I.S. EN 13130-6:2004
Current
The latest, up-to-date edition.
MATERIALS AND ARTICLES IN CONTACT WITH FOODSTUFFS - PLASTICS SUBSTANCES SUBJECT TO LIMITATION - PART 6: DETERMINATION OF VINYLIDENE CHLORIDE IN PLASTICS
Hardcopy , PDF
English
01-01-2004
For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.
Only cited Standards give presumption of conformance to New Approach Directives/Regulations.
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Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Samples
6.1 Sample storage
6.2 Test sample preparation
6.2.1 General
6.2.2 Preparation of dissolved test sample solutions and
standard addition solutions
6.2.3 Preparation of blank samples
6.2.4 Preparation of 'hot jar' test samples
7 Procedure
7.1 GC preparation
7.1.1 GC parameters
7.1.2 Electron capture detector optimization
7.1.3 Performance of GC measurements
7.2 Calibration
8 Expression of results
8.1 Method of calculation
8.1.1 GC interferences
8.1.2 Graphical determination using internal standard
8.1.3 Graphical determination via external standardization
8.1.4 Calculation of the concentration using a response
factor
8.2 Precision
8.2.1 Validation
8.2.2 Repeatability and reproducibility
8.2.3 Detection limit
9 Confirmation
9.1 Requirement for confirmation
9.2 Confirmation by combined gas chromatography-mass
spectrometry
9.3 Confirmation by analysis on a GC column of different
polarity
10 Test report
Annex A (normative) Manual sample injection
Bibliography
Specifies a method for the determination of vinylidene chloride (VdC) in plastics materials and articles.
| DevelopmentNote |
Supersedes I.S. ENV 13130-6. (02/2006)
|
| DocumentType |
Standard
|
| Pages |
18
|
| PublisherName |
National Standards Authority of Ireland
|
| Status |
Current
|
| Supersedes |
| Standards | Relationship |
| NBN EN 13130-6 : 2004 | Identical |
| NS EN 13130-6 : 1ED 2004 | Identical |
| UNE-EN 13130-6:2005 | Identical |
| NF EN 13130-6 : 2004 | Identical |
| NEN EN 13130-6 : 2004 | Identical |
| EN 13130-6:2004 | Identical |
| BS EN 13130-6:2004 | Identical |
| SN EN 13130-6 : 2004 | Identical |
| UNI EN 13130-6 : 2005 | Identical |
| DIN EN 13130-6:2004-08 | Identical |
| ISO 5725-1:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| EN 13130-1:2004 | Materials and articles in contact with foodstuffs - Plastics substances subject to limitation - Part 1: Guide to test methods for the specific migration of substances from plastics to foods and food simulants and the determination of substances in plastics and the selection of conditions of exposure to food simulants |
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