ISO 23697-1:2023

This document specifies a method for the determination of total bound nitrogen(ST-TN_b) in water of various origins: groundwater, surface water, and wastewater, in a measuring range of concentration generally between 0,5mg/l and 220mg/l of ST-TN_b using the small-scale sealed tube method. Different measuring ranges of small-scale sealed tube methods can be required.

The measuring ranges can vary depending on the type of small-scale sealed tube method of different manufacturers. It is up to the user to choose the small-scale sealed tube with the appropriate application range or to adapt samples with concentrations exceeding the measuring range of a test by preliminary dilution.

NOTE The results of a small-scale sealed tube are most precise in the middle of the application range of the test.

All small-scale sealed tube methods are based on a heated alkaline potassium persulfate oxidation in a heating block. Different digestion temperatures, 100°C or 120°C or 170°C, and different digestion times are applicable. Dimethylphenol colour reactions are applied, depending on the typical operating procedure of the small-scale sealed tube used, see Clause9.