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EN 15944:2010

Current

Current

The latest, up-to-date edition.

Liquid petroleum products - Determination of nickel and vanadium content - Inductively coupled plasma optical emission spectrometry method (ICP OES)

Published date

10-11-2010

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Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Sampling
7 Preparation of calibration solutions
8 Calibration
9 Sample analysis
10 Calculation
11 Expression of results
12 Precision
13 Test report
Bibliography

This European Standard specifies an inductively coupled plasma optical emission spectrometry (ICP OES) method for the determination of nickel content in the range 4 mg/kg to 55 mg/kg and of vanadium content in the range 4 mg/kg to 150 mg/kg in fuel oils and residual fuel oils.NOTE 1Nickel content can be determined from 2 mg/kg to 4 mg/kg and vanadium content can be determined from 1 mg/kg to 4 mg/kg. However, the precision was not established as no samples with nickel and vanadium contents in these ranges were included in the interlaboratory test. Nickel and vanadium contents higher than those reported can be determined after sample dilution. However, the precision was not established for diluted samples.NOTE 2For the purposes of this European Standard, the term "% (V/V)" is used to represent the volume fraction (phi).WARNING - The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.

Committee
CEN/TC 19
DevelopmentNote
Supersedes PREN 15944. (04/2011)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
UNI EN 15944 : 2011 Identical
BS EN 15944:2010 Identical
I.S. EN 15944:2010 Identical
NF EN 15944 : 2011 Identical
NEN EN 15944 : 2010 Identical
IP 587 : 2011 Identical
NBN EN 15944 : 2010 Identical
NS EN 15944 : 2010 Identical
UNE-EN 15944:2011 Identical
PN EN 15944 : SEP 2011 Identical
SN EN 15944:2011 Identical
BS 2000-587(2010) : 2010 Identical
DIN EN 15944:2011-02 Identical

ISO 3171:1988 Petroleum liquids — Automatic pipeline sampling
ISO 3170:2004 Petroleum liquids — Manual sampling
ISO 1042:1998 Laboratory glassware — One-mark volumetric flasks
EN ISO 1042:1999 Laboratory glassware - One-mark volumetric flasks (ISO 1042:1998)
DIN 51790-6:2007-11 TESTING OF LIQUID FUELS - DETERMINATION OF THE VANADIUM AND NICKEL CONTENT - PART 6: DIRECT DETERMINATION BY OPTICAL EMISSION SPECTRAL ANALYSIS WITH INDUCTIVELY COUPLED PLASMA (ICP OES)
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
EN 13131:2000 Liquid petroleum products - Determination of nickel and vanadium content - Atomic absorption spectrometric method
EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 3171:1999 Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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