ISO 22959:2009
Current
The latest, up-to-date edition.
Animal and vegetable fats and oils Determination of polycyclic aromatic hydrocarbons by on-line donor-acceptor complex chromatography and HPLC with fluorescence detection
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13-05-2009
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ISO 22959:2009 specifies a high performance liquid chromatographic (HPLC) procedure for the determination of polycyclic aromatic hydrocarbons (PAHs) in edible fats and oils.
The method has been validated for coconut, olive, sunflower, and soybean oil, and is possibly applicable to other oils, dependent on the determination of appropriate parameters.
The lowest level of quantification for the PAHs is 0,1 g/kg. The lowest possible amount of each PAH which can be distinguished from the baseline noise has not been determined. The validated concentration range of the method is 0,1 g/kg to 3,5 g/kg for each individual PAH. For samples containing (light) PAH contents > 3,5 g/kg, dilution to bring the contents into the validated range is possible. It is also possible to adjust the range of the calibration curves. However, ranges exceeding 3,5 g/kg have not been validated.
PAHs which can be determined by this method are: anthracene, phenanthrene, fluoranthene, pyrene, chrysene, benzo[a]anthracene, benzo[e]pyrene, benzo[a]pyrene, perylene, benzo[ghi]perylene, anthanthrene, dibenzo[a,h]anthracene, coronene, indeno[1,2,3-cd]pyrene, benzo[a]fluoranthene, benzo[b]fluoranthene, benzo[k]fluoranthene.
| DevelopmentNote |
Supersedes ISO/DIS 22959. (05/2009)
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| DocumentType |
Standard
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| Pages |
22
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| PublisherName |
International Organization for Standardization
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| Status |
Current
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| Standards | Relationship |
| NF EN ISO 22959 : 2009 | Identical |
| NBN EN ISO 22959 : 2009 | Identical |
| NEN EN ISO 22959 : 2009 | Identical |
| NS EN ISO 22959 : 2009 | Identical |
| I.S. EN ISO 22959:2009 | Identical |
| SN EN ISO 22959:2009 | Identical |
| UNI EN ISO 22959 : 2009 | Identical |
| BS EN ISO 22959:2009 | Identical |
| UNE-EN ISO 22959:2010 | Identical |
| EN ISO 22959:2009 | Identical |
| DIN EN ISO 22959:2009-10 | Identical |
| BS EN 16619:2015 | Food analysis. Determination of benzo[a]pyrene, benz[a]anthracene, chrysene and benzo[b]fluoranthene in foodstuffs by gas chromatography mass spectrometry (GC-MS) |
| PD CEN/TS 16621:2014 | Food analysis. Determination of benzo[a]pyrene, benz[a]anthracene, chrysene and benzo[b]fluoranthene in foodstuffs by high performance liquid chromatography with fluorescence detection (HPLC-FD) |
| CEN/TS 16621:2014 | Food analysis - Determination of benzo[a]pyrene, benz[a]anthracene, chrysene and benzo[b]fluoranthene in foodstuffs by high performance liquid chromatography with fluorescence detection (HPLC-FD) |
| I.S. EN 16619:2015 | FOOD ANALYSIS - DETERMINATION OF BENZO[A]PYRENE, BENZ[A]ANTHRACENE, CHRYSENE AND BENZO[B]FLUORANTHENE IN FOODSTUFFS BY GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS) |
| S.R. CEN/TS 16621:2014 | FOOD ANALYSIS - DETERMINATION OF BENZO[A]PYRENE, BENZ[A]ANTHRACENE, CHRYSENE AND BENZO[B]FLUORANTHENE IN FOODSTUFFS BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY WITH FLUORESCENCE DETECTION (HPLC-FD) |
| DIN EN 16619:2015-06 | FOOD ANALYSIS - DETERMINATION OF BENZO[A]PYRENE, BENZ[A]ANTHRACENE, CHRYSENE AND BENZO[B]FLUORANTHENE IN FOODSTUFFS BY GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS) |
| EN 16619:2015 | Food analysis - Determination of benzo[a]pyrene, benz[a]anthracene, chrysene and benzo[b]fluoranthene in foodstuffs by gas chromatography mass spectrometry (GC-MS) |
| UNE-EN 16619:2015 | Food analysis - Determination of benzo[a]pyrene, benz[a]anthracene, chrysene and benzo[b]fluoranthene in foodstuffs by gas chromatography mass spectrometry (GC-MS) |
| UNI CEN/TS 16621 : 2014 | Food analysis - Determination of benzo [a] pyrene, benzo [a] anthracene, chrysene and benzo [b] fluoranthene in food products by high resolution liquid chromatography with fluorescence detector (HPLC-FD) |
| ISO 5725-1:1994 | Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions |
| ISO 5555:2001 | Animal and vegetable fats and oils — Sampling |
| ISO 1042:1998 | Laboratory glassware — One-mark volumetric flasks |
| ISO 5725-2:1994 | Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method |
| ISO 661:2003 | Animal and vegetable fats and oils — Preparation of test sample |
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