• EN 15979:2011

    Current The latest, up-to-date edition.

    Testing of ceramic raw and basic materials - Direct determination of mass fractions of impurities in powders and granules of silicon carbide by OES by DC arc excitation

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    Published date:  26-01-2011

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Principle
    3 Spectrometry
    4 Apparatus
    5 Reagents
    6 Sampling and preparation of test samples
    7 Calibration
    8 Procedure
    9 Calculation
    10 Expression of results
    11 Precision
    12 Test report
    Annex A (informative) - Results of inter-laboratory study
    Annex B (informative) - Wavelength and working range
    Annex C (informative) - Possible interferences and their
            elimination
    Annex D (informative) - Information regarding the evaluation of
            the uncertainty of the mean value
    Annex E (informative) - Commercial certified reference materials
    Bibliography

    Abstract - (Show below) - (Hide below)

    This European Standard describes the method for the analysis of mass fractions of the impurities Al, B, Ca, Cr, Cu, Fe, Mg, Ni, Ti, V and Zr in powder and grain-shaped silicon carbide of ceramic raw and basic materials. This application can also be extended to other metallic elements and other similar non-metallic powder and grain-shaped materials such as carbides, nitrides, graphite, carbon blacks, cokes, carbon, as well as a number of further oxidic raw and basic materials after appropriate testing. NOTEThere are positive interferences for materials such as e.g. graphite, B4C, BN, WC and several refractory metal oxides.This testing procedure is applicable to mass fractions of the impurities mentioned above from approximately 1 mg/kg up to approximately 3 000 mg/kg, after verification. In some cases it may be possible to extend the range up to 5 000 mg/kg depending on element, wavelength, arc parameter, and sample weight.

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 187
    Development Note Supersedes PREN 15979. (08/2011)
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    UNI EN ISO 1927-3 : 2013 MONOLITHIC (UNSHAPED) REFRACTORY PRODUCTS - PART 3: CHARACTERIZATION AS RECEIVED
    BS EN ISO 1927-3:2012 Monolithic (unshaped) refractory products Characterization as received
    DIN EN ISO 1927-3:2013-03 MONOLITHIC (UNSHAPED) REFRACTORY MATERIALS - PART 3: CHARACTERIZATION AS RECEIVED (ISO 1927-3:2012)
    EN ISO 1927-3:2012 Monolithic (unshaped) refractory products - Part 3: Characterization as received (ISO 1927-3:2012)
    17/30327875 DC : DRAFT JAN 2017 BS ISO 16169 - PREPARATION OF SILICON CARBIDE AND SIMILAR MATERIALS FOR ANALYSIS BY ISO 12677 X-RAY FLUORESCENCE (XRF) - FUSED CAST-BEAD METHOD
    I.S. EN ISO 1927-3:2012 MONOLITHIC (UNSHAPED) REFRACTORY PRODUCTS - PART 3: CHARACTERIZATION AS RECEIVED (ISO 1927-3:2012)
    ISO 1927-3:2012 Monolithic (unshaped) refractory products — Part 3: Characterization as received

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 5022:1979 Shaped refractory products Sampling and acceptance testing
    EN ISO 21068-1:2008 Chemical analysis of silicon-carbide-containing raw materials and refractory products - Part 1: General information and sample preparation (ISO 21068-1:2008)
    ISO 5725-4:1994 Accuracy (trueness and precision) of measurement methods and results Part 4: Basic methods for the determination of the trueness of a standard measurement method
    ISO 21068-1:2008 Chemical analysis of silicon-carbide-containing raw materials and refractory products Part 1: General information and sample preparation
    ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
    ISO 8656-1:1988 Refractory products Sampling of raw materials and unshaped products Part 1: Sampling scheme
    ISO/IEC Guide 98-3:2008 Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)
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