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EN 17053:2018
Current
The latest, up-to-date edition.
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Animal feeding stuffs: Methods of sampling and analysis - Determination of trace elements, heavy metals and other elements in feed by ICP-MS (multi-method)
24-01-2018
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Sampling
7 Preparation and preservation of test samples
8 Procedure
9 Calculation
10 Precision
11 Test report
Annex A (informative) - Statistical results of interlaboratory
tests (listed by element)
Annex B (informative) - Interferences
Bibliography
This European Standard specifies a method for the determination of trace elements, heavy metals and other elements in animal feed by inductively coupled plasma mass spectrometry (ICP-MS). The method is used to determine As, Cd, Co, Cu, Fe, Hg, Mn, Mo, Pb, Se, Tl, U and Zn in the extraction solution after pressurized digestion. For the determination of extractable lead in minerals and feeds containing phyllosilicates (e.g. kaolinite clay) wet digestion with nitric acid should be used. The method described is suitable for use in quadrupole instruments equipped either with or without additional technology to reduce molecular ion interferences (e.g. collision or reaction technologies) as well as in high-resolution sector-field systems.The method was fully statistically tested and evaluated in a collaborative trial comprising eight animal feeding stuff samples for the elements As, Cd, Co, Cu, Fe, Hg, Mn, Mo, Pb, Se, Tl, U and Zn. For elements with a HORRAT value higher than 2 (e.g. mercury, see Annex A) the method is more applicable as a screening method and not for confirmatory purposes. High-resolution sector-field ICP-MS was not tested in the validation ring trial.The limit of quantification for each element is dependent on the sample matrix as well as the instrument. For the elements Co, Mn, Mo, Pb, Tl, U a limit of quantification of 0,10 mg/kg should normally be obtained, for the elements Fe and Zn 5,0 mg/kg, while for Cd 0,03 mg/kg, Hg 0,04 mg/kg and As 0,05 mg/kg should normally be quantifiable.Details on the successfully tested working range for each element are described in this standard.
Committee |
CEN/TC 327
|
DocumentType |
Standard
|
PublisherName |
Comite Europeen de Normalisation
|
Status |
Current
|
Standards | Relationship |
NF EN 17053 : 2018 | Identical |
DIN EN 17053:2018-03 | Identical |
NS EN 17053 : 2018 | Identical |
SS-EN 17053:2018 | Identical |
DIN EN 17053 E : 2018 | Identical |
NEN EN 17053 : 2018 | Identical |
ONORM EN 17053 : 2018 | Identical |
UNE-EN 17053:2018 | Identical |
UNI EN 17053:2018 | Identical |
PN-EN 17053:2018-03 | Identical |
I.S. EN 17053:2018 | Identical |
SN EN 17053:2018 | Identical |
BS EN 17053:2018 | Identical |
EN ISO 6498:2012 | Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012) |
EN ISO 6497:2005 | Animal feeding stuffs - Sampling (ISO 6497:2002) |
EN ISO 3696:1995 | Water for analytical laboratory use - Specification and test methods (ISO 3696:1987) |
ISO 5725-5:1998 | Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method |
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