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  • EN 15192:2006

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    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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    Characterisation of waste and soil - Determination of Chromium(VI) in solid material by alkaline digestion and ion chromatography with spectrophotometric detection

    Available format(s): 

    Superseded date:  15-07-2021

    Language(s): 

    Published date:  15-11-2006

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and Definitions
    4 Safety remarks
    5 Principle
    6 Apparatus
    7 Reagents
    8 Sample pretreatment
    9 Alkaline digestion procedure
    10 Analytical procedure
    11 Calculation
    12 Expression of results
    13 Test report
    Annex A (informative) Alternative methods for direct
            determination of Cr(VI) in the alkaline digestion
            solution
    Annex B Ion chromatographic system
    Annex C (informative) Requirements for test portion
            preparation
    Annex D (informative) Background on methods for the
            determination of Cr(VI) in solid samples
       D.1 Summary of literature methods for Cr(VI)
            determinations in solids [6]
       D.2 Theoretical kinetic background for Cr(III)-Cr(VI)
            inter-conversions [6]
       D.3 Special needs for Cr(VI) determination in soil
            extracts [7]
       D.4 Determination of Cr(VI) in glass
       D.5 Determination of Cr(VI) in air particulate matter
    Annex E (informative) Validation
    Bibliography

    Abstract - (Show below) - (Hide below)

    This standard describes the determination of Cr(VI) in solid waste material and soil by alkaline digestion and ion chromatography with spectrophotometric detection. This method can be used to determine Cr(VI)-mass fractions in solids higher than 0,1 mg/kg.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 444
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Superseded
    Superseded By

    Standards Referenced By This Book - (Show below) - (Hide below)

    DIN EN 16318:2016-07 FERTILIZERS AND LIMING MATERIALS - DETERMINATION OF CHROMIUM(6) BY PHOTOMETRY (METHOD A) AND BY ION CHROMATOGRAPHY WITH SPECTROPHOTOMETRIC DETECTION (METHOD B)
    CEN/TS 16318:2012 Fertilizers - Determination of trace elements - Determination of chromium(VI) by photometry (method A) and by ion chromatography with spectrophotometric detection (method B)
    DIN EN 16318 E : 2016 FERTILIZERS AND LIMING MATERIALS - DETERMINATION OF CHROMIUM(6) BY PHOTOMETRY (METHOD A) AND BY ION CHROMATOGRAPHY WITH SPECTROPHOTOMETRIC DETECTION (METHOD B)
    UNI EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    I.S. EN 16457:2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    S.R. CEN/TS 16318:2012 FERTILIZERS - DETERMINATION OF TRACE ELEMENTS - DETERMINATION OF CHROMIUM(6) BY PHOTOMETRY (METHOD A) AND BY ION CHROMATOGRAPHY WITH SPECTROPHOTOMETRIC DETECTION (METHOD B)
    17/30348303 DC : 0 BS EN 17087 - CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE FOR TESTING OF RELEASE AND ANALYSIS OF CONTENT
    UNE-EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
    I.S. EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    13/30276853 DC : 0 BS EN 16318 - FERTILIZERS - DETERMINATION OF TRACE ELEMENTS - DETERMINATION OF CHROMIUM (6) BY PHOTOMETRY (METHOD A) AND BY ION CHROMATOGRAPHY WITH SPECTROPHOTOMETRIC DETECTION (METHOD B)
    UNE-EN 16457:2014 Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
    UNI CEN/TS 16318 : 2012 FERTILIZERS - DETERMINATION OF TRACE ELEMENTS - DETERMINATION OF CHROMIUM (6) BY PHOTOMETRY (METHOD A) AND BY ION CHROMATOGRAPHY WITH SPECTROPHOTOMETRIC DETECTION (METHOD B)
    12/30263896 DC : 0 BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    BS ISO 18512:2007 Soil quality. Guidance on long and short term storage of soil samples
    DIN ISO 18512:2009-03 SOIL QUALITY - GUIDANCE ON LONG AND SHORT TERM STORAGE OF SOIL SAMPLES
    DIN EN 16457:2014-07 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    I.S. EN 16318:2013 FERTILIZERS AND LIMING MATERIALS - DETERMINATION OF CHROMIUM(6) BY PHOTOMETRY (METHOD A) AND BY ION CHROMATOGRAPHY WITH SPECTROPHOTOMETRIC DETECTION (METHOD B)
    BS EN 16318 : 2013 FERTILIZERS AND LIMING MATERIALS - DETERMINATION OF CHROMIUM(6) BY PHOTOMETRY (METHOD A) AND BY ION CHROMATOGRAPHY WITH SPECTROPHOTOMETRIC DETECTION (METHOD B)
    ISO 18512:2007 Soil quality Guidance on long and short term storage of soil samples
    13/30291099 DC : 0 BS EN 15002 - CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    DIN EN 15002:2015-07 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
    EN 16457:2014 Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
    DIN EN 16457 E : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    PD CEN/TS 16318:2012 Fertilizers. Determination of trace elements. Determination of chromium(VI) by photometry (method A) and by ion chromatography with spectrophotometric detection (method B)
    BS EN 16457:2014 Characterization of waste. Framework for the preparation and application of a testing programme. Objectives, planning and report
    DIN EN 15002 E : 2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    BS EN 15002:2015 Characterization of waste. Preparation of test portions from the laboratory sample
    EN 16318:2013+A1:2016 Fertilizers and liming materials - Determination of chromium(VI) by photometry (method A) and by ion chromatography with spectrophotometric detection (method B)
    UNE-EN 16318:2015 Fertilizers - Determination of trace elements - Determination of chromium(VI) by photometry (method A) and by ion chromatography with spectrophotometric detection (method B)

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
    PREN 14346 : DRAFT 2004 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE AND WATER CONTENT
    EN ISO 11885:2009 Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (ISO 11885:2007)
    CEN/TR 14589:2003 Characterization of waste - State of the art document - Chromium VI specification in solid matrices
    ISO 11083:1994 Water quality — Determination of chromium(VI) — Spectrometric method using 1,5-diphenylcarbazide
    EN ISO 15586 : 2003 WATER QUALITY - DETERMINATION OF TRACE ELEMENTS USING ATOMIC ABSORPTION SPECTROMETRY WITH GRAPHITE FURNACE
    ISO 11464:2006 Soil quality Pretreatment of samples for physico-chemical analysis
    ISO 10304-3:1997 Water quality — Determination of dissolved anions by liquid chromatography of ions — Part 3: Determination of chromate, iodide, sulfite, thiocyanate and thiosulfate
    ISO 11885:2007 Water quality Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES)
    ISO 16740:2005 Workplace air Determination of hexavalent chromium in airborne particulate matter Method by ion chromatography and spectrophotometric measurement using diphenyl carbazide
    ISO 15586:2003 Water quality Determination of trace elements using atomic absorption spectrometry with graphite furnace
    ISO 5725:1986 Precision of test methods Determination of repeatability and reproducibility for a standard test method by inter-laboratory tests
    ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
    EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
    EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
    EN 12506:2003 Characterization of waste - Analysis of eluates - Determination of pH, As, Ba, Cd, Cl-, Co, Cr, Cr Vl, Cu, Mo, Ni, NO2-, Pb, total S, SO42-, V and Zn
    ISO 17294-2:2016 Water quality — Application of inductively coupled plasma mass spectrometry (ICP-MS) — Part 2: Determination of selected elements including uranium isotopes
    EN ISO 17294-2:2016 Water quality - Application of inductively coupled plasma mass spectrometry (ICP-MS) - Part 2: Determination of selected elements including uranium isotopes (ISO 17294-2:2016)
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