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EN ISO 18857-1:2006

Current

Current

The latest, up-to-date edition.

Water quality - Determination of selected alkylphenols - Part 1: Method for non-filtered samples using liquid-liquid extraction and gas chromatography with mass selective detection (ISO 18857-1:2005)

Published date

23-08-2006

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Foreword
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents
6 Apparatus
7 Sampling and sample pretreatment
8 Procedure
9 Calibration
10 Calculation
11 Expression of results
12 Test report
Annex A (informative) Suitable capillary columns
Annex B (informative) Examples of chromatograms
Annex C (informative) Recovery tests - 4-nonylphenol
                      (mixture of isomers)
Annex D (informative) Example of a separator
Annex E (informative) Method performance data
Bibliography

ISO 18857-1:2005 specifies a method for the determination of 4-nonylphenol (mixture of isomers) and 4-(1,1,3,3-tetramethylbutyl)phenol in non-filtered samples of drinking water, ground water and surface water. The method is applicable in a concentration range from 0,005 micrograms per litre to 0,2 micrograms per litre for 4-(1,1,3,3-tetramethylbutyl)phenol and from 0,02 micrograms per litre to 0,2 micrograms per litre for 4-nonylphenol (mixture of isomers). Depending on the matrix, the method is also applicable to waste water containing the analyzed compounds in the concentration range from 0,1 micrograms per litre to 50 micrograms per litre. Higher concentrations can be measured after appropriate dilution of the sample.

Committee
CEN/TC 230
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

S.R. CEN/TS 16182:2012 SLUDGE TREATED BIOWASTE AND SOIL - DETERMINATION OF NONYLPHENOLS (NP) AND NONYLPHENOL-MONO- AND DIETHOXYLATES USING GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GCMS)
UNI CEN/TS 16182 : 2012 SLUDGE TREATED BIOWASTE AND SOIL - DETERMINATION OF NONYLPHENOLS (NP) AND NONYLPHENOL-MONO- AND DIETHOXYLATES USING GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GCMS)
CEN/TS 16182:2012 Sludge treated biowaste and soil - Determination of nonylphenols (NP) and nonylphenol-mono- and diethoxylates using gas chromatography with mass selective detection (GC-MS)

ISO 5667-2:1991 Water quality Sampling Part 2: Guidance on sampling techniques
ISO 5667-3:2012 Water quality Sampling Part 3: Preservation and handling of water samples
ISO 5667-1:2006 Water quality Sampling Part 1: Guidance on the design of sampling programmes and sampling techniques
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
ISO 8466-1:1990 Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function

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