EN 16852:2017
Current
The latest, up-to-date edition.
Foodstuffs - Determination of ethyl carbamate in stone fruit spirits, fruit marc spirits and other spirit drinks - GC-MS method
10-05-2017
European foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Procedure
7 Gas chromatography and mass spectrometry
(GC-MS)
8 Calculation
9 Precision
10 Test report
Annex A (informative) - Typical chromatograms
Annex B (informative) - Precision data
Bibliography
This European Standard specifies a gas chromatographic method using mass spectrometric detection for the determination of ethyl carbamate (EC) in stone fruit spirits, fruit marc spirits and other spirit drinks.The method has been validated in an interlaboratory study for stone fruit spirits and fruit liqueurs, at levels ranging from 0,253 mg/l to 1,11 mg/l. However, linearity of the instrument response was proven for the concentration ranges 0,10 mg/l to 4,0 mg/l (simplified method) and 0,025 mg/l to 3,0 mg/l (procedure including sample clean-up), respectively.
| Committee |
CEN/TC 275
|
| DevelopmentNote |
Supersedes PREN 16852. (05/2017)
|
| DocumentType |
Standard
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Current
|
| Standards | Relationship |
| DIN EN 16852:2017-07 | Identical |
| NS EN 16852 : 2017 | Identical |
| DIN EN 16852:2015-04 (Draft) | Identical |
| BS EN 16852:2017 | Identical |
| PN EN 16852 : 2017 | Identical |
| UNE-EN 16852:2017 | Identical |
| NEN EN 16852 : 2017 | Identical |
| UNI EN 16852 : 2017 | Identical |
| SN EN 16852:2017 | Identical |
| I.S. EN 16852:2017 | Identical |
| NF EN 16852 : 2017 | Identical |
| ISO/IEC 17025:2005 | General requirements for the competence of testing and calibration laboratories |
| ISO 1042:1998 | Laboratory glassware — One-mark volumetric flasks |
| EN ISO 1042:1999 | Laboratory glassware - One-mark volumetric flasks (ISO 1042:1998) |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
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