EN 16319:2013+A1:2015
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
Fertilizers and liming materials - Determination of cadmium, chromium, lead and nickel by inductively coupled plasma-atomic emission spectrometry (ICP-AES) after aqua regia dissolution
23-12-2015
30-06-2016
European foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Sampling and sample preparation
6 Reagents
7 Apparatus
8 Procedure
9 Calculation and expression of the results
10 Precision
11 Test report
Annex A (informative) - Results of the inter-laboratory test
Bibliography
This European Standard specifies a method for the determination of the content of cadmium, chromium, nickel and lead in fertilizers with inductively coupled plasma atomic emission spectrometry (ICP-AES) after extraction with aqua regia. Limits of quantification are dependent on the sample matrix as well as on the instrument, but can roughly be expected to be 0,3 mg/kg for Cd and 1 mg/kg for Cr, Ni and Pb.NOTEDue to significant interference from Cu, Fe and Mn, no valid results can be reported using this method for fertilizer matrices containing high concentrations (>/= 10 %) of these micro-nutrients.
| Committee |
CEN/TC 260
|
| DevelopmentNote |
Supersedes PREN 16319 & CEN/TS 16319. (10/2013) 2013 Edition Re-Issued in December 2015 & incorporates AMD 1 2015. (01/2016)
|
| DocumentType |
Standard
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Withdrawn
|
| Supersedes |
| Standards | Relationship |
| NS EN 16319 : 2013 + A1 2015 | Identical |
| BS EN 16319 : 2013 | Identical |
| NBN EN 16319 : 2013 + A1 2016 | Identical |
| PN EN 16319 : 2014 + A1 2016 | Identical |
| I.S. EN 16319:2013 | Identical |
| NEN EN 16319 : 2013 + A1 2016 | Identical |
| DIN EN 16319:2016-03 | Identical |
| NF EN 16319 : 2014 + A1 2016 | Identical |
| I.S. EN 16319:2013+A1:2015 | Identical |
| BS EN 16319:2013+A1:2015 | Equivalent |
| UNE-EN 16319:2015 | Identical |
| BS EN 16319:2013+A1:2015 | Identical |
| UNE-EN 16319:2015+A1:2016 | Identical |
| I.S. EN 16964:2018 | FERTILIZERS - EXTRACTION OF TOTAL MICRO-NUTRIENTS IN FERTILIZERS USING AQUA REGIA |
| EN 16964:2018 | Fertilizers - Extraction of total micro-nutrients in fertilizers using aqua regia |
| EN 16963:2018 | Fertilizers - Determination of boron, cobalt, copper, iron, manganese, molybdenum and zinc using ICP-AES |
| 14/30250835 DC : 0 | BS ISO 17318 - FERTILIZERS AND SOIL CONDITIONERS - DETERMINATION OF ARSENIC, CADMIUM, CHROMIUM, LEAD AND MERCURY CONTENTS |
| 16/30330776 DC : 0 | BS EN 16963 - FERTILIZERS - DETERMINATION OF BORON, COBALT, COPPER, IRON, MANGANESE, MOLYBDENUM AND ZINC USING ICP-AES |
| 16/30330779 DC : 0 | BS EN 16964 - FERTILIZERS - EXTRACTION OF TOTAL MICRO-NUTRIENTS IN FERTILIZERS AND REMOVAL OF ORGANIC COMPOUNDS FROM FERTILIZER EXTRACTS |
| I.S. EN 16963:2018 | FERTILIZERS - DETERMINATION OF BORON, COBALT, COPPER, IRON, MANGANESE, MOLYBDENUM AND ZINC USING ICP-AES |
| ISO 5725-1:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions |
| EN 1482-2:2007 | Fertilizers and liming materials - Sampling and sample preparation - Part 2: Sample preparation |
| EN 12944-3:2001 | Fertilizers and liming materials - Vocabulary - Part 3: Terms relating to liming materials |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
| EN 1482-1:2007 | Fertilizers and liming materials - Sampling and sample preparation - Part 1: Sampling |