ENV 14029:2001
Withdrawn
A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.
Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation of the lead matrix
26-08-2022
18-07-2001
Foreword 000
1. Scope
2. Normative references
3. Principle
3.1 Preparation of the test solution
3.2 Instrumental techniques
4. Apparatus
4.1 General
4.2 Volumetric glassware
4.3 Filtration system
4.4 Instruments
5. Reagents
5.1 General
5.2 Nitric acid
5.3 Hydrochloric acid
5.4 Pure lead
5.5 Standard solutions
6. Sampling and sample preparation
7. Procedure
7.1 Preparation of the test solution
7.2 Preparation of the synthetic test solution
7.3 Preparation of the blank test solution
7.4 Preparation of calibration solutions
8. Determination of elements by FAAS 002
8.1 General
8.2 Calibration and measurement of the test solution
8.3 Expression of results
9. Determination of elements by ICP-ES
9.1 General
9.2 Calibration and measurement of the test solution
9.3 Expression of results
10. Test report
This European Prestandard specifies methods using flame atomic absorption spectrometry (FAAS) and inductively coupled plasma emission spectrometry (ICP-ES) for the determination of elements at low content in lead for the ranges given in Table 1.Higher contents than those listed in Table 1 should be determined according to ENV 13800.Table 1 - Ranges of application for the determination of elementsElementRanges of applications (% m/m)FAASICP-ESAg0,00001-0,0010,00001-0,001Al0,0001-0,0050,00005-0,005As0,0002-0,0050,00005-0,005Bi0,00005-0,00250,00005-0,0025Ca0,00005-0,0010,00001-0,001Cd0,00005-0,0010,00001-0,001Co0,00005-0,0010,00005-0,001Cr0,00005-0,0010,00005-0,001Cu0,00001-0,0010,00001-0,001Fe0,00005-0,0010,00005-0,001Mg0,00005-0,0010,00005-0,001Mn0,00005-0,0010,00005-0,001Na0,00005-0,0010,00001-0,001Ni0,00005-0,0010,00001-0,001Sb0,0002-0,00250,0002-0,0025Se0,0002-0,0050,0002-0,005Sn0,0005-0,0050,0002-0,005Te0,00002-0,00250,00002-0,0025TI0,00002-0,00250,00002-0,0025Zn0,00001-0,0010,00001-0,001These methods are intended as the definitive methods in case of dispute for the determination of elements at low content in lead. They are also recommended for the analysis of Certified Reference Materials (CRM) and Reference Materials (RM) which are used in analysis according to ENV 12908.
| Committee |
CEN/TC 306
|
| DocumentType |
Standard Recommendation
|
| PublisherName |
Comite Europeen de Normalisation
|
| Status |
Withdrawn
|
| Standards | Relationship |
| I.S. ENV 14029:2001 | Identical |
| UNI ENV 14029 : 2002 | Identical |
| DIN V ENV 14029:2001-12 | Identical |
| NEN NVN ENV 14029 : 2001 | Identical |
| XP ENV 14029 : 2001 XP | Identical |
| NBN ENV 14029 : 2001 | Identical |
| DD ENV 14029:2001 | Identical |
| ENV 14138:2001 | Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation by co-precipitation |
| DD ENV 14138:2001 | Lead and lead alloys. Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emissions spectrometry (ICP-ES), after separation by co-precipitation |
| I.S. ENV 14138:2002 | LEAD AND LEAD ALLOYS - ANALYSIS BY FLAME ATOMIC ABSORPTION SPECTROMETRY (FAAS) OR INDUCTIVELY COUPLED PLASMA EMISSION SPECTROMETRY (ICP-ES), AFTER SEPARATION BY CO-PRECIPITATION |
| EN 12402:1999 | Lead and lead alloys - Methods of sampling for analysis |
| ISO 1042:1998 | Laboratory glassware — One-mark volumetric flasks |
| ISO 648:2008 | Laboratory glassware — Single-volume pipettes |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| ENV 13800:2000 | Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), without separation of the lead matrix |
| ENV 12908:1997 | Lead and lead alloys - Analysis by Optical Emission Spectrometry (OES) with spark excitation |
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