I.S. EN 15309:2007
Current
The latest, up-to-date edition.
CHARACTERIZATION OF WASTE AND SOIL - DETERMINATION OF ELEMENTAL COMPOSITION BY X-RAY FLUORESCENCE
Hardcopy , PDF
English
01-01-2007
For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.
Only cited Standards give presumption of conformance to New Approach Directives/Regulations.
Dates of withdrawal of national standards are available from NSAI.
Important note : Users cannot be edited or removed once added to your Multi user PDF.
Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Safety remarks
5 Principle
6 Apparatus
7 Reagents
8 Interferences and sources of error
9 Sample preparation
9.1 General
9.2 Drying and determination of dry mass
9.3 Preparation of pressed pellet
9.4 Preparation of fused beads
10 Procedure
10.1 Analytical measurement conditions
10.2 Calibration
10.3 Analysis of the samples
11 Quality control
11.1 Drift correction procedure
11.2 Blank test
11.3 Reference materials
12 Calculation of the result
13 Test report
Annex A (informative) Semi-quantitative screening analysis
of waste, sludge and soil samples
Annex B (informative) Examples for operational steps of the
sample preparation for soil and waste samples
Annex C (informative) Suggested analytical lines, crystals
and operating conditions
Annex D (informative) List of reference materials applicable
for XRF-analysis
Annex E (informative) Validation
Bibliography
Specifies the procedure for a quantitative determination of major and trace element concentrations in homogeneous solid waste, soil and soil-like material by energy dispersive X-ray fluorescence (EDXRF) spectrometry or wavelength dispersive X-ray fluorescence (WDXRF) spectrometry using a calibration with matrix-matched standards.
| DocumentType |
Standard
|
| Pages |
43
|
| PublisherName |
National Standards Authority of Ireland
|
| Status |
Current
|
| Standards | Relationship |
| EN 15309:2007 | Identical |
| ISO/IEC 17025:2005 | General requirements for the competence of testing and calibration laboratories |
| ISO Guide 32:1997 | Calibration in analytical chemistry and use of certified reference materials |
| DIN 51418-2:2015-03 | X-RAY SPECTROMETRY - X-RAY EMISSION AND X-RAY FLUORESCENCE ANALYSIS (XRF) - PART 2: DEFINITIONS AND BASIC PRINCIPLES FOR MEASUREMENTS, CALIBRATION AND EVALUATION OF RESULTS |
| ISO 12980:2000 | Carbonaceous materials used in the production of aluminium — Green coke and calcined coke for electrodes — Analysis using an X-ray fluorescence method |
| DIN 51418-1:2008-08 | X-RAY SPECTROMETRY - X-RAY EMISSION- AND X-RAY FLUORESCENCE ANALYSIS (XRF) - PART 1: DEFINITIONS AND BASIC PRINCIPLES |
| ISO 12677:2011 | Chemical analysis of refractory products by X-ray fluorescence (XRF) Fused cast-bead method |
| ISO 11464:2006 | Soil quality Pretreatment of samples for physico-chemical analysis |
| ISO Guide 33:2015 | Reference materials — Good practice in using reference materials |
| EN 14346:2006 | Characterization of waste - Calculation of dry matter by determination of dry residue or water content |
| CEN/TR 15018:2005 | Characterization of waste - Digestion of waste samples using alkali-fusion techniques |
| ISO 14869-2:2002 | Soil quality — Dissolution for the determination of total element content — Part 2: Dissolution by alkaline fusion |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| EN 15002:2015 | Characterization of waste - Preparation of test portions from the laboratory sample |
| EN 13656:2002 | Characterization of waste - Microwave assisted digestion with hydrofluoric (HF), nitric (HNO3) and hydrochloric (HCl) acid mixture for subsequent determination of elements |
| EN ISO 12677:2011 | Chemical analysis of refractory products by X-ray fluorescence (XRF) - Fused cast-bead method (ISO 12677:2011) |
| EN 13657:2002 | Characterization of waste - Digestion for subsequent determination of aqua regia soluble portion of elements |
| ISO 9516-1:2003 | Iron ores — Determination of various elements by X-ray fluorescence spectrometry — Part 1: Comprehensive procedure |
| ISO Guide 34:2009 | General requirements for the competence of reference material producers |
Access your standards online with a subscription
Features
-
Simple online access to standards, technical information and regulations.
-
Critical updates of standards and customisable alerts and notifications.
-
Multi-user online standards collection: secure, flexible and cost effective.