especially esters and other carbonyl compounds which possess absorption bands in the spectral region used for quantification of FAME. If such interfering components are present, this test method is expected to produce higher values.NOTE 1For the purposes of this European Standard, the term "% (V/V)" is used to represent the volume fraction () of a material.NOTE 2For conversion of grams FAME per litre (g FAME/l) to volume fraction, a fixed density for FAME of 883,0 kg/m³ is adopted.WARNING - The use of this European Standard may involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Committee
CEN/TC 19
DevelopmentNote
Supersedes PREN 14078. (05/2014)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current
Supersedes

BS EN 16734 : 2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
PD CEN/TR 16557:2013 Automotive fuels. High FAME diesel fuel blends (B11-B30). Background to the parameters required and their respective limits and determination
PD CEN/TR 16389:2017 Automotive fuels. Paraffinic diesel fuel and blends with FAME. Background to the parameters required and their respective limits and determination
S.R. CEN/TR 16557:2013 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL BLENDS (B11 - B30) - BACKGROUND TO THE PARAMETERS REQUIRED AND THEIR RESPECTIVE LIMITS AND DETERMINATION
S.R. CEN/TS 15940:2012 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
EN 16734:2016 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
BS EN 16709 : 2015 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
EN 15940:2016 Automotive fuels - Paraffinic diesel fuel from synthesis or hydrotreatment - Requirements and test methods
S.R. CEN/TR 16389:2017 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL AND BLENDS WITH FAME - BACKGROUND TO THE PARAMETERS REQUIRED AND THEIR RESPECTIVE LIMITS AND DETERMINATION
I.S. EN 16734:2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
14/30298209 DC : 0 BS EN 16734 - AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
ASTM D 7467 : 2017-03 SPECIFICATION FOR DIESEL FUEL OIL, BIODIESEL BLEND (B6 TO B20)
I.S. EN 16709:2015 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
DIN EN 15940:2016-09 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
DIN EN 590:2017-10 Automotive fuels - Diesel - Requirements and test methods (includes Amendment :2017)
PREN 590 : DRAFT 2011 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
14/30310326 DC : 0 BS EN 15940 - AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
UNE-EN 16734:2017 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
I.S. EN 15940:2016 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
CEN/TR 16557:2013 Automotive fuels - High FAME diesel fuel blends (B11 - B30) - Background to the parameters required and their respective limits and determination
DIN ISO 8217:2013-12 PETROLEUM PRODUCTS - FUELS (CLASS F) - SPECIFICATIONS OF MARINE FUELS (ISO 8217:2012)
EN 590:2013 Automotive fuels - Diesel - Requirements and test methods
11/30249539 DC : 0 BS EN 590 - AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
UNI CEN/TS 15940 : 2012 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
I.S. EN 590:2013+A1:2017&LC:2017 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
DIN EN 16709:2015-12 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
BS EN 590 : 2013 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
UNE-EN 15940:2016 Automotive fuels - Paraffinic diesel fuel from synthesis or hydrotreatment - Requirements and test methods
UNE-EN 16709:2016 Automotive fuels - High FAME diesel fuel (B20 and B30) - Requirements and test methods
UNE-EN 590:2014 Automotive fuels - Diesel - Requirements and test methods
CEN/TR 16389:2017 Automotive fuels - Paraffinic diesel fuel and blends with FAME - Background to the parameters required and their respective limits and determination
CEN/TS 15940:2012 Automotive fuels - Paraffinic diesel fuel from synthesis or hydrotreatment - Requirements and test methods

ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
ISO 3170:2004 Petroleum liquids — Manual sampling
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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