• EN ISO 14577-1:2015

    Current The latest, up-to-date edition.

    Metallic materials - Instrumented indentation test for hardness and materials parameters - Part 1: Test method (ISO 14577-1:2015)

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    Language(s): 

    Published date:  29-07-2015

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Symbols and designations
    4 Principle
    5 Testing machine
    6 Test piece
    7 Procedure
    8 Uncertainty of the results
    9 Test report
    Annex A (normative) - Materials parameters determined
            from the force/indentation depth data set
    Annex B (informative) - Types of control use for the
            indentation process
    Annex C (normative) - Machine compliance and indenter
            area function
    Annex D (informative) - Notes on diamond indenters
    Annex E (normative) - Influence of the test piece surface
            roughness on the accuracy of the results
    Annex F (informative) - Correlation of indentation hardness
            H[IT] to Vickers hardness
    Annex G (normative) - Drift and creep rate determination
    Annex H (informative) - Estimation of uncertainty of the
            calculated values of hardness and materials parameters
    Annex I (normative) - Calculation of radial displacement
            Correction
    Bibliography

    Abstract - (Show below) - (Hide below)

    ISO 14577-1:2015 specifies the method of instrumented indentation test for determination of hardness and other materials parameters for the following three ranges: macro range: 2 N ≤ F ≤ 30 kN; micro range: 2 N > F; h > 0,2 µm; and nano range: h ≤ 0,2 µm.For the nano range, the mechanical deformation strongly depends on the real shape of indenter tip and the calculated material parameters are significantly influenced by the contact area function of the indenter used in the testing machine. Therefore, careful calibration of both instrument and indenter shape is required in order to achieve an acceptable reproducibility of the materials parameters determined with different machines.The macro and micro ranges are distinguished by the test forces in relation to the indentation depth.Attention is drawn to the fact that the micro range has an upper limit given by the test force (2 N) and a lower limit given by the indentation depth of 0,2 µm.The determination of hardness and other material parameters is given in Annex A.At high contact pressures, damage to the indenter is possible. For this reason in the macro range, hardmetal indenters are often used. For test pieces with very high hardness and modulus of elasticity, permanent indenter deformation can occur and can be detected using suitable reference materials. It is necessary that its influence on the test result be taken into account.This test method can also be applied to thin metallic and non-metallic coatings and non-metallic materials. In this case, it is recommended that the specifications in the relevant standards be taken into account (see also 6.3 and ISO 14577‑4).

    General Product Information - (Show below) - (Hide below)

    Committee CEN/TC 459/SC 1
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    PD CEN/TS 17010:2016 Nanotechnologies. Guidance on measurands for characterising nano-objects and materials that contain them
    CEN/TS 17010:2016 Nanotechnologies - Guidance on measurands for characterising nano-objects and materials that contain them
    S.R. CEN/TS 17010:2016 NANOTECHNOLOGIES - GUIDANCE ON MEASURANDS FOR CHARACTERISING NANO-OBJECTS AND MATERIALS THAT CONTAIN THEM
    VDI 3822 Blatt 2.1.8:2012-01 Failure analysis - Defects of thermoplastic products made of plastics caused by weather-induced stress
    VDI 2083 Blatt 18:2012-01 Cleanroom technology - Biocontamination control
    VDI/VDE 2616 Blatt 2:2014-07 Hardness testing of plastics and elastomers

    Standards Referencing This Book - (Show below) - (Hide below)

    ISO 4287:1997 Geometrical Product Specifications (GPS) — Surface texture: Profile method — Terms, definitions and surface texture parameters
    ISO 14577-4:2016 Metallic materials Instrumented indentation test for hardness and materials parameters Part 4: Test method for metallic and non-metallic coatings
    ISO 14577-3:2015 Metallic materials Instrumented indentation test for hardness and materials parameters Part 3: Calibration of reference blocks
    ISO 14577-2:2015 Metallic materials Instrumented indentation test for hardness and materials parameters Part 2: Verification and calibration of testing machines
    ISO/IEC Guide 98-3:2008 Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)
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