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ONORM EN 13656 : 2002

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

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CHARACTERIZATION OF WASTE - MICROWAVE ASSISTED DIGESTION WITH HYDROFLUROIC (HF), NITRIC (HNO[3]) AND HYDROCHLORIC (HCI) ACID MIXTURE FOR SUBSEQUENT DETERMINATION OF ELEMENTS IN WASTE

Withdrawn date

15-05-2021

Published date

12-01-2013

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Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Safety remarks
5 Sample
   5.1 Sample pre-treatment
   5.2 Mass of test portion
6 Equipment
   6.1 Closed vessel system
       6.1.1 Microwave unit
       6.1.2 Digestion vessels
   6.2 Semi-open vessel system
       6.2.1 Microwave unit
       6.2.2 Digestion vessels
   6.3 General equipment
7 Reagents
8 Interferences and sources of error
   8.1 General informations
   8.2 Closed vessel system
   8.3 Semi-open vessel system
9 Procedure
   9.1 Blank test
   9.2 Procedure for closed vessels
       9.2.1 Amount of samples and reagents
       9.2.2 Digestion
       9.2.3 Complexation of HF
       9.2.4 Preparation of the solution for analysis
   9.3 Procedure for semi-open vessels
       9.3.1 Amount of samples
       9.3.2 Digestion and complexation of HF
       9.3.3 Preparation of the solution for analysis
10 Test report
Annex A (normative) Calibration of the powder adjustment
Annex B (informative) Validation
Bibliography

Gives methods of microwave assisted digestion with hydrofluoric (HF), nitric (HNO[3]) and hydrochloric (HCL) acid mixture. Solutions produced by the methods are suitable for analysis e.g. by atomic absorption spectrometry (FLAAS, HGAAS, CVAAS, GFAAS), inductively coupled plasma emission spectrometry (ICP-OES) and inductive coupled plasma mass spectrometry (ICP-MS).

Committee
TC 224
DocumentType
Standard
PublisherName
Osterreichisches Normungsinstitut/Austrian Standards
Status
Withdrawn
SupersededBy

Standards Relationship
NF EN 13656 : 2003 Identical
NS EN 13656 : 1ED 2002 Identical
DIN EN 13656:2003-01 Identical
NBN EN 13656 : 2002 Identical
SN EN 13656 : 2002 Identical
UNE-EN 13656:2003 Identical
EN 13656:2002 Identical
NEN EN 13656 : 2002 Identical
BS EN 13656:2002 Identical
I.S. EN 13656:2002 Identical
UNI EN 13656 : 2004 Identical

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