EN 16877:2016
Current
The latest, up-to-date edition.
Animal feeding stuffs: Methods of sampling and analysis - Determination of T-2 and HT-2 toxins, Deoxynivalenol and Zearalenone, in feed materials and compound feed by LC-MS
30-11-2016
European foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Procedures
7 Measurements
8 Determination of mass fraction
9 Precision
10 Test report
Annex A (informative) - Precision data
Annex B (informative) - Examples
Annex C (informative) - Examples of chromatograms
according to the settings of the examples in Annex B
Bibliography
This method of analysis is applicable to the determination of HT-2 toxin (HT2) in the tested range of 22 µg/kg to 178 µg/kg, T-2 toxin (T2) in the tested range of 7 µg/kg to 50 µg/kg, Deoxynivalenol (DON) in the tested range of 88 µg/kg to 559 µg/kg, and Zearalenone (ZON) in the tested range of 14 µg/kg to 430 µg/kg in cereals and cereal-based compound animal feed. The actual working ranges may extend beyond the tested ranges. It is the responsibility of the laboratory to prove that the limit of quantitation (LOQ) for HT-2 and T-2 toxin is ≤ 10 µg/kg, for DON ≤ 100 µg/kg, and for ZON ≤ 20µg/kg.
Committee |
CEN/TC 327
|
DevelopmentNote |
Supersedes PREN 16877. (12/2016)
|
DocumentType |
Standard
|
PublisherName |
Comite Europeen de Normalisation
|
Status |
Current
|
Standards | Relationship |
DIN EN 16877:2017-03 | Identical |
NF EN 16877 : 2016 | Identical |
NS EN 16877 : 2016 | Identical |
PN EN 16877 : 2017 | Identical |
SN EN 16877:2017 | Identical |
I.S. EN 16877:2016 | Identical |
UNI EN 16877 : 2017 | Identical |
UNE-EN 16877:2017 | Identical |
DIN EN 16877:2015-07 (Draft) | Identical |
BS EN 16877:2016 | Identical |
NEN EN 16877 : 2016 | Identical |
EN ISO 6498:2012 | Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012) |
ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
ISO 6498:2012 | Animal feeding stuffs — Guidelines for sample preparation |
ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
ISO 5725-5:1998 | Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method |
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