• EN 15751:2014

    Current The latest, up-to-date edition.

    Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidation stability by accelerated oxidation method

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    Published date:  26-03-2014

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Reagents and materials
    6 Apparatus
    7 Sampling
    8 Preparation of measurement
    9 Measurement
    10 Calculation and evaluation
    11 Expression of results
    12 Precision
    13 Test report
    Annex A (informative) - Background of the method
    Bibliography

    Abstract - (Show below) - (Hide below)

    This European Standard specifies a test method for the determination of the oxidation stability of fuels for diesel engines, by means of measuring the induction period of the fuel up to 48 h. The method is applicable to fatty acid methyl esters (FAME) intended for the use as pure biofuel or as a blending component for diesel fuels, and to blends of FAME with diesel fuel containing 2 % (V/V) of FAME at minimum.NOTE 1EN 14112 [1] describes a similar test method for oxidation stability determination of pure fatty acid methyl esters (see the Introduction to this European Standard).NOTE 2For induction periods higher than 48 h the precision is not covered by the precision statement of this method. The limit values of the relevant fuel standards are well within the scope of this test method.NOTE 3The presence of cetane improver can reduce the oxidation stability determined by this test method. Limited studies with EHN (2-ethyl hexyl nitrate) indicated, however, that the stability is reduced to an extent which is within the reproducibility of the test method.NOTE 4For the purposes of this European Standard, the term "% (V/V)" is used to represent the volume fraction (φ) of a material.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 19
    Development Note Supersedes PREN 15751. (04/2014)
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    14/30299493 DC : 0 BS EN 14112 - FAT AND OIL DERIVATIVES - FATTY ACID METHYL ESTERS (FAME) - DETERMINATION OF OXIDATION STABILITY (ACCELERATED OXIDATION TEST)
    DIN EN 15940 E : 2016 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
    14/30294041 DC : 0 BS EN 16709 - AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 OR B30) - REQUIREMENTS AND TEST METHODS
    PD CEN/TR 16557:2013 Automotive fuels. High FAME diesel fuel blends (B11-B30). Background to the parameters required and their respective limits and determination
    PD CEN/TR 16389:2017 Automotive fuels. Paraffinic diesel fuel and blends with FAME. Background to the parameters required and their respective limits and determination
    09/30205523 DC : 0 BS EN 14214 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
    11/30249539 DC : 0 BS EN 590 - AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
    13/30277078 DC : 0 BS EN 16568 - AUTOMOTIVE FUELS - FATTY ACID METHYL ESTER (FAME) FUEL AND BLENDS WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C
    S.R. CEN/TS 15940:2012 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
    I.S. EN 15940:2016 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
    EN 16709:2015/AC:2016 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
    EN 16734:2016 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
    BS EN 16709 : 2015 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
    EN 15940:2016 Automotive fuels - Paraffinic diesel fuel from synthesis or hydrotreatment - Requirements and test methods
    I.S. EN 16709:2015 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
    CEN/TR 16366:2012 Liquid petroleum products - Middle distillates and fatty acid methyl ester (FAME) fuels and blends - Round Robin report on applicability of Rapid Small Scale Oxidation Test method
    DIN EN 16568 E : 2015 AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C
    PD CEN/TR 16885:2015 Liquid petroleum products. Investigation on test method for measurement of the oxidation stability of diesel and diesel/FAME blends by Acid Number after ageing
    DIN EN 15940:2016-09 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
    UNE-EN 16734:2017 Automotive fuels - Automotive B10 diesel fuel - Requirements and test methods
    DIN EN 590:2017-10 Automotive fuels - Diesel - Requirements and test methods (includes Amendment :2017)
    S.R. CWA 16379:2011 FUELS AND BIOFUELS - PURE PLANT OIL FUEL FOR DIESEL ENGINE CONCEPTS - REQUIREMENTS AND TEST METHODS
    UNE-EN 16709:2016 Automotive fuels - High FAME diesel fuel (B20 and B30) - Requirements and test methods
    EN 14112:2016 Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of oxidation stability (accelerated oxidation test)
    I.S. EN 14112:2016 FAT AND OIL DERIVATIVES - FATTY ACID METHYL ESTERS (FAME) - DETERMINATION OF OXIDATION STABILITY (ACCELERATED OXIDATION TEST)
    14/30298209 DC : 0 BS EN 16734 - AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
    MIL-STD-3004 Revision D:2014 QUALITY ASSURANCE/SURVEILLANCE FOR FUELS, LUBRICANTS AND RELATED PRODUCTS
    PREN 590 : DRAFT 2011 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
    14/30310326 DC : 0 BS EN 15940 - AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
    CEN/TR 16885:2015 Liquid petroleum products - Investigation on test method for measurement of the oxidation stability of diesel and diesel/FAME blends by Acid Number after ageing
    I.S. EN 16734:2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
    S.R. CEN/TR 16885:2015 LIQUID PETROLEUM PRODUCTS - INVESTIGATION ON TEST METHOD FOR MEASUREMENT OF THE OXIDATION STABILITY OF DIESEL AND DIESEL/FAME BLENDS BY ACID NUMBER AFTER AGEING
    BS EN 590 : 2013 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
    DIN EN 16709 E : 2015 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
    CEN/TR 16557:2013 Automotive fuels - High FAME diesel fuel blends (B11 - B30) - Background to the parameters required and their respective limits and determination
    BS 2000-620(2014) : 2014 AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C
    PREN 14214 : DRAFT 2009 AUTOMOTIVE FUELS - FATTY ACID METHYL ESTERS (FAME) FOR DIESEL ENGINES - REQUIREMENTS AND TEST METHODS
    BS EN 16568:2014 Automotive fuels. Blends of Fatty acid methyl ester (FAME) with diesel fuel. Determination of oxidation stability by rapidly accelerated oxidation method at 120 °C
    S.R. CEN/TR 16389:2017 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL AND BLENDS WITH FAME - BACKGROUND TO THE PARAMETERS REQUIRED AND THEIR RESPECTIVE LIMITS AND DETERMINATION
    S.R. CEN/TR 16557:2013 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL BLENDS (B11 - B30) - BACKGROUND TO THE PARAMETERS REQUIRED AND THEIR RESPECTIVE LIMITS AND DETERMINATION
    DIN EN 16568:2015-03 AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C
    18/30369065 DC : DRAFT FEB 2018 BS EN 14214 AMD 2 - LIQUID PETROLEUM PRODUCTS - FATTY ACID METHYL ESTERS (FAME) FOR USE IN DIESEL ENGINES AND HEATING APPLICATIONS - REQUIREMENTS AND TEST METHODS
    EN 590:2013 Automotive fuels - Diesel - Requirements and test methods
    BS EN 14112:2003 Fat and oil derivatives. Fatty acid methyl esters (FAME). Determination of oxidation stability (accelerated oxidation test)
    EN 16568:2014 Automotive fuels - Blends of Fatty acid methyl ester (FAME) with diesel fuel - Determination of oxidation stability by rapidly accelerated oxidation method at 120 °C
    BS EN 16734 : 2016 AUTOMOTIVE FUELS - AUTOMOTIVE B10 DIESEL FUEL - REQUIREMENTS AND TEST METHODS
    I.S. EN 16568:2014 AUTOMOTIVE FUELS - BLENDS OF FATTY ACID METHYL ESTER (FAME) WITH DIESEL FUEL - DETERMINATION OF OXIDATION STABILITY BY RAPIDLY ACCELERATED OXIDATION METHOD AT 120 DEGREES C
    PREN 14112 : DRAFT 2014 FAT AND OIL DERIVATIVES - FATTY ACID METHYL ESTERS (FAME) - DETERMINATION OF OXIDATION STABILITY (ACCELERATED OXIDATION TEST)
    PD CEN/TR 16366:2012 Liquid petroleum products. Middle distillates and fatty acid methyl ester (FAME) fuels and blends. Round Robin report on applicability of Rapid Small Scale Oxidation Test method
    UNI CEN/TS 15940 : 2012 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS
    S.R. CEN/TR 16366:2012 LIQUID PETROLEUM PRODUCTS - MIDDLE DISTILLATES AND FATTY ACID METHYL ESTER (FAME) FUELS AND BLENDS - ROUND ROBIN REPORT ON APPLICABILITY OF RAPID SMALL SCALE OXIDATION TEST METHOD
    I.S. EN 590:2013+A1:2017&LC:2017 AUTOMOTIVE FUELS - DIESEL - REQUIREMENTS AND TEST METHODS
    DIN EN 16709:2015-12 AUTOMOTIVE FUELS - HIGH FAME DIESEL FUEL (B20 AND B30) - REQUIREMENTS AND TEST METHODS
    ASTM D 7467 : 2017-03 SPECIFICATION FOR DIESEL FUEL OIL, BIODIESEL BLEND (B6 TO B20)
    UNE-EN 15940:2016 Automotive fuels - Paraffinic diesel fuel from synthesis or hydrotreatment - Requirements and test methods
    UNE-EN 590:2014 Automotive fuels - Diesel - Requirements and test methods
    UNE-EN 14112:2017 Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of oxidation stability (accelerated oxidation test)
    CEN/TR 16389:2017 Automotive fuels - Paraffinic diesel fuel and blends with FAME - Background to the parameters required and their respective limits and determination
    CEN/TS 15940 : 2012 AUTOMOTIVE FUELS - PARAFFINIC DIESEL FUEL FROM SYNTHESIS OR HYDROTREATMENT - REQUIREMENTS AND TEST METHODS

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
    ISO 3170:2004 Petroleum liquids — Manual sampling
    ISO 6886:2016 Animal and vegetable fats and oils Determination of oxidative stability (accelerated oxidation test)
    EN 14112:2016 Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of oxidation stability (accelerated oxidation test)
    ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
    ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
    EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
    EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
    EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)
    EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)
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