I.S. EN 13130-5:2004
Current
The latest, up-to-date edition.
MATERIALS AND ARTICLES IN CONTACT WITH FOODSTUFFS - PLASTICS SUBSTANCES SUBJECT TO LIMITATION - PART 5: DETERMINATION OF VINYLIDENE CHLORIDE IN FOOD SIMULANTS
Hardcopy , PDF
English
01-01-2004
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Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
4.1 Analyte and internal standard
4.1.1 Analyte
4.1.2 Internal standard
4.2 Chemicals
4.3 Solutions of standards and internal standard
4.3.1 Preparation of stock solutions of vinylidene
chloride
4.3.2 Intermediate solutions of vinylidene chloride
4.3.3 Internal standard stock solution
4.3.4 Intermediate internal standard solution
5 Apparatus
6 Samples
6.1 Laboratory samples
6.2 Preparation of test samples
6.2.1 General
6.2.2 Aqueous food simulants
6.2.3 Fatty food simulant
6.3 Preparation of blank samples
6.4 Preparation of calibration samples
7 Procedure
8 Expression of results
8.1 Method of calculation
8.1.1 GC interferences
8.1.2 Graphical determination using internal standard
8.1.3 Graphical determination via external standardization
8.1.4 Calculation of the concentration using a response
factor
8.1.5 Calculation of the specific migration
8.2 Precision
8.2.1 Validation
8.2.2 Repeatability and reproducibility
8.2.3 Detection limit
9 Confirmation
9.1 Requirement for confirmation
9.2 Confirmation by combined gas chromatography-mass
spectrometry
9.3 Confirmation by analysis on a GC column of different
polarity
10 Test report
Annex A (normative) Method of standard addition
Annex B (normative) Manual sample injection
Bibliography
Describes a method for the determination of vinylidene chloride monomer in food simulants.
| DevelopmentNote |
Supersedes I.S. ENV 13130-5. (02/2006)
|
| DocumentType |
Standard
|
| Pages |
20
|
| PublisherName |
National Standards Authority of Ireland
|
| Status |
Current
|
| Supersedes |
| Standards | Relationship |
| UNE-EN 13130-5:2005 | Identical |
| NS EN 13130-5 : 1ED 2004 | Identical |
| NBN EN 13130-5 : 2004 | Identical |
| BS EN 13130-5:2004 | Identical |
| EN 13130-5:2004 | Identical |
| SN EN 13130-5 : 2004 | Identical |
| DIN EN 13130-5:2004-08 | Identical |
| NEN EN 13130-5 : 2004 | Identical |
| NF EN 13130-5 : 2004 | Identical |
| UNI EN 13130-5 : 2005 | Identical |
| ISO 5725-1:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| EN 13130-1:2004 | Materials and articles in contact with foodstuffs - Plastics substances subject to limitation - Part 1: Guide to test methods for the specific migration of substances from plastics to foods and food simulants and the determination of substances in plastics and the selection of conditions of exposure to food simulants |
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