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  • PD CEN/TS 13649:2014

    Current The latest, up-to-date edition.

    Stationary source emissions. Determination of the mass concentration of individual gaseous organic compounds. Sorptive sampling method followed by solvent extraction or thermal desorption

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  31-12-2014

    Publisher:  British Standards Institution

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Apparatus and materials
    6 Sampling procedure
    7 Analytical procedure
    8 Calculation of results
    9 Quality control
    10 Report
    Annex A (normative) - Sample trains
    Annex B (informative) - Solvent extraction of activated
            charcoal tubes
    Annex C (informative) - Additional information on flue
            gas sampling using thermal desorption tubes
    Annex D (informative) - Validation of monitoring methods
            for speciated organic substances in stack gas
    Annex E (informative) - Safety measures
    Bibliography

    Abstract - (Show below) - (Hide below)

    Defines procedures for the sampling, preparation and analysis of individual volatile organic compounds (VOCs) in waste gas, such as those arising from solvent using processes.

    Scope - (Show below) - (Hide below)

    This Technical Specification specifies procedures for the sampling, preparation and analysis of individual volatile organic compounds (VOCs) in waste gas, such as those arising from solvent using processes. Sampling occurs by adsorption on sorbents, preparation by solvent extraction or thermodesorption and analysis by gas chromatography. Examples of individual VOC are given in relevant industry sector BAT Reference documents (BREFs). The results obtained are expressed as the mass concentration (mg/m 3) of the individual gaseous organic compounds. This document is suitable for measuring individual VOCs whose ranges vary depending on compound and test method, refer to AnnexB and C. This Technical Specification may be used to meet the monitoring requirements of the Industrial Emission Directive (IED) and associated supporting documents. This Technical Specification is not suitable for measuring total organic carbon (TOC). For the measurement of the mass concentration of total organic carbon then EN12619 [3] is applicable.

    General Product Information - (Show below) - (Hide below)

    Committee EH/2/1
    Development Note Supersedes BS EN 13649 & 11/30243100 DC. (12/2014)
    Document Type Standard
    Publisher British Standards Institution
    Status Current
    Supersedes

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 3686 : 2013 : REDLINE Standard Practice for Sampling Atmospheres to Collect Organic Compound Vapors (Activated Charcoal Tube Adsorption Method)
    CEN/TS 14793:2005 Stationary source emission - Intralaboratory validation procedure for an alternative method compared to a reference method
    ISO 14956:2002 Air quality Evaluation of the suitability of a measurement procedure by comparison with a required measurement uncertainty
    EN ISO 16017-1:2000 Indoor, ambient and workplace air - Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography - Part 1: Pumped sampling (ISO 16017-1:2000)
    EN 1076:2009 Workplace exposure - Procedures for measuring gases and vapours using pumped samplers - Requirements and test methods
    ISO 16017-1:2000 Indoor, ambient and workplace air — Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography — Part 1: Pumped sampling
    EN 15259:2007 Air quality - Measurement of stationary source emissions - Requirements for measurement sections and sites and for the measurement objective, plan and report
    EN 12619:2013 Stationary source emissions - Determination of the mass concentration of total gaseous organic carbon - Continuous flame ionisation detector method
    EN ISO 14956 : 2002 AIR QUALITY - EVALUATION OF THE SUITABILITY OF A MEASUREMENT PROCEDURE BY COMPARISON WITH A REQUIRED MEASUREMENT UNCERTAINTY
    ISO 16000-6:2011 Indoor air Part 6: Determination of volatile organic compounds in indoor and test chamber air by active sampling on Tenax TA sorbent, thermal desorption and gas chromatography using MS or MS-FID
    ISO/IEC Guide 98-3:2008 Uncertainty of measurement — Part 3: Guide to the expression of uncertainty in measurement (GUM:1995)
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