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CEN
ENV 14029:2001

ENV 14029:2001

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation of the lead matrix

Withdrawn date

26-08-2022

Published date

18-07-2001

Publisher

Comite Europeen de Normalisation

Foreword 000
1. Scope
2. Normative references
3. Principle
    3.1 Preparation of the test solution
    3.2 Instrumental techniques
4. Apparatus
   4.1 General
    4.2 Volumetric glassware
    4.3 Filtration system
    4.4 Instruments
5. Reagents
    5.1 General
    5.2 Nitric acid
    5.3 Hydrochloric acid
    5.4 Pure lead
    5.5 Standard solutions
6. Sampling and sample preparation
7. Procedure
    7.1 Preparation of the test solution
    7.2 Preparation of the synthetic test solution
    7.3 Preparation of the blank test solution
    7.4 Preparation of calibration solutions
8. Determination of elements by FAAS 002
    8.1 General
    8.2 Calibration and measurement of the test solution
    8.3 Expression of results
9. Determination of elements by ICP-ES
    9.1 General
    9.2 Calibration and measurement of the test solution
    9.3 Expression of results
10. Test report

This European Prestandard specifies methods using flame atomic absorption spectrometry (FAAS) and inductively coupled plasma emission spectrometry (ICP-ES) for the determination of elements at low content in lead for the ranges given in Table 1.Higher contents than those listed in Table 1 should be determined according to ENV 13800.Table 1 - Ranges of application for the determination of elementsElementRanges of applications (% m/m)FAASICP-ESAg0,00001-0,0010,00001-0,001Al0,0001-0,0050,00005-0,005As0,0002-0,0050,00005-0,005Bi0,00005-0,00250,00005-0,0025Ca0,00005-0,0010,00001-0,001Cd0,00005-0,0010,00001-0,001Co0,00005-0,0010,00005-0,001Cr0,00005-0,0010,00005-0,001Cu0,00001-0,0010,00001-0,001Fe0,00005-0,0010,00005-0,001Mg0,00005-0,0010,00005-0,001Mn0,00005-0,0010,00005-0,001Na0,00005-0,0010,00001-0,001Ni0,00005-0,0010,00001-0,001Sb0,0002-0,00250,0002-0,0025Se0,0002-0,0050,0002-0,005Sn0,0005-0,0050,0002-0,005Te0,00002-0,00250,00002-0,0025TI0,00002-0,00250,00002-0,0025Zn0,00001-0,0010,00001-0,001These methods are intended as the definitive methods in case of dispute for the determination of elements at low content in lead. They are also recommended for the analysis of Certified Reference Materials (CRM) and Reference Materials (RM) which are used in analysis according to ENV 12908.

Committee
CEN/TC 306
DocumentType
Standard Recommendation
PublisherName
Comite Europeen de Normalisation
Status
Withdrawn

Standards Relationship
I.S. ENV 14029:2001 Identical
UNI ENV 14029 : 2002 Identical
DIN V ENV 14029:2001-12 Identical
NEN NVN ENV 14029 : 2001 Identical
XP ENV 14029 : 2001 XP Identical
NBN ENV 14029 : 2001 Identical
DD ENV 14029:2001 Identical

ENV 14138:2001 Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation by co-precipitation
DD ENV 14138:2001 Lead and lead alloys. Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emissions spectrometry (ICP-ES), after separation by co-precipitation
I.S. ENV 14138:2002 LEAD AND LEAD ALLOYS - ANALYSIS BY FLAME ATOMIC ABSORPTION SPECTROMETRY (FAAS) OR INDUCTIVELY COUPLED PLASMA EMISSION SPECTROMETRY (ICP-ES), AFTER SEPARATION BY CO-PRECIPITATION

EN 12402 : 1999 LEAD AND LEAD ALLOYS - METHODS OF SAMPLING FOR ANALYSIS
ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
ISO 648:2008 Laboratory glassware — Single-volume pipettes
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
ENV 13800:2000 Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), without separation of the lead matrix
ENV 12908:1997 Lead and lead alloys - Analysis by Optical Emission Spectrometry (OES) with spark excitation

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