I.S. EN 13130-4:2004
Current
The latest, up-to-date edition.
MATERIALS AND ARTICLES IN CONTACT WITH FOODSTUFFS - PLASTICS SUBSTANCES SUBJECT TO LIMITATION - PART 4: DETERMINATION OF 1,3-BUTADIENE IN PLASTICS
Hardcopy , PDF
English
01-01-2004
For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.
Only cited Standards give presumption of conformance to New Approach Directives/Regulations.
Dates of withdrawal of national standards are available from NSAI.
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Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Samples
6.1 General
6.2 Sample preparation for gas chromatography
6.2.1 Test samples
6.2.2 Calibration samples for the standard addition method
6.2.3 Bank samples
7 Procedure
7.1 GC preparation
7.2 Performance of GC measurements
8 Expression of results
8.1 Method of calculation
8.1.1 GC interferences
8.1.2 Determination of the 1,3-butadiene concentration
in the polymer
8.2 Repeatability and reproducibility
8.2.1 Validation
8.2.2 Repeatability and reproducibility
8.2.3 Detection of limit
9 Confirmation
9.1 Requirements for confirmation
9.2 Confirmation by combined gas chromatography/mass spectrometry
10 Test report
Annex A (normative) Calibration via external standardization
A.1 General
A.2 Construction of the calibration graph
A.3 Graphical determination
A.4 Calculation from the regression parameters
Annex B (normative) Manual sample injection
Bibliography
Describes a method for the determination of butadiene monomer in polymers.
| DevelopmentNote |
Supersedes I.S. ENV 13130-4. (02/2006)
|
| DocumentType |
Standard
|
| Pages |
19
|
| PublisherName |
National Standards Authority of Ireland
|
| Status |
Current
|
| Supersedes |
| Standards | Relationship |
| NEN EN 13130-4 : 2004 | Identical |
| UNI EN 13130-4 : 2005 | Identical |
| NF EN 13130-4 : 2004 | Identical |
| BS EN 13130-4:2004 | Identical |
| SN EN 13130-4 : 2004 | Identical |
| UNE-EN 13130-4:2005 | Identical |
| NS EN 13130-4 : 1ED 2004 | Identical |
| NBN EN 13130-4 : 2004 | Identical |
| DIN EN 13130-4:2004-08 | Identical |
| EN 13130-4:2004 | Identical |
| DIN 32645:2008-11 | CHEMICAL ANALYSIS - DECISION LIMIT, DETECTION LIMIT AND DETERMINATION LIMIT UNDER REPEATABILITY CONDITIONS - TERMS, METHODS, EVALUATION |
| EN 13130-1:2004 | Materials and articles in contact with foodstuffs - Plastics substances subject to limitation - Part 1: Guide to test methods for the specific migration of substances from plastics to foods and food simulants and the determination of substances in plastics and the selection of conditions of exposure to food simulants |
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