NEN EN 13130-6 : 2004
Current
The latest, up-to-date edition.
MATERIALS AND ARTICLES IN CONTACT WITH FOODSTUFFS - PLASTICS SUBSTANCES SUBJECT TO LIMITATION - PART 6: DETERMINATION OF VINYLIDENE CHLORIDE IN PLASTICS
12-01-2013
Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Samples
6.1 Sample storage
6.2 Test sample preparation
6.2.1 General
6.2.2 Preparation of dissolved test sample solutions and
standard addition solutions
6.2.3 Preparation of blank samples
6.2.4 Preparation of 'hot jar' test samples
7 Procedure
7.1 GC preparation
7.1.1 GC parameters
7.1.2 Electron capture detector optimization
7.1.3 Performance of GC measurements
7.2 Calibration
8 Expression of results
8.1 Method of calculation
8.1.1 GC interferences
8.1.2 Graphical determination using internal standard
8.1.3 Graphical determination via external standardization
8.1.4 Calculation of the concentration using a response
factor
8.2 Precision
8.2.1 Validation
8.2.2 Repeatability and reproducibility
8.2.3 Detection limit
9 Confirmation
9.1 Requirement for confirmation
9.2 Confirmation by combined gas chromatography-mass
spectrometry
9.3 Confirmation by analysis on a GC column of different
polarity
10 Test report
Annex A (normative) Manual sample injection
Bibliography
Specifies a method for the determination of vinylidene chloride (VdC) in plastics materials and articles.
DevelopmentNote |
Supersedes NEN NVN ENV 13130-6. (06/2004)
|
DocumentType |
Standard
|
PublisherName |
Netherlands Standards
|
Status |
Current
|
Supersedes |
Standards | Relationship |
DIN EN 13130-6:2004-08 | Identical |
I.S. EN 13130-6:2004 | Identical |
EN 13130-6:2004 | Identical |
BS EN 13130-6:2004 | Identical |
UNI EN 13130-6 : 2005 | Identical |
UNE-EN 13130-6:2005 | Identical |
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