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I.S. EN 16277:2012

Current

Current

The latest, up-to-date edition.

ANIMAL FEEDING STUFFS - DETERMINATION OF MERCURY BY COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CVAAS) AFTER MICROWAVE PRESSURE DIGESTION (EXTRACTION WITH 65% NITRIC ACID AND 30% HYDROGEN PEROXIDE)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2012

For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.

Only cited Standards give presumption of conformance to New Approach Directives/Regulations.


Dates of withdrawal of national standards are available from NSAI.

Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus and equipment
6 Procedure
7 Calculation
8 Precision
9 Test report
Annex A (informative) - Results of the interlaboratory tests
Annex B (informative) - Flowchart - Determination of mercury
        by CVAAS after microwave digestion
Annex C (informative) - Alternative digestion procedure with
        the same extraction efficiency: Acid digestion with a
        mixture of 65% nitric acid and 70% perchloric acid
        (7:3 v/v) at atmospheric pressure
Annex D (informative) - Alternative digestion procedure with
        the same extraction efficiency: Acid digestion with a
        mixture of 65% nitric acid, 37% hydrochloric acid
        and 30% hydrogen peroxide under reflux
Bibliography

Provides a method for the determination of mercury in animal feeding stuffs by Cold-Vapour Atomic Absorption Spectrometry (CVAAS) after microwave pressure digestion.

DocumentType
Standard
Pages
20
PublisherName
National Standards Authority of Ireland
Status
Current

Standards Relationship
EN 16277 : 2012 Identical

EN 1483:2007 Water quality - Determination of mercury - Method using atomic absorption spectrometry
ISO 6497:2002 Animal feeding stuffs Sampling
EN 15550:2017 Animal feeding stuffs: Methods of sampling and analysis - Determination of cadmium and lead by graphite furnace atomic absorption spectrometry (GF-AAS) after pressure digestion
EN ISO 6498:2012 Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012)
EN 13806:2002 Foodstuffs - Determination of trace elements - Determination of mercury by cold-vapour atomic absorption spectrometry (CVAAS) after pressure digestion
EN 13804:2013 Foodstuffs - Determination of elements and their chemical species - General considerations and specific requirements
EN 13805:2014 Foodstuffs - Determination of trace elements - Pressure digestion
EN ISO 6497 : 2005 ANIMAL FEEDING STUFFS - SAMPLING
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 15621:2017 Animal feeding stuffs: Methods of sampling and analysis - Determination of calcium, sodium, phosphorus, magnesium, potassium, sulphur, iron, zinc, copper, manganese and cobalt after pressure digestion by ICP-AES

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