ISO/TS 17182:2014
Current
The latest, up-to-date edition.
Soil quality — Determination of some selected phenols and chlorophenols — Gas chromatographic method with mass spectrometric detection
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21-11-2014
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ISO/TS 17182:2014 describes the gas chromatographic determination of phenols, methyl phenols, di-methylphenols and tri-methylphenols (see Table 1) and selected chlorophenols (see Table 2) by using mass spectrometric detection in soil samples. This method can also be used for other solid samples, such as sediments and solid wastes. This International Standard describes an acidic liquid extraction of soil, followed by acetylation and then liquid/liquid extraction. Determination takes place by gas chromatography and mass spectrometric detection.
With this method, phenols and chlorophenols can be determined at the lowest of mass concentrations ranging from approximately 0,01 mg/kg to 0,1 mg/kg depending on the component sensitivity and the quantity of sample used. In some cases, complete separation of isomers cannot be achieved. Then the sum is reported.
NOTE With this method, other higher methylated phenols can also be analysed provided that the suitability and the validity of the method is proven.
| Committee |
ISO/TC 190/SC 3
|
| DocumentType |
Technical Specification
|
| Pages |
15
|
| PublisherName |
International Organization for Standardization
|
| Status |
Current
|
| Standards | Relationship |
| PD ISO/TS 17182:2014 | Identical |
| ISO 10381-1:2002 | Soil quality Sampling Part 1: Guidance on the design of sampling programmes |
| EN 12673:1998 | Water quality - Gas chromatographic determination of some selected chlorophenols in water |
| ISO 22892:2006 | Soil quality Guidelines for the identification of target compounds by gas chromatography and mass spectrometry |
| ISO 11709:2011 | Soil quality Determination of selected coal-tar-derived phenolic compounds using high performance liquid chromatography (HPLC) |
| ISO 14507:2003 | Soil quality Pretreatment of samples for determination of organic contaminants |
| ISO 3696:1987 | Water for analytical laboratory use — Specification and test methods |
| ISO 14154:2005 | Soil quality — Determination of some selected chlorophenols — Gas-chromatographic method with electron-capture detection |
| ISO 18512:2007 | Soil quality Guidance on long and short term storage of soil samples |
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