EN ISO 22032:2009
Current
The latest, up-to-date edition.
Water quality - Determination of selected polybrominated diphenyl ethers in sediment and sewage sludge - Method using extraction and gas chromatography/mass spectrometry (ISO 22032:2006)
25-02-2009
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences
5 Reagents and standards
6 Apparatus
7 Sampling and sample pre-treatment
8 Procedure
9 Calibration
10 Test report
Annex A (informative) - Clean-up procedures
Annex B (informative) - Examples for separation conditions
in gas chromatography and mass spectrometry
Annex C (informative) - Typical ions and time windows for
electron impact ionization detection
Annex D (informative) - Examples of chromatograms and spectra
Annex E (informative) - Precision data
Bibliography
ISO 22032:2006 specifies a method for the determination of selected polybrominated diphenyl ethers (PBDE) in sediment and sludge using gas chromatography/mass spectrometry (GC-MS) in the electron impact (EI) or negative ion chemical ionization (NCI) mode. When using GC-EI-MS, the method is applicable to samples containing 0,05 to 25 micrograms per kilogram of tetra- to octabromo congeners and 0,3 to 100 micrograms per kilogram of decabromo diphenyl ether (BDE-209), respectively.
| Committee |
CEN/TC 230
|
| DocumentType |
Standard
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Current
|
| Standards | Relationship |
| NEN EN ISO 22032 : 2009 | Identical |
| I.S. EN ISO 22032:2009 | Identical |
| SS-EN ISO 22032:2009 | Identical |
| BS EN ISO 22032:2009 | Identical |
| PN EN ISO 22032 : 2009 | Identical |
| UNE-EN ISO 22032:2009 | Identical |
| UNI EN ISO 22032 : 2009 | Identical |
| NBN EN ISO 22032 : 2009 | Identical |
| SN EN ISO 22032:2009 | Identical |
| DIN EN ISO 22032:2009-07 | Identical |
| NS EN ISO 22032 : 2009 | Identical |
| ISO 22032:2006 | Identical |
| NF EN ISO 22032 : 2009 | Identical |
| BS 6068-2.99(2006) : 2006 | Identical |
| DIN EN 16694:2015-12 | WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENLY ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) |
| UNE-EN 16694:2016 | Water quality - Determination of selected polybrominated diphenly ether (PBDE) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography - mass spectrometry (GC-MS) |
| CEN/TR 16417:2016 | Footwear - Footwear industry guideline for substances of very high concern (Annex XIV of REACH) |
| 13/30291096 DC : 0 | BS EN 16694 - WATER QUALITY - DETERMINATION OF PENTABROMODIPHENYL ETHER (PBDE) IN WHOLE WATER SAMPLES USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS) |
| UNE-EN 16377:2014 | Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste |
| S.R. CEN/TR 16417:2016 | FOOTWEAR - FOOTWEAR INDUSTRY GUIDELINE FOR SUBSTANCES OF VERY HIGH CONCERN (ANNEX 14 OF REACH) |
| BS EN 16377:2013 | Characterization of waste. Determination of brominated flame retardants (BFR) in solid waste |
| DIN EN 16377:2013-12 | Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste |
| PD CEN/TR 16417:2016 | Footwear. Footwear industry guideline for substances of very high concern (Annex XIV of REACH) |
| UNI EN 16377 : 2014 | CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE |
| EN 16694:2015 | Water quality - Determination of selected polybrominated diphenly ether (PBDE) in whole water samples - Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography - mass spectrometry (GC-MS) |
| EN 16377:2013 | Characterization of waste - Determination of brominated flame retardants (BFR) in solid waste |
| BS EN 16694:2015 | Water quality. Determination of selected polybrominated diphenly ether (PBDE) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography-mass spectrometry (GC-MS) |
| I.S. EN 16694:2015 | WATER QUALITY - DETERMINATION OF SELECTED POLYBROMINATED DIPHENYL ETHER (PBDE) IN WHOLE WATER SAMPLES - METHOD USING SOLID PHASE EXTRACTION (SPE) WITH SPE-DISKS COMBINED WITH GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS) |
| 12/30255723 DC : 0 | BS EN 16377 - CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE |
| I.S. EN 16377:2013 | CHARACTERIZATION OF WASTE - DETERMINATION OF BROMINATED FLAME RETARDANTS (BFR) IN SOLID WASTE |
| ISO 5667-13:2011 | Water quality Sampling Part 13: Guidance on sampling of sludges |
| ISO/TR 13530:1997 | Water quality Guide to analytical quality control for water analysis |
| EN 12880:2000 | Characterization of sludges - Determination of dry residue and water content |
| DIN 32645:2008-11 | CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| ISO 8466-1:1990 | Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function |
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