ISO 13859:2014
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The latest, up-to-date edition.
Soil quality — Determination of polycyclic aromatic hydrocarbons (PAH) by gas chromatography (GC) and high performance liquid chromatography (HPLC)
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03-02-2014
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ISO 13859:2014 specifies the quantitative determination of 16 PAH in sludge, soil, and treated biowaste using GC-MS and HPLC-UV-DAD/FLD covering a wide range of PAH contamination levels. When using fluorescence detection, acenaphthylene cannot be measured.
The limit of detection depends on the determinants, the equipment used, the quality of chemicals used for the extraction of the sample, and the clean-up of the extract. Typically, a lower limit of application of 0,01 mg/kg (expressed as dry matter) can be ensured for each individual PAH.
Sludge, soil, and treated biowaste can differ in properties and also in the expected contamination levels of PAH and presence of interfering substances. These differences make it impossible to describe one general procedure. ISO 13859:2014 contains decision tables based on the properties of the sample and the extraction and clean-up procedure to be used. Two general lines are followed, an agitation procedure (shaking) or use of Soxhlet/pressurized liquid extraction.
| Committee |
ISO/TC 190/SC 3
|
| DevelopmentNote |
Supersedes ISO/DIS 13859. (02/2014)
|
| DocumentType |
Standard
|
| Pages |
37
|
| PublisherName |
International Organization for Standardization
|
| Status |
Current
|
| Standards | Relationship |
| NEN ISO 13859 : 2014 | Identical |
| 15/30292347 DC : 0 | BS ISO 16751 - SOIL QUALITY - ENVIRONMENTAL AVAILABILITY OF NON-POLAR ORGANIC COMPOUNDS - DETERMINATION OF THE POTENTIAL BIOAVAILABLE FRACTION AND THE NON-BIOAVAILABLE FRACTION USING A STRONG ADSORBENT OR COMPLEXING AGENT |
| ISO/TS 16751:2018 | Soil quality Environmental availability of non-polar organic compounds Determination of the potential bioavailable fraction and the non-bioavailable fraction using a strong adsorbent or complexing agent |
| DIN 38414-23:2002-02 | GERMAN STANDARD METHODS FOR THE EXAMINATION OF WATER, WASTE WATER AND SLUDGE - SLUDGE AND SEDIMENTS (GROUP S) - PART 23: DETERMINATION OF 15 POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) AND FLUORESCENCE DETECTION (S 23) |
| ISO 22892:2006 | Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| ISO 18287:2006 | Soil quality Determination of polycyclic aromatic hydrocarbons (PAH) Gas chromatographic method with mass spectrometric detection (GC-MS) |
| EN 15308:2016 | Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by gas chromatography with electron capture or mass spectrometric detection |
| ISO 5667-15:2009 | Water quality — Sampling — Part 15: Guidance on the preservation and handling of sludge and sediment samples |
| ISO 17993:2002 | Water quality — Determination of 15 polycyclic aromatic hydrocarbons (PAH) in water by HPLC with fluorescence detection after liquid-liquid extraction |
| ISO 16720:2005 | Soil quality Pretreatment of samples by freeze-drying for subsequent analysis |
| ISO 28540:2011 | Water quality — Determination of 16 polycyclic aromatic hydrocarbons (PAH) in water — Method using gas chromatography with mass spectrometric detection (GC-MS) |
| ISO 14507:2003 | Soil quality Pretreatment of samples for determination of organic contaminants |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 8466-1:1990 | Water quality Calibration and evaluation of analytical methods and estimation of performance characteristics Part 1: Statistical evaluation of the linear calibration function |
| EN 15527:2008 | Characterization of waste - Determination of polycyclic aromatic hydrocarbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS) |
| ISO 18512:2007 | Soil quality Guidance on long and short term storage of soil samples |
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